2-Amino-4-(4-chlorophenyl)-5,6,7,8,9,10-hexahydrobenzo[8]annulene-1,3-dicarbonitrile

2-Amino-4-(4-chlorophenyl)-5,6,7,8,9,10-hexahydrobenzo[8]annulene-1,3-dicarbonitrile

In the title compound, C20H18ClN3, the cyclooctene ring exhibits conformational disorder of two methylene groups with a site-occupation factor of 0.859 (6) for the major occupied site. In the crystal, molecules are connected into inversion dimers via pairs of weak N—H...N hydroge...

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Bibliographic Details
Published in:Acta crystallographica. Section E, Structure reports online Vol. 68; no. 9; p. o2692
Main Authors: Rajni Swamy, V., Srinivasan, N., Ranjith Kumar, R., Krishnakumar, R.V.
Format: Journal Article
Language:English
Published: International Union of Crystallography 01-09-2012
Online Access:Get full text
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Summary:In the title compound, C20H18ClN3, the cyclooctene ring exhibits conformational disorder of two methylene groups with a site-occupation factor of 0.859 (6) for the major occupied site. In the crystal, molecules are connected into inversion dimers via pairs of weak N—H...N hydrogen bonds, forming an R22(12) graph-set motif. These dimers are further connected via weak N—H...Cl interactions into chains running along [011]. There are also C—H...N interactions present in the crystal.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536812034861