Removal of Arsenic (III) from groundwater applying a reusable Mg-Fe-Cl layered double hydroxide
BACKGROUND Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this present research is to develop a LDH to treat arsenite (As(III)). Both batch and column sorption studies were conducted to assess the effect of LDH...
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| Published in: | Journal of chemical technology and biotechnology (1986) Vol. 90; no. 6; pp. 1160 - 1166 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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Chichester, UK
John Wiley & Sons, Ltd
01-06-2015
Wiley Subscription Services, Inc |
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| Abstract | BACKGROUND
Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this present research is to develop a LDH to treat arsenite (As(III)). Both batch and column sorption studies were conducted to assess the effect of LDH dosage, contact time, solution pH and initial As(III) concentrations on the As(III) removal performance. The potential re‐use of this sorbent was also investigated.
RESULTS
For 2 g L−1 of Mg‐Fe‐Cl LDH, As(III) in test solution can be reduced from 400 µg L−1 to <10 µg L−1 after a contact time of 2 h. High As(III) concentration in Bangladesh groundwater can be reduced to meet the national drinking water standards (<50 µg L−1). The maximum adsorption capacity of As(III) by Mg‐Fe‐Cl LDH is 14.6 mg g−1‐LDH. Further, reusability of this sorbent was at least 20 cycles of regeneration with effective As(III) removal between 93.0 and 98.5%. Moreover, As(III) removal was unaffected by the solution pH but affected by the co‐existing competing anions and concentration of As(III). Finally, the main mechanism of As(III) removal by Mg‐Fe‐Cl LDH was suggested to be chemical sorption together with anion and ligand exchange with interlayer Cl− and OH− ions.
CONCLUSION
High efficiency of sorption of As(III) by the developed Mg‐Fe‐Cl LDH was demonstrated in this study which is generally not the case for most other sorbent materials. Pilot‐scale trials are needed to explore the suitability of full application of the developed Mg‐Fe‐Cl LDH for the removal of As(III). © 2014 Society of Chemical Industry |
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| AbstractList | BACKGROUND Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this present research is to develop a LDH to treat arsenite (As(III)). Both batch and column sorption studies were conducted to assess the effect of LDH dosage, contact time, solution pH and initial As(III) concentrations on the As(III) removal performance. The potential re-use of this sorbent was also investigated. RESULTS For 2 g L super(-1) of Mg-Fe-Cl LDH, As(III) in test solution can be reduced from 400 mu g L super(-1) to <10 mu g L super(-1) after a contact time of 2 h. High As(III) concentration in Bangladesh groundwater can be reduced to meet the national drinking water standards (<50 mu g L super(-1)). The maximum adsorption capacity of As(III) by Mg-Fe-Cl LDH is 14.6 mg g super(-1)-LDH. Further, reusability of this sorbent was at least 20 cycles of regeneration with effective As(III) removal between 93.0 and 98.5%. Moreover, As(III) removal was unaffected by the solution pH but affected by the co-existing competing anions and concentration of As(III). Finally, the main mechanism of As(III) removal by Mg-Fe-Cl LDH was suggested to be chemical sorption together with anion and ligand exchange with interlayer Cl super(-) and OH super(-) ions. CONCLUSION High efficiency of sorption of As(III) by the developed Mg-Fe-Cl LDH was demonstrated in this study which is generally not the case for most other sorbent materials. Pilot-scale trials are needed to explore the suitability of full application of the developed Mg-Fe-Cl LDH for the removal of As(III). copyright 2014 Society of Chemical Industry BACKGROUND Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this present research is to develop a LDH to treat arsenite (As(III)). Both batch and column sorption studies were conducted to assess the effect of LDH dosage, contact time, solution pH and initial As(III) concentrations on the As(III) removal performance. The potential re-use of this sorbent was also investigated. RESULTS For 2 g L-1 of Mg-Fe-Cl LDH, As(III) in test solution can be reduced from 400 µg L-1 to <10 µg L-1 after a contact time of 2 h. High As(III) concentration in Bangladesh groundwater can be reduced to meet the national drinking water standards (<50 µg L-1). The maximum adsorption capacity of As(III) by Mg-Fe-Cl LDH is 14.6 mg g-1-LDH. Further, reusability of this sorbent was