A convenient strategy for the synthesis of 3,5-diaryl-1,2,4-thiadiazoles: oxidative dimerization of arylthioamides using CC–DMSO in PEG-400

An inexpensive and effective preparative protocol for the highly efficient synthesis of structurally diverse 3,5-diaryl-1,2,4-thiadiazoles at ambient temperature with 2,4,6-trichloro-1,3,5-triazine (CC) and DMSO in polyethylene glycol 400 (PEG-400) as solvent is described. Graphical abstract

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Bibliographic Details
Published in:	Monatshefte für Chemie Vol. 141; no. 6; pp. 649 - 651
Main Authors:	Khosropour, Ahmad Reza, Noei, Jalil
Format:	Journal Article
Language:	English
Published:	Vienna Springer Vienna 01-06-2010
Subjects:	Analytical Chemistry Chemistry Chemistry and Materials Science Chemistry/Food Science Inorganic Chemistry Organic Chemistry Original Paper Physical Chemistry Theoretical and Computational Chemistry Thioamides Polyethylene glycol Room temperature Dimethyl sulfoxide 2,4,6-Trichloro-1,3,5-triazine
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Description
Summary:	An inexpensive and effective preparative protocol for the highly efficient synthesis of structurally diverse 3,5-diaryl-1,2,4-thiadiazoles at ambient temperature with 2,4,6-trichloro-1,3,5-triazine (CC) and DMSO in polyethylene glycol 400 (PEG-400) as solvent is described. Graphical abstract
ISSN:	0026-9247 1434-4475
DOI:	10.1007/s00706-010-0295-3