Efficient Synthetic Photocyclization for Phenacenes Using a Continuous Flow Reactor

Efficient Synthetic Photocyclization for Phenacenes Using a Continuous Flow Reactor

The continuous flow reaction technique has been applied to the photocyclization of 1,2-diarylethenes, the so-called Mallory reaction, to afford phenacenes in high chemical yields and efficiencies (114–288 mg h−1). The present technique will allow us to produce several grams of phenacenes at a time....

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Bibliographic Details
Published in:Chemistry letters Vol. 43; no. 7; pp. 994 - 996
Main Authors: Okamoto, Hideki, Takane, Takamitsu, Gohda, Shin, Kubozono, Yoshihiro, Sato, Kaori, Yamaji, Minoru, Satake, Kyosuke
Format: Journal Article
Language:English
Published: Tokyo The Chemical Society of Japan 05-07-2014
Chemical Society of Japan
Subjects:
Continuous flow
Reactors
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Summary:The continuous flow reaction technique has been applied to the photocyclization of 1,2-diarylethenes, the so-called Mallory reaction, to afford phenacenes in high chemical yields and efficiencies (114–288 mg h−1). The present technique will allow us to produce several grams of phenacenes at a time.
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ISSN:0366-7022
1348-0715
DOI:10.1246/cl.140182