A Simple Low- to Medium-Pressure Hydrogenation Manifold
A hydrogenation/reactive gas manifold designed for rapid screening of a wide range of reaction conditions on limited amounts of material is described. The manifold delivers reactive gas to four independent reactor ports, each equipped with inerting, pressurizing, and venting valves, as well as therm...
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| Published in: | Organic process research & development Vol. 1; no. 2; pp. 179 - 181 |
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| Main Authors: | , |
| Format: | Journal Article |
| Language: | English |
| Published: |
American Chemical Society
01-03-1997
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| Online Access: | Get full text |
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| Summary: | A hydrogenation/reactive gas manifold designed for rapid screening of a wide range of reaction conditions on limited amounts of material is described. The manifold delivers reactive gas to four independent reactor ports, each equipped with inerting, pressurizing, and venting valves, as well as thermocouple capability. Magnetic stirring and bath/mantle temperature control are used in the individual reactions; the reaction vessels are available in a wide range of sizes. Delivery of different pressures of reactive gas to the individual reactions is enabled by insertion of in-line regulators between ports. The modular nature of the design allows additional reaction ports to be added as needed. The manifold accommodates reaction pressures of up to 60 psig. |
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| ISSN: | 1083-6160 1520-586X |
| DOI: | 10.1021/op970203g |