Generation of high-purity hydrogen from cellulose by its mechanochemical treatment
Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods of X-ray diffraction (XRD), thermogravimetry/mass spectrometry (TG/MS) and gas chromatography (GC) were used to characterize the samples. Hydr...
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| Published in: | Bioresource technology Vol. 100; no. 15; pp. 3731 - 3733 |
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| Format: | Journal Article Conference Proceeding |
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| Abstract | Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods of X-ray diffraction (XRD), thermogravimetry/mass spectrometry (TG/MS) and gas chromatography (GC) were used to characterize the samples. Hydrogen was emitted when heating the milled sample around 400
°C together with low concentrations of methane, carbon monoxide and carbon dioxide. It is understood that an interaction occurs between cellulose and lithium hydroxide to convert the carbon of cellulose into lithium carbonate and to emit hydrogen correspondingly. It is also found that nickel catalyst is required to facilitate the interaction and the behaviours of three different nickel compounds were compared. When high yield of hydrogen emission is available, the prepared samples can also serve the purpose of hydrogen storage. |
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| AbstractList | Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods of X-ray diffraction (XRD), thermogravimetry/mass spectrometry (TG/MS) and gas chromatography (GC) were used to characterize the samples. Hydrogen was emitted when heating the milled sample around 400
°C together with low concentrations of methane, carbon monoxide and carbon dioxide. It is understood that an interaction occurs between cellulose and lithium hydroxide to convert the carbon of cellulose into lithium carbonate and to emit hydrogen correspondingly. It is also found that nickel catalyst is required to facilitate the interaction and the behaviours of three different nickel compounds were compared. When high yield of hydrogen emission is available, the prepared samples can also serve the purpose of hydrogen storage. Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods of X-ray diffraction (XRD), thermogravimetry/mass spectrometry (TG/MS) and gas chromatography (GC) were used to characterize the samples. Hydrogen was emitted when heating the milled sample around 400 °C together with low concentrations of methane, carbon monoxide and carbon dioxide. It is understood that an interaction occurs between cellulose and lithium hydroxide to convert the carbon of cellulose into lithium carbonate and to emit hydrogen correspondingly. It is also found that nickel catalyst is required to facilitate the interaction and the behaviours of three different nickel compounds were compared. When high yield of hydrogen emission is available, the prepared samples can also serve the purpose of hydrogen storage. Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods of X-ray diffraction (XRD), thermogravimetry/mass spectrometry (TG/MS) and gas chromatography (GC) were used to characterize the samples. Hydrogen was emitted when heating the milled sample around 400 degrees C together with low concentrations of methane, carbon monoxide and carbon dioxide. It is understood that an interaction occurs between cellulose and lithium hydroxide to convert the carbon of cellulose into lithium carbonate and to emit hydrogen correspondingly. It is also found that nickel catalyst is required to facilitate the interaction and the behaviours of three different nickel compounds were compared. When high yield of hydrogen emission is available, the prepared samples can also serve the purpose of hydrogen storage. Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods of X-ray diffraction (XRD), thermogravimetry/mass spectrometry (TG/MS) and gas chromatography (GC) were used to characterize the samples. Hydrogen was emitted when heating the milled sample around 400°C together with low concentrations of methane, carbon monoxide and carbon dioxide. It is understood that an interaction occurs between cellulose and lithium hydroxide to convert the carbon of cellulose into lithium carbonate and to emit hydrogen correspondingly. It is also found that nickel catalyst is required to facilitate the interaction and the behaviours of three different nickel compounds were compared. When high yield of hydrogen emission is available, the prepared samples can also serve the purpose of hydrogen storage. |
| Author | Kang, Incheol Saito, Fumio Tongamp, William Zhang, Qiwu |
| Author_xml | – sequence: 1 givenname: Qiwu surname: Zhang fullname: Zhang, Qiwu email: zhangqw@tagen.tohoku.ac.jp – sequence: 2 givenname: Incheol surname: Kang fullname: Kang, Incheol – sequence: 3 givenname: William surname: Tongamp fullname: Tongamp, William – sequence: 4 givenname: Fumio surname: Saito fullname: Saito, Fumio |
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| CitedBy_id | crossref_primary_10_1007_s12649_009_9004_z crossref_primary_10_1016_j_ijhydene_2014_08_129 crossref_primary_10_1016_j_biombioe_2010_11_039 crossref_primary_10_1016_j_crcon_2023_04_001 crossref_primary_10_4144_rpsj_60_36 crossref_primary_10_1080_05704928_2011_565533 crossref_primary_10_1021_acssuschemeng_0c04139 crossref_primary_10_1016_j_fuproc_2009_10_008 crossref_primary_10_1016_j_biortech_2015_11_055 crossref_primary_10_1021_ef300653b crossref_primary_10_4164_sptj_49_683 |
| Cites_doi | 10.1039/b801021h 10.1002/adma.200306557 10.1021/ie050432o 10.1021/ef040017t 10.1016/j.biortech.2005.06.002 10.1039/B406522K 10.1021/ef050282u 10.1038/nature01009 10.1016/j.scriptamat.2007.01.010 10.1038/nature01210 10.1016/0960-8524(92)90025-S |
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| Keywords | Mechanochemical Hydroxide Hydrogen Cellulose Purity Hydroxides |
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| Snippet | Cellulose was mixed with the hydroxides of lithium and nickel and the mixture was milled, followed by heating to produce hydrogen. Several analytical methods... |
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| SubjectTerms | biofuels biogas Biological and medical sciences biomass catalysts Cellulose Cellulose - chemistry chemical treatment Chromatography, Gas Fundamental and applied biological sciences. Psychology gasification heat treatment Hydrogen Hydrogen - metabolism Hydroxide hydroxides lithium Mass Spectrometry Mechanochemical nickel renewable energy sources X-Ray Diffraction |
| Title | Generation of high-purity hydrogen from cellulose by its mechanochemical treatment |
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