Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions

Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions

Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and compl...

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Bibliographic Details
Published in:Eclética química Vol. 34; no. 2; pp. 15 - 21
Main Authors: De Siqueira, Adriano Buzutti, De Carvalho, Cláudio Teodoro, Ionashiro, Elias Yuki, Ionashiro, Massao
Format: Journal Article
Language:English
Published: Universidade Estadual Paulista 01-04-2018
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Summary:Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds.
ISSN:1678-4618
1678-4618
DOI:10.26850/1678-4618eqj.v34.2.2009.p15-21