The detection of the 25B-NBOMe derivative of phenylethylamine in the biological material

This article is focused on the conditions for the detection and identification of 2-[4-bromo-2.5-dimethoxyl]-N-[(2-methoxyphenyl)methyl] ethamine (25B-NBOMe) and its major metabolites by the combination of the HPLC/MS/MS techniques. The high-resolution mass spectra obtained with the use of a linear...

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Bibliographic Details
Published in:	Sudebno-meditsinskaia ekspertiza Vol. 62; no. 2; p. 34
Main Authors:	Barsegyan, S S, Kiryushin, A N, Eroshchenko, N N, Tuaeva, N O, Nosyrev, A E, Kirilyuk, A A
Format:	Journal Article
Language:	English Russian
Published:	Russia (Federation) 2019
Subjects:	Anisoles - analysis Chromatography, High Pressure Liquid Forensic Sciences - methods Phenethylamines - analysis Tandem Mass Spectrometry narcotic drugs metabolites 25B-NBOMe tandem mass-spectrometry
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Summary:	This article is focused on the conditions for the detection and identification of 2-[4-bromo-2.5-dimethoxyl]-N-[(2-methoxyphenyl)methyl] ethamine (25B-NBOMe) and its major metabolites by the combination of the HPLC/MS/MS techniques. The high-resolution mass spectra obtained with the use of a linear ion trap are described. The results of the study give evidence of the possibility for the detection of the analytes within 24 hours after drug consumption and within 3 months after the storage of the biological material of interest in a refrigerator at a temperature of 3-5 °C. The data obtained confirmed high stability of 2-(4-bromo-2.5-dimethoxyl]-N-[(2-methoxyphenyl)methyl] ethamine and its metabolites in the biological tissues.
ISSN:	0039-4521
DOI:	10.17116/sudmed20196202134