Microwave synthesis of secondary phosphines and phosphine oxides from red phosphorus and allyl(methoxy)benzenes in KOH-DMSO

Microwave synthesis of secondary phosphines and phosphine oxides from red phosphorus and allyl(methoxy)benzenes in KOH-DMSO

Bis[1-(methoxyphenyl)propan-2-yl]phosphines and bis[1-(methoxyphenyl)propan-2-yl]phosphine oxides were synthesized by phosphorylation of allyl(methoxy)benzenes in the system red phosphorus-KOH · 0.5 H 2 O-DMSO under microwave irradiation.

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Bibliographic Details
Published in:Russian journal of organic chemistry Vol. 50; no. 10; pp. 1438 - 1442
Main Authors: Kuimov, V. A., Malysheva, S. F., Artem’ev, A. V., Kenzhetaeva, S. O., Belogorlova, N. A., Komarova, T. N., Gusarova, N. K., Trofimov, B. A.
Format: Journal Article
Language:English
Published: Moscow Pleiades Publishing 01-10-2014
Subjects:
Chemistry
Chemistry and Materials Science
Organic Chemistry
Allyl
Phosphine Oxide
Microwave Synthesis
Phosphine
Phosphinic Acid
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Description
Summary:Bis[1-(methoxyphenyl)propan-2-yl]phosphines and bis[1-(methoxyphenyl)propan-2-yl]phosphine oxides were synthesized by phosphorylation of allyl(methoxy)benzenes in the system red phosphorus-KOH · 0.5 H 2 O-DMSO under microwave irradiation.
ISSN:1070-4280
1608-3393
DOI:10.1134/S1070428014100078