Absolute configuration assignment and enantiopurity determination of chiral alkaloids and coumarins derived from O- and C-prenyl epoxides

Absolute configuration assignment and enantiopurity determination of chiral alkaloids and coumarins derived from O- and C-prenyl epoxides

A combination method of ozonolysis and chiral stationary phase (CSP)-GC-MS analysis has been developed to determine the enantiopurity values and absolute configurations of a range of alkaloid and coumarin hemiterpenoids derived from C- and O-prenyl epoxides.

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Bibliographic Details
Published in:Chemical communications (Cambridge, England) no. 24; p. 3070
Main Authors: Boyd, Derek R, Sharma, Narain D, Loke, Pui L, Malone, John F, McRoberts, W Colin, Hamilton, John T G
Format: Journal Article
Language:English
Published: England 21-12-2002
Subjects:
Alkaloids - chemistry
Coumarins - chemistry
Epoxy Compounds - chemistry
Molecular Conformation
Stereoisomerism
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Description
Summary:A combination method of ozonolysis and chiral stationary phase (CSP)-GC-MS analysis has been developed to determine the enantiopurity values and absolute configurations of a range of alkaloid and coumarin hemiterpenoids derived from C- and O-prenyl epoxides.
ISSN:1359-7345
DOI:10.1039/b208978e