Intercomparison of Calorimetry, Raman Spectroscopy, and Second Harmonic Generation Applied to Solid−Solid Phase Transitions

This paper compares several different observables for use in measuring the kinetics of solid−solid phase transitions. Relative advantages and disadvantages for each technique are described, and a direct comparison of results is made for the beta to delta polymorphic phase transition of the energetic...

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Bibliographic Details
Published in:	The journal of physical chemistry. A, Molecules, spectroscopy, kinetics, environment, & general theory Vol. 113; no. 35; pp. 9650 - 9657
Main Authors:	Smilowitz, L, Henson, B. F, Romero, J. J
Format:	Journal Article
Language:	English
Published:	United States American Chemical Society 03-09-2009
Subjects:	A: Kinetics, Spectroscopy
Online Access:	Get full text
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Summary:	This paper compares several different observables for use in measuring the kinetics of solid−solid phase transitions. Relative advantages and disadvantages for each technique are described, and a direct comparison of results is made for the beta to delta polymorphic phase transition of the energetic nitramine, octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine.
Bibliography:	ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23
ISSN:	1089-5639 1520-5215
DOI:	10.1021/jp902111c