Determination of cure-dependent properties of adhesives by thermal analysis using reaction kinetics and a novel experimental apparatus

This work deals with the determination of cure-dependent mechanical properties, especially the modulus, and the degree of cure. Therefore kinetic methods will be used to determine this degree of cure in addition to the direct measurement by differential scanning calorimetry. Furthermore, the experim...

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Bibliographic Details
Published in:	International journal of adhesion and adhesives Vol. 68; pp. 411 - 417
Main Authors:	Schiel, M., Kahrs, J., Stammen, E., Dilger, K.
Format:	Journal Article
Language:	English
Published:	Elsevier Ltd 01-07-2016
Subjects:	Adhesion Adhesive Adhesives Cures Curing Differential scanning calorimetry Dynamic tests Mechanical properties Reaction kinetics Thermal analysis Curing Thermal analysis Adhesive Reaction kinetics
Online Access:	Get full text
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Summary:	This work deals with the determination of cure-dependent mechanical properties, especially the modulus, and the degree of cure. Therefore kinetic methods will be used to determine this degree of cure in addition to the direct measurement by differential scanning calorimetry. Furthermore, the experimental part focuses on the reproducible preparation of samples for dynamic mechanical analysis at different states in the curing reaction. In combination with additional rheological data these different techniques of thermal analysis show a good correlation and offer a deeper understanding of the development of the mechanical properties during cure.
Bibliography:	ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23
ISSN:	0143-7496 1879-0127
DOI:	10.1016/j.ijadhadh.2015.12.015