Matrix effect in liquid chromatography–electrospray ionization mass spectrometry analysis of benzoxazinoid derivatives in plant material
Despite the increasing success of liquid chromatography (LC) coupled to mass spectrometry (MS), matrix effects have limited the ESI applications. Matrix effects result from co-eluting residual matrix components affecting the ionization efficiency of target analytes and can lead to erroneous results....
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| Published in: | Journal of Chromatography A Vol. 1157; no. 1; pp. 108 - 114 |
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| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
20-07-2007
Elsevier |
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| Abstract | Despite the increasing success of liquid chromatography (LC) coupled to mass spectrometry (MS), matrix effects have limited the ESI applications. Matrix effects result from co-eluting residual matrix components affecting the ionization efficiency of target analytes and can lead to erroneous results. The present work evaluates the LC–electrospray ionization (ESI)-MS behaviour of benzoxazinoid derivatives in wheat plant material as a case where endogenous matrix components were found to interfere with the ionization of target analytes. When LC–MS was applied to the analysis of foliage and root extracts, significant signal suppressions were observed. To compensate for this matrix signal suppression, different methods were applied: the use of internal standards, the application of standard dilution method and the dilution of the extracts before instrumental determination. The results obtained indicated that evaluation of matrix effects should become an integrated part of quantitative LC–ESI-MS method development and validation. |
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| AbstractList | Despite the increasing success of liquid chromatography (LC) coupled to mass spectrometry (MS), matrix effects have limited the ESI applications. Matrix effects result from co-eluting residual matrix components affecting the ionization efficiency of target analytes and can lead to erroneous results. The present work evaluates the LC-electrospray ionization (ESI)-MS behaviour of benzoxazinoid derivatives in wheat plant material as a case where endogenous matrix components were found to interfere with the ionization of target analytes. When LC-MS was applied to the analysis of foliage and root extracts, significant signal suppressions were observed. To compensate for this matrix signal suppression, different methods were applied: the use of internal standards, the application of standard dilution method and the dilution of the extracts before instrumental determination. The results obtained indicated that evaluation of matrix effects should become an integrated part of quantitative LC-ESI-MS method development and validation. |
| Author | Guillamón, M. Eljarrat, E. Barceló, D. Villagrasa, M. |
| Author_xml | – sequence: 1 givenname: M. surname: Villagrasa fullname: Villagrasa, M. – sequence: 2 givenname: M. surname: Guillamón fullname: Guillamón, M. – sequence: 3 givenname: E. surname: Eljarrat fullname: Eljarrat, E. email: eeeqam@cid.csic.es – sequence: 4 givenname: D. surname: Barceló fullname: Barceló, D. |
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| Keywords | Ion suppression Benzoxazinoid derivatives Benzoxazinones Electrospray ionization Benzoxazolinones LC–MS Matrix effect Wheat Allelochemicals Monocotyledones Chemical analysis Lactam HPLC chromatography Organic carbamate Electrospray Cereal crop Triticum Gramineae Angiospermae Bicyclic compound Aromatic compound Oxygen nitrogen heterocycle Below ground plant part Benzoxazole derivatives Root Coupled method Plant leaf LC-MS Spermatophyta Mass spectrometry Semiochemicals |
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| SubjectTerms | Agronomy. Soil science and plant productions Allelochemicals Benzoxazines - analysis Benzoxazinoid derivatives Benzoxazinones Benzoxazolinones Biological and medical sciences Chemical constitution Chromatography, Liquid - methods Economic plant physiology Electrospray ionization Fundamental and applied biological sciences. Psychology Ion suppression ionization LC–MS leaves liquid chromatography mass spectrometry Matrix effect plant extracts Plants - chemistry Reference Standards roots Spectrometry, Mass, Electrospray Ionization - methods Triticum aestivum Wheat |
| Title | Matrix effect in liquid chromatography–electrospray ionization mass spectrometry analysis of benzoxazinoid derivatives in plant material |
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