Heterogeneous Catalytic Hydrogenation of Biobased Levulinic and Succinic Acids in Aqueous Solutions
Supported noble‐metal catalysts (Ru, Pd or Pt) and the corresponding Re‐promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reactio...
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| Published in: | ChemSusChem Vol. 6; no. 12; pp. 2388 - 2395 |
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| Main Authors: | , , , , , , , , , |
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| Language: | English |
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WILEY-VCH Verlag
01-12-2013
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| Abstract | Supported noble‐metal catalysts (Ru, Pd or Pt) and the corresponding Re‐promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reaction conditions. The highest selectivity to 1,4‐pentanediol of 82 % is achieved at 140 °C in the presence of the 1.9 % Ru–3.6 % Re/C catalyst.
Switching between diols and lactones: This article focuses mainly on the comparison of the reactivity of two biobased carboxylic acids, namely levulinic acid and succinic acid, in water in the presence of carbon‐supported noble metals. The optimization of the reaction conditions allows to increase the yield and selectivity to diols (butanediol and pentanediol). Thus, it is possible to obtain pentanediol from levulinic acid under milder conditions compared to succinic acid. |
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| AbstractList | Supported noble-metal catalysts (Ru, Pd or Pt) and the corresponding Re-promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reaction conditions. The highest selectivity to 1,4-pentanediol of 82 % is achieved at 140 °C in the presence of the 1.9 % Ru-3.6 % Re/C catalyst. Supported noble-metal catalysts (Ru, Pd or Pt) and the corresponding Re-promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reaction conditions. The highest selectivity to 1,4-pentanediol of 82% is achieved at 140 degrees C in the presence of the 1.9%Ru-3.6%Re/C catalyst. Supported noble‐metal catalysts (Ru, Pd or Pt) and the corresponding Re‐promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reaction conditions. The highest selectivity to 1,4‐pentanediol of 82 % is achieved at 140 °C in the presence of the 1.9 % Ru–3.6 % Re/C catalyst. Switching between diols and lactones: This article focuses mainly on the comparison of the reactivity of two biobased carboxylic acids, namely levulinic acid and succinic acid, in water in the presence of carbon‐supported noble metals. The optimization of the reaction conditions allows to increase the yield and selectivity to diols (butanediol and pentanediol). Thus, it is possible to obtain pentanediol from levulinic acid under milder conditions compared to succinic acid. Abstract Supported noble‐metal catalysts (Ru, Pd or Pt) and the corresponding Re‐promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reaction conditions. The highest selectivity to 1,4‐pentanediol of 82 % is achieved at 140 °C in the presence of the 1.9 % Ru–3.6 % Re/C catalyst. Supported noble-metal catalysts (Ru, Pd or Pt) and the corresponding Re-promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic acids. Levulinic acid and succinic acid are converted into the lactones or the diols depending on the nature of the catalyst and the reaction conditions. The highest selectivity to 1,4-pentanediol of 82% is achieved at 140°C in the presence of the 1.9%Ru-3.6%Re/C catalyst. [PUBLICATION ABSTRACT] |
| Author | Minh, Doan-Pham Especel, Catherine Besson, Michèle Corbel-Demailly, Louis Tapin, Benoit Cabiac, Amandine Pinel, Catherine Guillon, Emmanuelle Epron, Florence Ly, Bao-Khanh |
| Author_xml | – sequence: 1 givenname: Louis surname: Corbel-Demailly fullname: Corbel-Demailly, Louis organization: IRCELYON, Institut de recherches sur la catalyse et l'environnement de Lyon, UMR 5256 CNRS-Université Lyon1, 2 Avenue Albert Einstein, 69626 Villeurbanne (France) – sequence: 2 givenname: Bao-Khanh surname: Ly fullname: Ly, Bao-Khanh organization: IRCELYON, Institut de recherches sur la catalyse et l'environnement de Lyon, UMR 5256 CNRS-Université Lyon1, 2 Avenue Albert Einstein, 69626 Villeurbanne (France) – sequence: 3 givenname: Doan-Pham surname: Minh fullname: Minh, Doan-Pham organization: IRCELYON, Institut de recherches sur la catalyse et l'environnement de Lyon, UMR 5256 CNRS-Université Lyon1, 2 Avenue Albert Einstein, 69626 Villeurbanne (France) – sequence: 4 givenname: Benoit surname: Tapin fullname: Tapin, Benoit organization: IC2MP, Institut de Chimie des Milieux et Matériaux de Poitiers, UMR 7285 CNRS-Université de Poitiers, 4 rue Michel Brunet, 86022 Poitiers (France) – sequence: 5 givenname: Catherine surname: Especel fullname: Especel, Catherine organization: IC2MP, Institut de Chimie des Milieux et Matériaux de Poitiers, UMR 7285 CNRS-Université de Poitiers, 4 rue Michel Brunet, 86022 Poitiers (France) – sequence: 6 givenname: Florence surname: Epron fullname: Epron, Florence organization: IC2MP, Institut de Chimie des Milieux et Matériaux de Poitiers, UMR 7285 CNRS-Université de Poitiers, 4 rue Michel Brunet, 86022 Poitiers (France) – sequence: 7 givenname: Amandine surname: Cabiac fullname: Cabiac, Amandine organization: IFPEN-Lyon, BP3, 69360 Solaize (France) – sequence: 8 givenname: Emmanuelle surname: Guillon fullname: Guillon, Emmanuelle organization: IFPEN-Lyon, BP3, 69360 Solaize (France) – sequence: 9 givenname: Michèle surname: Besson fullname: Besson, Michèle organization: IRCELYON, Institut de recherches sur la catalyse et l'environnement de Lyon, UMR 5256 CNRS-Université Lyon1, 2 Avenue Albert Einstein, 69626 Villeurbanne (France) – sequence: 10 givenname: Catherine surname: Pinel fullname: Pinel, Catherine email: catherine.pinel@ircelyon.univ-lyon1.fr organization: IRCELYON, Institut de recherches sur la catalyse et l'environnement de Lyon, UMR 5256 CNRS-Université Lyon1, 2 Avenue Albert Einstein, 69626 Villeurbanne (France) |
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| Keywords | biomass diols heterogeneous catalysis hydrogenation carboxylic acids |
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| Snippet | Supported noble‐metal catalysts (Ru, Pd or Pt) and the corresponding Re‐promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic... Supported noble-metal catalysts (Ru, Pd or Pt) and the corresponding Re-promoted catalysts exhibit a high activity for the hydrogenation of biobased carboxylic... Abstract Supported noble‐metal catalysts (Ru, Pd or Pt) and the corresponding Re‐promoted catalysts exhibit a high activity for the hydrogenation of biobased... |
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| SubjectTerms | biomass Carbon - chemistry carboxylic acids Catalysis Chemical Sciences diols Environment and Society Environmental Sciences heterogeneous catalysis Hydrogenation Levulinic Acids - chemistry Metals, Heavy - chemistry Solutions Succinates - chemistry |
| Title | Heterogeneous Catalytic Hydrogenation of Biobased Levulinic and Succinic Acids in Aqueous Solutions |
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