Crystal structure of palladium(II) complex with 2,2′-dipyridylamine and 4-toluenesulfonyl-L-serine
The [Pd(dpa)(tsser)] complex ( 1 ) is prepared from the reaction of PdCl 2 and 2,2′-dipyridylamine (dpa) with 4-toluenesulfonyl-L-serine (tsserH 2 ). This complex is characterized by spectral methods (IR, UV-Vis, 1 H NMR, and luminescence), elemental analysis, thermal analysis (TG, DTA), and single...
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| Published in: | Journal of structural chemistry Vol. 57; no. 3; pp. 534 - 541 |
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| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
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Pleiades Publishing
01-05-2016
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| Abstract | The [Pd(dpa)(tsser)] complex (
1
) is prepared from the reaction of PdCl
2
and 2,2′-dipyridylamine (dpa) with 4-toluenesulfonyl-L-serine (tsserH
2
). This complex is characterized by spectral methods (IR, UV-Vis,
1
H NMR, and luminescence), elemental analysis, thermal analysis (TG, DTA), and single crystal X-ray diffraction. X-ray structure determinations show that in this complex, Pd
II
atoms are four-coordinated in a distorted square-planar configuration by two N atoms from a bidentate 2,2′-dipyridylamine ligand and one N atom and one O atom from a bidentate tsser
2–
ligand. |
|---|---|
| AbstractList | The [Pd(dpa)(tsser)] complex (
1
) is prepared from the reaction of PdCl
2
and 2,2′-dipyridylamine (dpa) with 4-toluenesulfonyl-L-serine (tsserH
2
). This complex is characterized by spectral methods (IR, UV-Vis,
1
H NMR, and luminescence), elemental analysis, thermal analysis (TG, DTA), and single crystal X-ray diffraction. X-ray structure determinations show that in this complex, Pd
II
atoms are four-coordinated in a distorted square-planar configuration by two N atoms from a bidentate 2,2′-dipyridylamine ligand and one N atom and one O atom from a bidentate tsser
2–
ligand. |
| Author | Amani, V. Bahrami, H. Mehdipour, E. Shamaei, S. |
| Author_xml | – sequence: 1 givenname: E. surname: Mehdipour fullname: Mehdipour, E. email: e_mehdipour@yahoo.com organization: Department of Chemistry, Faculty of Science, Lorestan University – sequence: 2 givenname: H. surname: Bahrami fullname: Bahrami, H. organization: Department of Chemistry, Faculty of Science, Lorestan University – sequence: 3 givenname: S. surname: Shamaei fullname: Shamaei, S. organization: Department of Chemistry, Faculty of Science, Khoramabad Branch, Islamic Azad University – sequence: 4 givenname: V. surname: Amani fullname: Amani, V. organization: Young Researchers and Elite Club, Yadegar-e-Imam Khomeini (RAH) Branch, Islamic Azad University |
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| Cites_doi | 10.1021/jm060436a 10.1016/j.ica.2011.07.022 10.1021/jm990492u 10.1007/BF01038377 10.1039/C3NJ01281F 10.1016/S0162-0134(99)00105-1 10.1080/00958972.2013.767447 10.1016/j.ejmech.2011.08.037 10.3233/MGC-2012-0075 10.5012/bkcs.2008.29.3.679 10.2298/HEMIND110928096I 10.1111/jphp.12162 10.1039/C1MT00144B 10.1016/j.ica.2010.03.077 10.1007/s00280-008-0721-y 10.1016/j.ejmech.2012.09.052 10.1016/j.ccr.2008.09.011 10.1016/j.poly.2014.04.064 10.1080/00958972.2012.713102 10.1016/j.ejmech.2009.10.029 10.1016/j.bmc.2013.03.073 10.1016/S0010-8545(00)80455-5 10.1016/j.saa.2011.08.034 10.2174/1871520610909030356 10.2174/157341291001140102103324 10.1016/j.ejmech.2010.08.058 10.1039/c3gc40645h 10.1016/0277-5387(96)00303-8 10.1016/j.bmcl.2014.02.056 10.1248/cpb.56.908 10.1016/j.poly.2011.05.012 10.1107/S0021889899006020 10.1107/S0108767307043930 10.1002/anie.201400134 10.1007/s12039-013-0531-6 10.1021/am900932z 10.1107/S0021889897003117 10.1071/CH12549 10.1007/s00706-011-0607-2 10.1016/0277-5387(95)00545-5 10.1080/00958972.2011.653638 10.1007/s13738-012-0209-x 10.1016/0584-8539(71)80028-4 |
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| Keywords | 2,2′-dipyridylamine differential thermal analyses 4-toluenesulfonyl-L-serine luminescent properties thermal gravimetric crystal structure palladium(II) complex |
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| Snippet | The [Pd(dpa)(tsser)] complex (
1
) is prepared from the reaction of PdCl
2
and 2,2′-dipyridylamine (dpa) with 4-toluenesulfonyl-L-serine (tsserH
2
). This... |
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| SubjectTerms | Atomic Atomic/Molecular Structure and Spectra Chemistry Chemistry and Materials Science Inorganic Chemistry Molecular Optical and Plasma Physics Physical Chemistry Solid State Physics |
| Title | Crystal structure of palladium(II) complex with 2,2′-dipyridylamine and 4-toluenesulfonyl-L-serine |
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