Effect of Solvent and Reagent Ratio on the Size of Gold Nanoparticles in Nanocomposites Formed in the Redox Reaction of H[AuCl.sub.4] with Two-Dimensional MoS.sub.2
It was shown that the redox reaction of tetrachloroauric acid with exfoliated molybdenum disulfide leads to the formation of Au@MoS.sub.2nanocomposites containing nanoparticles of metallic gold. The reduction rate of the gold(III) is higher in dimethylformamide than in N-methylpyrrolidone. It was sh...
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| Published in: | Theoretical and experimental chemistry p. 109 |
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| Language: | English |
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01-05-2015
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| Abstract | It was shown that the redox reaction of tetrachloroauric acid with exfoliated molybdenum disulfide leads to the formation of Au@MoS.sub.2nanocomposites containing nanoparticles of metallic gold. The reduction rate of the gold(III) is higher in dimethylformamide than in N-methylpyrrolidone. It was shown that the size of the nanoparticles can be controlled by varying the concentration ratio of the reagents from 2 : 1 to 5 : 1, and under the investigated conditions it increases stepwise from 6.5 to 13 nm. |
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| AbstractList | It was shown that the redox reaction of tetrachloroauric acid with exfoliated molybdenum disulfide leads to the formation of Au@MoS.sub.2nanocomposites containing nanoparticles of metallic gold. The reduction rate of the gold(III) is higher in dimethylformamide than in N-methylpyrrolidone. It was shown that the size of the nanoparticles can be controlled by varying the concentration ratio of the reagents from 2 : 1 to 5 : 1, and under the investigated conditions it increases stepwise from 6.5 to 13 nm. |
| Audience | Academic |
| Author | Lampeka, Ya. D Tsymbal, L. V |
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| Copyright | COPYRIGHT 2015 Springer |
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| DOI | 10.1007/s11237-015-9404-z |
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| SubjectTerms | Chemical tests and reagents Dimethylformamide Nanoparticles |
| Title | Effect of Solvent and Reagent Ratio on the Size of Gold Nanoparticles in Nanocomposites Formed in the Redox Reaction of H[AuCl.sub.4] with Two-Dimensional MoS.sub.2 |
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