Effects of water-storage on the physical and ultramorphological features of adhesives and primer/adhesive mixtures

The aims of this study were to evaluate the ultimate tensile strength (UTS) and elastic modulus (E) of adhesives, and primer/adhesive mixtures after aging for 6 months in water or oil; and to compare silver uptake patterns under the TEM. A one-step self-etching adhesive (One-up Bond F: OB), two two-...

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Published in:	Dental Materials Journal Vol. 29; no. 6; pp. 697 - 705
Main Authors:	REIS, Andre F., CARRILHO, Marcela R.O., GHANAME, Eduardo, PEREIRA, Patricia N.R., GIANNINI, Marcelo, NIKAIDO, Toru, TAGAMI, Junji
Format:	Journal Article
Language:	English
Published:	Japan The Japanese Society for Dental Materials and Devices 2010 Japanese Society for Dental Materials and Devices
Subjects:	Adhesiveness Adhesives Bisphenol A-Glycidyl Methacrylate - chemistry Chemical Phenomena Dental Stress Analysis - instrumentation Dentin-Bonding Agents - chemistry Dentistry Diffusion Elastic Modulus Humans Materials Testing Methacrylates - chemistry Microscopy, Electron, Transmission Mineral Oil - chemistry Polymethacrylic Acids - chemistry Resin Cements - chemistry Silver Staining Stress, Mechanical Tensile Strength Time Factors Transmission electron microscopy Ultimate tensile strength Water - chemistry
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Abstract	The aims of this study were to evaluate the ultimate tensile strength (UTS) and elastic modulus (E) of adhesives, and primer/adhesive mixtures after aging for 6 months in water or oil; and to compare silver uptake patterns under the TEM. A one-step self-etching adhesive (One-up Bond F: OB), two two-step self-etching primers (SE Bond: SE and Protect Bond: CP), and two etch-and-rinse systems (Single Bond: SB and Prime&Bond NT: PB) were used. Bonding and primer solutions of self-etching systems were also mixed (SE+P and CP+P). Most adhesives presented decreased UTS after water-storage. Similar or increased UTS was observed after oil storage. Except for SB, E values did not change after water-storage, but they increased after storage in oil. OB, CP+P and SE+P presented more silver uptake. The effects of water-storage were material-dependent, and significantly affected the mechanical properties and silver uptake patterns of adhesives.
AbstractList	The aims of this study were to evaluate the ultimate tensile strength (UTS) and elastic modulus (E) of adhesives, and primer/adhesive mixtures after aging for 6 months in water or oil; and to compare silver uptake patterns under the TEM. A one-step self-etching adhesive (One-up Bond F: OB), two two-step self-etching primers (SE Bond: SE and Protect Bond: CP), and two etch-and-rinse systems (Single Bond: SB and Prime&Bond NT: PB) were used. Bonding and primer solutions of self-etching systems were also mixed (SE+P and CP+P). Most adhesives presented decreased UTS after water-storage. Similar or increased UTS was observed after oil storage. Except for SB, E values did not change after water-storage, but they increased after storage in oil. OB, CP+P and SE+P presented more silver uptake. The effects of water-storage were material-dependent, and significantly affected the mechanical properties and silver uptake patterns of adhesives. The aims of this study were to evaluate the ultimate tensile strength (UTS) and elastic modulus (E) of adhesives, and primer/adhesive mixtures after aging for 6 months in water or oil; and to compare silver uptake patterns under the TEM. A one-step self-etching adhesive (One-up Bond F: OB), two two-step self-etching primers (SE Bond: SE and Protect Bond: CP), and two etch-and-rinse systems (Single Bond: SB and Prime&Bond NT: PB) were used. Bonding and primer solutions of self-etching systems were also mixed (SE+P and CP+P). Most adhesives presented decreased UTS after water-storage. Similar or increased UTS was observed after oil storage. Except for SB, E values did not change after water-storage, but they increased after storage in oil. OB, CP+P and SE+P presented more silver uptake. The effects of water-storage were material-dependent, and significantly affected the mechanical properties and silver uptake patterns of adhesives.
Author	GHANAME, Eduardo REIS, Andre F. TAGAMI, Junji CARRILHO, Marcela R.O. PEREIRA, Patricia N.R. GIANNINI, Marcelo NIKAIDO, Toru
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Cites_doi	10.1002/(SICI)1097-4628(19990131)71:5<787::AID-APP12>3.0.CO;2-A 10.1016/j.dental.2005.05.005 10.1177/154405910508400204 10.1016/S0300-5712(98)00042-6 10.1046/j.1365-2842.1998.00309.x 10.1016/j.biomaterials.2004.01.026 10.1002/pol.1984.180220208 10.1016/j.dental.2006.10.006 10.1177/10454411010120020401 10.1177/154405910208100708 10.1002/pen.760200417 10.1002/jbm.b.30076 10.1002/(SICI)1099-0488(20000301)38:5<792::AID-POLB16>3.0.CO;2-H 10.1016/j.jdent.2004.08.004 10.1177/00220345000790060601 10.1016/S0109-5641(01)00046-X 10.1177/00220345990780041101 10.1016/S0142-9612(98)00215-4 10.1016/j.biomaterials.2005.04.052 10.1016/j.biomaterials.2005.09.037 10.1016/S0014-3057(00)00025-2 10.1007/BF00550593 10.1016/S0142-9612(03)00144-3 10.1016/j.dental.2005.11.020 10.1016/S0300-5712(02)00064-7 10.1016/S0109-5641(00)00075-0 10.1016/S0142-9612(02)00380-0 10.2341/06-13 10.1016/S0032-3861(98)00546-1 10.1002/jbm.b.30909 10.1016/S0142-9612(02)00521-5 10.4012/dmj.18.11 10.1016/j.dental.2004.06.001 10.1002/jbm.820270314 10.1111/j.1600-0722.2007.00452.x 10.1002/(SICI)1097-4636(19981205)42:3<465::AID-JBM17>3.3.CO;2-T
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SubjectTerms	Adhesiveness Adhesives Bisphenol A-Glycidyl Methacrylate - chemistry Chemical Phenomena Dental Stress Analysis - instrumentation Dentin-Bonding Agents - chemistry Dentistry Diffusion Elastic Modulus Humans Materials Testing Methacrylates - chemistry Microscopy, Electron, Transmission Mineral Oil - chemistry Polymethacrylic Acids - chemistry Resin Cements - chemistry Silver Staining Stress, Mechanical Tensile Strength Time Factors Transmission electron microscopy Ultimate tensile strength Water - chemistry
Title	Effects of water-storage on the physical and ultramorphological features of adhesives and primer/adhesive mixtures
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