Characterization and Phosphate Adsorption Capability of Novel Nickel–Aluminum–Zirconium Complex Hydroxide
In this study, the adsorption capability of phosphate ion using a novel tri-metals complex hydroxide was evaluated for preventing the eutrophication in water environment. A nickel–aluminum–zirconium complex hydroxide (NAZ) was synthesized using each inorganic sulfate mixing ratio of 0.9 : 1.0 : 0.1...
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| Published in: | Chemical & pharmaceutical bulletin Vol. 68; no. 3; pp. 292 - 297 |
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The Pharmaceutical Society of Japan
01-03-2020
Pharmaceutical Society of Japan Japan Science and Technology Agency |
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| Abstract | In this study, the adsorption capability of phosphate ion using a novel tri-metals complex hydroxide was evaluated for preventing the eutrophication in water environment. A nickel–aluminum–zirconium complex hydroxide (NAZ) was synthesized using each inorganic sulfate mixing ratio of 0.9 : 1.0 : 0.1 and was calcined at different temperatures. The characteristics of the NAZ were analyzed by scanning electron microscopy images, X-ray diffraction analysis, elemental distribution, and binding energy. Moreover, the amount adsorbed of phosphate ion onto uncalcined and calcined NAZ was measured. That of phosphate ions onto the uncalcined was the largest of all. These results suggested that the adsorption of phosphate ions tends to depend on the physicochemical properties (e.g., amount of hydroxyl groups, pore volumes, and pH) of the adsorbents. Moreover, the adsorption mechanism of phosphate ions was evaluated on the basis of binding energy and elemental analysis. After adsorption, the binding energy of phosphorus P (2s and 2p) peaked and the sulfur peak intensity S(2s) reduced. This result indicated that the adsorption mechanism of phosphate would be exchanged with sulfate ions. |
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| AbstractList | In this study, the adsorption capability of phosphate ion using a novel tri-metals complex hydroxide was evaluated for preventing the eutrophication in water environment. A nickel–aluminum–zirconium complex hydroxide (NAZ) was synthesized using each inorganic sulfate mixing ratio of 0.9 : 1.0 : 0.1 and was calcined at different temperatures. The characteristics of the NAZ were analyzed by scanning electron microscopy images, X-ray diffraction analysis, elemental distribution, and binding energy. Moreover, the amount adsorbed of phosphate ion onto uncalcined and calcined NAZ was measured. That of phosphate ions onto the uncalcined was the largest of all. These results suggested that the adsorption of phosphate ions tends to depend on the physicochemical properties (e.g., amount of hydroxyl groups, pore volumes, and pH) of the adsorbents. Moreover, the adsorption mechanism of phosphate ions was evaluated on the basis of binding energy and elemental analysis. After adsorption, the binding energy of phosphorus P (2s and 2p) peaked and the sulfur peak intensity S(2s) reduced. This result indicated that the adsorption mechanism of phosphate would be exchanged with sulfate ions. In this study, the adsorption capability of phosphate ion using a novel tri-metals complex hydroxide was evaluated for preventing the eutrophication in water environment. A nickel–aluminum–zirconium complex hydroxide (NAZ) was synthesized using each inorganic sulfate mixing ratio of 0.9 : 1.0 : 0.1 and was calcined at different temperatures. The characteristics of the NAZ were analyzed by scanning electron microscopy images, X-ray diffraction analysis, elemental distribution, and binding energy. Moreover, the amount adsorbed of phosphate ion onto uncalcined and calcined NAZ was measured. That of phosphate ions onto the uncalcined was the largest of all. These results suggested that the adsorption of phosphate ions tends to depend on the physicochemical properties (e.g., amount of hydroxyl groups, pore volumes, and pH) of the adsorbents. Moreover, the adsorption mechanism of phosphate ions was evaluated on the basis of binding energy and elemental analysis. After adsorption, the binding energy of phosphorus P (2s and 2p) peaked and the sulfur peak intensity S(2s) reduced. This result indicated that the adsorption mechanism of phosphate would be exchanged with sulfate ions. Graphical Abstract |
| Author | Iijima, Shouko Toda, Megumu Otani, Masashi Nakamura, Takehiro Kawasaki, Naohito Ogata, Fumihiko |
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| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/32115537$$D View this record in MEDLINE/PubMed |
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| Cites_doi | 10.1007/s11270-012-1186-5 10.1007/BF02706760 10.1016/j.jcis.2006.03.026 10.1016/S0043-1354(97)00371-0 10.1016/j.cej.2011.03.102 10.1016/j.jcis.2010.05.068 10.1016/j.jcis.2015.02.048 10.1248/jhs.54.324 10.1016/j.chemosphere.2011.02.001 10.1016/j.jcis.2007.04.004 10.1080/10643389.2013.866621 10.1016/j.scitotenv.2016.03.151 10.1525/bio.2011.61.2.6 10.1016/j.jhazmat.2010.02.086 10.1016/j.powtec.2012.08.024 10.1016/j.watres.2018.09.005 10.2166/wst.2016.492 10.1016/j.seppur.2013.12.042 10.1016/j.watres.2016.03.063 10.1021/es025950u 10.1016/j.jhazmat.2007.06.033 10.1016/j.jhazmat.2008.05.131 10.1248/cpb.c15-00613 10.1016/j.watres.2008.12.030 10.1016/j.jcis.2005.12.054 10.1016/j.watres.2009.06.003 10.2166/wst.2018.273 10.1016/j.jece.2019.102897 10.1016/j.jiec.2015.11.005 10.1246/nikkashi.1978.1057 10.1016/j.jhazmat.2012.01.069 |
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| SubjectTerms | Adsorption Aluminum Aluminum - chemistry Binding energy Coordination Complexes - chemical synthesis Coordination Complexes - chemistry Coordination compounds Energy Energy distribution Eutrophication Evaluation Heavy metals Hydroxides - chemistry Hydroxyl groups Ions Nickel Nickel - chemistry nickel–aluminum–zirconium complex hydroxide Particle Size Phosphate phosphate ion Phosphates - chemistry Phosphorus Physicochemical properties Roasting Scanning electron microscopy Sulfates Sulfur Surface Properties Thermodynamics X-ray diffraction Zirconium Zirconium - chemistry |
| Title | Characterization and Phosphate Adsorption Capability of Novel Nickel–Aluminum–Zirconium Complex Hydroxide |
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