Electrochemical Behaviour of Tinidazole at 1,4-Benzoquinone Modified Carbon Paste Electrode and Its Direct Determination in Pharmaceutical Tablets and Urine by Differential Pulse Voltammetry
A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at −0.344 V on a 1,4-BQMCPE....
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| Published in: | Journal of analytical methods in chemistry Vol. 2017; no. 2017; pp. 1 - 10 |
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| Language: | English |
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Cairo, Egypt
Hindawi Publishing Corporation
01-01-2017
Hindawi John Wiley & Sons, Inc Hindawi Limited |
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| Abstract | A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at −0.344 V on a 1,4-BQMCPE. Compared with that on a bare CPE, the reduction peak of TDZ increased significantly on the modified CPE and the effects of different parameters on the voltammetric responses were also investigated. Differential pulse voltammetric method was proposed and optimized for TDZ determination and its reductive peak current response at 1,4-BQMCPE was found to show linear dependence on the concentration of TDZ in the range of 1.0 × 10−6 to 5.0 × 10−4 M with a linear regression equation, correlation coefficient, limit of detection (LOD), and limit of quantification (LOQ) of IPC (μA) = 0.19958 + 0.02657C (μM), 0.99486, 1.10 × 10−7 M, and 3.77 × 10−7, respectively. Excellent recovery results for spiked TDZ in pharmaceutical tablet samples ranging within 97.44–97.51% and in urine ranging within 95.37–96.91% were observed. The selectivity of the method for TDZ was further studied in the presence of selected potential interferents and confirmed the potential applicability of the developed method for the determination of TDZ. |
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| AbstractList | A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at −0.344 V on a 1,4-BQMCPE. Compared with that on a bare CPE, the reduction peak of TDZ increased significantly on the modified CPE and the effects of different parameters on the voltammetric responses were also investigated. Differential pulse voltammetric method was proposed and optimized for TDZ determination and its reductive peak current response at 1,4-BQMCPE was found to show linear dependence on the concentration of TDZ in the range of 1.0 × 10−6 to 5.0 × 10−4 M with a linear regression equation, correlation coefficient, limit of detection (LOD), and limit of quantification (LOQ) of IPC (μA) = 0.19958 + 0.02657C (μM), 0.99486, 1.10 × 10−7 M, and 3.77 × 10−7, respectively. Excellent recovery results for spiked TDZ in pharmaceutical tablet samples ranging within 97.44–97.51% and in urine ranging within 95.37–96.91% were observed. The selectivity of the method for TDZ was further studied in the presence of selected potential interferents and confirmed the potential applicability of the developed method for the determination of TDZ. A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at -0.344 V on a 1,4-BQMCPE. Compared with that on a bare CPE, the reduction peak of TDZ increased significantly on the modified CPE and the effects of different parameters on the voltammetric responses were also investigated. Differential pulse voltammetric method was proposed and optimized for TDZ determination and its reductive peak current response at 1,4-BQMCPE was found to show linear dependence on the concentration of TDZ in the range of 1.0 × 10 to 5.0 × 10 M with a linear regression equation, correlation coefficient, limit of detection (LOD), and limit of quantification (LOQ) of ( A) = 0.19958 + 0.02657 ( M), 0.99486, 1.10 × 10 M, and 3.77 × 10 , respectively. Excellent recovery results for spiked TDZ in pharmaceutical tablet samples ranging within 97.44-97.51% and in urine ranging within 95.37-96.91% were observed. The selectivity of the method for TDZ was further studied in the presence of selected potential interferents and confirmed the potential applicability of the developed method for the determination of TDZ. A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at −0.344 V on a 1,4-BQMCPE. Compared with that on a bare CPE, the reduction peak of TDZ increased significantly on the modified CPE and the effects of different parameters on the voltammetric responses were also investigated. Differential pulse voltammetric method was proposed and optimized for TDZ determination and its reductive peak current response at 1,4-BQMCPE was found to show linear dependence on the concentration of TDZ in the range of 1.0 × 10 −6 to 5.0 × 10 −4 M with a linear regression equation, correlation coefficient, limit of detection (LOD), and limit of quantification (LOQ) of I PC ( μ A) = 0.19958 + 0.02657 C ( μ M), 0.99486, 1.10 × 10 −7 M, and 3.77 × 10 −7 , respectively. Excellent recovery results for spiked TDZ in pharmaceutical tablet samples ranging within 97.44–97.51% and in urine ranging within 95.37–96.91% were observed. The selectivity of the method for TDZ was further studied in the presence of selected potential interferents and confirmed the potential applicability of the developed method for the determination of TDZ. A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at -0.344 V on a 1,4-BQMCPE. Compared with that on a bare CPE, the reduction peak of TDZ increased significantly on the modified CPE and the effects of different parameters on the voltammetric responses were also investigated. Differential pulse voltammetric method was proposed and optimized for TDZ determination and its reductive peak current response at 1,4-BQMCPE was found to show linear dependence on the concentration of TDZ in the range of 1.0 x [10.sup.-6] to 5.0 x [10.sup.-4] M with a linear regression equation, correlation coefficient, limit of detection (LOD), and limit of quantification (LOQ) of [I.sub.PC] ([miccro]A) = 0.19958 + 0.02657C ([micro]M), 0.99486, 1.10 x [10.sup.-7] M, and 3.77 x [10.sup.-7], respectively. Excellent recovery results for spiked TDZ in pharmaceutical tablet samples ranging within 97.44-97.51% and in urine ranging within 95.37-96.91% were observed. The selectivity of the method for TDZ was further studied in the presence of selected potential interferents and confirmed the potential applicability of the developed method for the determination of TDZ. A simple and highly sensitive electrochemical method based on a 1,4-benzoquinone modified carbon paste electrode (1,4-BQMCPE) was described for the determination of tinidazole (TDZ). In Britton Robinson buffer solution, TDZ yields well-defined irreversible reduction peak at −0.344 V on a 1,4-BQMCPE. Compared with that on a bare CPE, the reduction peak of TDZ increased significantly on the modified CPE and the effects of different parameters on the voltammetric responses were also investigated. Differential pulse voltammetric method was proposed and optimized for TDZ determination and its reductive peak current response at 1,4-BQMCPE was found to show linear dependence on the concentration of TDZ in the range of 1.0 × 10 −6 to 5.0 × 10 −4 M with a linear regression equation, correlation coefficient, limit of detection (LOD), and limit of quantification (LOQ) of I P C ( μ A) = 0.19958 + 0.02657 C ( μ M), 0.99486, 1.10 × 10 −7 M, and 3.77 × 10 −7 , respectively. Excellent recovery results for spiked TDZ in pharmaceutical tablet samples ranging within 97.44–97.51% and in urine ranging within 95.37–96.91% were observed. The selectivity of the method for TDZ was further studied in the presence of selected potential interferents and confirmed the potential applicability of the developed method for the determination of TDZ. |
| Audience | Academic |
| Author | Nikodimos, Yosef Hagos, Beyene |
| AuthorAffiliation | Department of Chemistry, Woldia University, P.O. Box 400, Woldia, Ethiopia |
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| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29250454$$D View this record in MEDLINE/PubMed |
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| Cites_doi | 10.4172/2155-9872.1000110 10.1155/2016/3612943 10.1016/S1452-3981(23)19509-5 10.1093/jac/31.1.9 10.1136/adc.51.5.385 10.1016/j.talanta.2008.04.042 10.1128/AAC.19.5.754 10.2116/analsci.20.821 10.4314/bcse.v30i1.1 10.4103/0973-8398.59951 10.4172/2157-7439.1000413 10.4314/tjpr.v13i6.23 10.1016/S0022-0728(79)80075-3 10.1016/j.arabjc.2011.05.019 10.1093/chromsci/bmt028 10.1007/s40090-015-0058-4 10.4172/2153-2435.1000354 |
| ContentType | Journal Article |
| Copyright | Copyright © 2017 Yosef Nikodimos and Beyene Hagos. COPYRIGHT 2017 John Wiley & Sons, Inc. Copyright © 2017 Yosef Nikodimos and Beyene Hagos.; This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. Copyright © 2017 Yosef Nikodimos and Beyene Hagos. 2017 |
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| SubjectTerms | Analysis Bacterial infections Carbon Chemical properties Chromatography Composition Correlation coefficients Drug dosages Electric properties Electrochemical analysis Electrochemical reactions Electrodes Electrodes, Carbon Graphite Infections Laboratories Methods Parameter modification Pharmaceuticals Pharmacy Quinone Quinones R&D Reduction Research & development Selectivity Tablets Tinidazole Urine Voltammetry |
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| Title | Electrochemical Behaviour of Tinidazole at 1,4-Benzoquinone Modified Carbon Paste Electrode and Its Direct Determination in Pharmaceutical Tablets and Urine by Differential Pulse Voltammetry |
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