at least 20 cycles of regeneration with effective As(III) removal between 93.0 and 98.5%. Moreover, As(III) removal was unaffected by the solution pH but affected by the co-existing competing anions and concentration of As(III). Finally, the main mechanism of As(III) removal by Mg-Fe-Cl LDH was suggested to be chemical sorption together with anion and ligand exchange with interlayer Cl- and OH- ions. CONCLUSION High efficiency of sorption of As(III) by the developed Mg-Fe-Cl LDH was demonstrated in this study which is generally not the case for most other sorbent materials. Pilot-scale trials are needed to explore the suitability of full application of the developed Mg-Fe-Cl LDH for the removal of As(III). © 2014 Society of Chemical Industry BACKGROUND Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this present research is to develop a LDH to treat arsenite (As(III)). Both batch and column sorption studies were conducted to assess the effect of LDH dosage, contact time, solution pH and initial As(III) concentrations on the As(III) removal performance. The potential re‐use of this sorbent was also investigated. RESULTS For 2 g L−1 of Mg‐Fe‐Cl LDH, As(III) in test solution can be reduced from 400 µg L−1 to <10 µg L−1 after a contact time of 2 h. High As(III) concentration in Bangladesh groundwater can be reduced to meet the national drinking water standards (<50 µg L−1). The maximum adsorption capacity of As(III) by Mg‐Fe‐Cl LDH is 14.6 mg g−1‐LDH. Further, reusability of this sorbent was at least 20 cycles of regeneration with effective As(III) removal between 93.0 and 98.5%. Moreover, As(III) removal was unaffected by the solution pH but affected by the co‐existing competing anions and concentration of As(III). Finally, the main mechanism of As(III) removal by Mg‐Fe‐Cl LDH was suggested to be chemical sorption together with anion and ligand exchange with interlayer Cl− and OH− ions. CONCLUSION High efficiency of sorption of As(III) by the developed Mg‐Fe‐Cl LDH was demonstrated in this study which is generally not the case for most other sorbent materials. Pilot‐scale trials are needed to explore the suitability of full application of the developed Mg‐Fe‐Cl LDH for the removal of As(III). © 2014 Society of Chemical Industry |
| Author | Badruzzaman, A Borhan M Jiang, Jia-Qian Hargreaves, Justin S. J. Ashekuzzaman, S.M. McFarlane, Andrew R. Tarek, Mehedi Hasan |
| Author_xml | – sequence: 1 givenname: Jia-Qian surname: Jiang fullname: Jiang, Jia-Qian email: jiaqian.jiang@gcu.ac.uk organization: School of Engineering and Built Environment, Glasgow Caledonian University, Glasgow G4 0BA, Scotland, UK – sequence: 2 givenname: S.M. surname: Ashekuzzaman fullname: Ashekuzzaman, S.M. organization: School of Engineering and Built Environment, Glasgow Caledonian University, Glasgow G4 0BA, Scotland, UK – sequence: 3 givenname: Justin S. J. surname: Hargreaves fullname: Hargreaves, Justin S. J. organization: School of Chemistry, WestCHEM, Joseph Black Building, University of Glasgow, Glasgow G12 8QQScotland, UK – sequence: 4 givenname: Andrew R. surname: McFarlane fullname: McFarlane, Andrew R. organization: School of Chemistry, WestCHEM, Joseph Black Building, University of Glasgow, Glasgow G12 8QQScotland, UK – sequence: 5 givenname: A Borhan M surname: Badruzzaman fullname: Badruzzaman, A Borhan M organization: Department of Civil Engineering, Bangladesh University of Engineering and Technology, Dhaka-1000, Bangladesh – sequence: 6 givenname: Mehedi Hasan surname: Tarek fullname: Tarek, Mehedi Hasan organization: Department of Civil Engineering, Bangladesh University of Engineering and Technology, Dhaka-1000, Bangladesh |
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| References_xml | – volume: 239–240 start-page: 279 year: 2012 end-page: 288 article-title: Adsorption of arsenate on Cu/Mg/Fe/La layered double hydroxide from aqueous solutions publication-title: J Hazard Mater – volume: 10 start-page: 18 year: 2013 end-page: 46 article-title: Arsenic contaminated groundwater and its treatment options in Bangladesh publication-title: Int J Environ Res Public Health – volume: 5 start-page: 182 year: 2005 end-page: 190 article-title: Remediation technologies for arsenic contaminated drinking waters publication-title: J Soils Sediments – volume: 68 start-page: 4539 year: 2004 end-page: 4557 article-title: Mobility of arsenic in a Bangladesh aquifer: inferences from geochemical profiles, leaching data, and mineralogical characterization publication-title: Geochimica Cosmochimica Acta – year: 2005 – volume: 171 start-page: 665 year: 2009 end-page: 670 article-title: Adsorption of