Behavior of Hydroxyl Groups in Quartz Glass during Heat Treatment in the Range 750–950°C

The concentration of hydroxyl groups in different types of quartz glass tubes, the OH concentration profile across the tube wall, and the kinetics of OH removal during heat treatment in the temperature range 750–950°C have been studied by Fourier transform IR spectroscopy. For TK-I tubes, produced b...

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Published in:	Inorganic materials Vol. 54; no. 9; pp. 925 - 930
Main Authors:	Velmuzhov, A. P., Sukhanov, M. V., Churbanov, M. F., Kotereva, T. V., Shabarova, L. V., Kirillov, Yu. P.
Format:	Journal Article
Language:	English
Published:	Moscow Pleiades Publishing 2018 Springer Nature B.V
Subjects:	ACTIVATION ENERGY ANNEALING CHALCOGENIDES Chemistry Chemistry and Materials Science CONCENTRATION RATIO CONTROLLED ATMOSPHERES DIFFUSION Diffusion coefficient Electric arc melting FOURIER TRANSFORM SPECTROMETERS Fourier transforms GLASS Heat treating Heat treatment HYDROGEN Hydroxyl groups HYDROXYL RADICALS Industrial Chemistry/Chemical Engineering INFRARED SPECTRA Infrared spectroscopy Inorganic Chemistry MATERIALS SCIENCE QUARTZ REACTION KINETICS Silica glass TEMPERATURE RANGE 1000-4000 K TUBES quartz glass diffusion OH groups IR spectroscopy
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Abstract	The concentration of hydroxyl groups in different types of quartz glass tubes, the OH concentration profile across the tube wall, and the kinetics of OH removal during heat treatment in the temperature range 750–950°C have been studied by Fourier transform IR spectroscopy. For TK-I tubes, produced by vacuum electromelting of quartz, followed by annealing in a hydrogen atmosphere, we have calculated the diffusion coefficient of OH groups in this temperature range and the activation energy for diffusion: 215 ± 10 kJ/mol. We have found heat treatment conditions that ensure a considerable decrease in the concentration of OH groups in quartz tubes that are used in the fabrication of reactors for the preparation of extrapure chalcogenide glasses.
AbstractList	The concentration of hydroxyl groups in different types of quartz glass tubes, the OH concentration profile across the tube wall, and the kinetics of OH removal during heat treatment in the temperature range 750–950°C have been studied by Fourier transform IR spectroscopy. For TK-I tubes, produced by vacuum electromelting of quartz, followed by annealing in a hydrogen atmosphere, we have calculated the diffusion coefficient of OH groups in this temperature range and the activation energy for diffusion: 215 ± 10 kJ/mol. We have found heat treatment conditions that ensure a considerable decrease in the concentration of OH groups in quartz tubes that are used in the fabrication of reactors for the preparation of extrapure chalcogenide glasses.
Author	Shabarova, L. V. Kirillov, Yu. P. Churbanov, M. F. Sukhanov, M. V. Velmuzhov, A. P. Kotereva, T. V.
Author_xml	– sequence: 1 givenname: A. P. surname: Velmuzhov fullname: Velmuzhov, A. P. email: velmuzhov.ichps@mail.ru organization: Devyatykh Institute of Chemistry of High-Purity Substances, Russian Academy of Sciences – sequence: 2 givenname: M. V. surname: Sukhanov fullname: Sukhanov, M. V. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Russian Academy of Sciences – sequence: 3 givenname: M. F. surname: Churbanov fullname: Churbanov, M. F. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Russian Academy of Sciences – sequence: 4 givenname: T. V. surname: Kotereva fullname: Kotereva, T. V. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Russian Academy of Sciences – sequence: 5 givenname: L. V. surname: Shabarova fullname: Shabarova, L. V. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Russian Academy of Sciences – sequence: 6 givenname: Yu. P. surname: Kirillov fullname: Kirillov, Yu. P. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Russian Academy of Sciences
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SubjectTerms	ACTIVATION ENERGY ANNEALING CHALCOGENIDES Chemistry Chemistry and Materials Science CONCENTRATION RATIO CONTROLLED ATMOSPHERES DIFFUSION Diffusion coefficient Electric arc melting FOURIER TRANSFORM SPECTROMETERS Fourier transforms GLASS Heat treating Heat treatment HYDROGEN Hydroxyl groups HYDROXYL RADICALS Industrial Chemistry/Chemical Engineering INFRARED SPECTRA Infrared spectroscopy Inorganic Chemistry MATERIALS SCIENCE QUARTZ REACTION KINETICS Silica glass TEMPERATURE RANGE 1000-4000 K TUBES
Title	Behavior of Hydroxyl Groups in Quartz Glass during Heat Treatment in the Range 750–950°C
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