Determination of Dihydrobenzoacridinone Structures by NMR, IR, and UV Spectroscopy and Mass Spectrometry

Determination of Dihydrobenzoacridinone Structures by NMR, IR, and UV Spectroscopy and Mass Spectrometry

Condensation of 2-naphthylamine, aromatic aldehydes, and dimedone was found to produce 9,10-dihydrobenzo[a] acridin-11-one derivatives according to PMR, 13 C NMR, and IR spectroscopy and mass spectrometry. Correlation spectroscopy showed that the carbonyl in the synthesized dihydrobenzoacridinone de...

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Bibliographic Details
Published in:Journal of applied spectroscopy Vol. 82; no. 6; pp. 915 - 919
Main Authors: Kozlov, N. G., Zhiharko, Yu. D., Skakovsky, E. D., Baranovsky, A. V., Ogorodnikova, M. M., Basalaeva, L. I.
Format: Journal Article
Language:English
Published: New York Springer US 2016
Springer
Subjects:
Aldehydes
Analytical Chemistry
Atomic/Molecular Structure and Spectra
Mass spectrometry
Nuclear magnetic resonance spectroscopy
Physics
Physics and Astronomy
three-component condensation
2-naphthylamine
spectroscopy
dihydrobenzoacridinones
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Summary:Condensation of 2-naphthylamine, aromatic aldehydes, and dimedone was found to produce 9,10-dihydrobenzo[a] acridin-11-one derivatives according to PMR, 13 C NMR, and IR spectroscopy and mass spectrometry. Correlation spectroscopy showed that the carbonyl in the synthesized dihydrobenzoacridinone derivatives was located on C 11 .
ISSN:0021-9037
1573-8647
DOI:10.1007/s10812-016-0204-6