As(V) from water using Mg‐Fe‐based hydrotalcite (FeHT) publication-title: J Hazard Mater – volume: 333 start-page: 63 year: 2009 end-page: 70 article-title: Sorption/desorption of arsenate on/from Mg‐Al layered double hydroxides: influence of phosphate publication-title: J Col Int Sci – volume: 246 start-page: 97 year: 2014 end-page: 105 article-title: Study on the sorption–desorption‐regeneration performance of Ca‐ publication-title: Mg‐ and CaMg‐based layered double hydroxides for removing phosphate from water. Chem Eng J – volume: 70 start-page: 2017 year: 2006 end-page: 2027 article-title: Kinetics of arsenate sorptiondesorption from metal oxides: effect of residence time publication-title: Soil Sci Soc Am J – volume: 43 start-page: 79 year: 2009 end-page: 85 article-title: Arsenate adsorption by Mg/Al‐NO layered double hydroxides with varying the Mg/Al ratio publication-title: Appl Clay Sci – volume: 228 start-page: 731 year: 2013 end-page: 740 article-title: Performance and mechanism of Mg/Fe layered double hydroxides for fluoride and arsenate removal from aqueous solution publication-title: Chem Eng J – volume: 46 start-page: 4577 year: 2007 end-page: 4583 article-title: Laboratory study of boron removal by Mg/Al double‐layered hydroxides publication-title: Ind Eng Chem Res – volume: 35 start-page: 2049 year: 2001 end-page: 2057 article-title: Adsorption of arsenite and arsenate within activated alumina grains: equilibrium and kinetics publication-title: Water Res – volume: 8 start-page: 286 year: 2011 end-page: 304 article-title: A critical review of the separation of arsenic oxyanions from dilute aqueous solution publication-title: Int J Environ Waste Manage – volume: 328 start-page: 15 year: 2008 end-page: 20 article-title: Adsorption of tripolyphosphate from aqueous solution by Mg‐Al‐CO ‐layered double hydroxides publication-title: Colloid Surf A: Physicochem Eng Aspect – volume: 31 start-page: 305 year: 1983 end-page: 311 article-title: Anion‐exchange properties of hydrotalcite‐like compounds publication-title: Clays Clay Miner – volume: 61 start-page: 478 year: 2005 end-page: 483 article-title: Adsorption of arsenate by activated carbon prepared from oat hulls publication-title: Chemosphere – volume: 1 start-page: 191 year: 2012 end-page: 199 article-title: Development of novel inorganic adsorbent for water treatment publication-title: Curr Opin Chem Eng – volume: 61 start-page: 1411 year: 2010 end-page: 1417 article-title: Removal of arsenate from aqueous solution by nanocrystalline Mg/Al layered double hydroxide: sorption characteristics, prospects and challenges publication-title: Water Sci Technol – volume: 225 start-page: 704 year: 2013 end-page: 709 article-title: Effect of competing ligands on the sorption/desorption of arsenite on/from Mg–Fe layered double hydroxides (Mg–Fe‐LDH) publication-title: Chem Eng J – volume: 162 start-page: 440 year: 2009 end-page: 447 article-title: Arsenic adsorption from aqueous solution on synthetic zeolites publication-title: J Hazard Mater – volume: 38 start-page: 924 year: 2004 end-page: 931 article-title: Arsenic removal using mesoporous alumina prepared via a templating method publication-title: Environ Sci Technol – volume: 189 start-page: 564 year: 2011 end-page: 571 article-title: Sorption of arsenite and arsenate on ferrihydrite: effect of organic and inorganic ligands publication-title: J Hazard Mater – volume: 44 start-page: 89 year: 2001 end-page: 98 article-title: Removing arsenic from groundwater for the developing world publication-title: Water Sci Technol – volume: 17 start-page: 517 year: 2002 end-page: 568 article-title: A review of the source, behavior and distribution of arsenic in natural waters publication-title: App. Geochem – volume: 246 start-page: 97 year: 2014 ident: e_1_2_6_21_1 article-title: Study on the sorption–desorption‐regeneration performance of Ca‐ publication-title: Mg‐ and CaMg‐based layered double hydroxides for removing phosphate from water. 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Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this... BACKGROUND Layered double hydroxide compounds (LDHs) have been applied for the removal of oxyanions including arsenate (As(V)). However, the aim of this... |
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| SubjectTerms | arsenic removal Contact desorption drinking water treatment Groundwater Hydroxides layered double hydroxide (LDH) Magnesium Sorbents Sorption sorption, desorption |
| Title | Removal of Arsenic (III) from groundwater applying a reusable Mg-Fe-Cl layered double hydroxide |
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