Three-Dimensional Smart Catalyst Electrode for Oxygen Evolution Reaction
A multifunctional catalyst electrode mimicking external stimuli–responsive property has been prepared by the in situ growth of nitrogen (N)‐doped NiFe double layered hydroxide (N–NiFe LDH) nanolayers on a 3D nickel foam substrate framework. The electrode demonstrates superior performance toward cata...
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| Published in: | Advanced energy materials Vol. 5; no. 18; pp. np - n/a |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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Weinheim
Blackwell Publishing Ltd
01-09-2015
Wiley Subscription Services, Inc |
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| Abstract | A multifunctional catalyst electrode mimicking external stimuli–responsive property has been prepared by the in situ growth of nitrogen (N)‐doped NiFe double layered hydroxide (N–NiFe LDH) nanolayers on a 3D nickel foam substrate framework. The electrode demonstrates superior performance toward catalyzing oxygen evolution reaction (OER), affording a low overpotential of 0.23 V at the current density of 10 mA cm−2, high Faradaic efficiency of ≈98%, and stable operation for >60 h. Meanwhile, the electrode can dynamically change its color from gray silver to dark black with the OER happening, and the coloration/bleaching processes persist for at least 5000 cycles, rendering it a useful tool to monitor the catalytic process. Mechanism study reveals that the excellent structural properties of electrode such as 3D conductive framework, ultra thickness of N–NiFe LDH nanolayer (≈0.8 nm), and high N‐doping content (≈17.8%) make significant contribution to achieving enhanced catalytic performance, while N–NiFe LDH nanolayer on electrode is the main contributor to the stimuli‐responsive property with the reversible extraction/insertion of electrons from/into N–NiFe LDH leading to the coloration/bleaching processes. Potential application of this electrode has been further demonstrated by integrating it into a Zn–air battery device to identify the charging process during electrochemical cycling.
A 3D catalyst electrode mimicking external stimuli–responsive functionality is fabricated. It exhibits superior performance toward catalyzing oxygen evolution reaction (OER) and dynamically changes its color with the OER, providing an opportunity to quickly monitor the catalytic reaction. |
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| AbstractList | A multifunctional catalyst electrode mimicking external stimuli–responsive property has been prepared by the in situ growth of nitrogen (N)‐doped NiFe double layered hydroxide (N–NiFe LDH) nanolayers on a 3D nickel foam substrate framework. The electrode demonstrates superior performance toward catalyzing oxygen evolution reaction (OER), affording a low overpotential of 0.23 V at the current density of 10 mA cm−2, high Faradaic efficiency of ≈98%, and stable operation for >60 h. Meanwhile, the electrode can dynamically change its color from gray silver to dark black with the OER happening, and the coloration/bleaching processes persist for at least 5000 cycles, rendering it a useful tool to monitor the catalytic process. Mechanism study reveals that the excellent structural properties of electrode such as 3D conductive framework, ultra thickness of N–NiFe LDH nanolayer (≈0.8 nm), and high N‐doping content (≈17.8%) make significant contribution to achieving enhanced catalytic performance, while N–NiFe LDH nanolayer on electrode is the main contributor to the stimuli‐responsive property with the reversible extraction/insertion of electrons from/into N–NiFe LDH leading to the coloration/bleaching processes. Potential application of this electrode has been further demonstrated by integrating it into a Zn–air battery device to identify the charging process during electrochemical cycling.
A 3D catalyst electrode mimicking external stimuli–responsive functionality is fabricated. It exhibits superior performance toward catalyzing oxygen evolution reaction (OER) and dynamically changes its color with the OER, providing an opportunity to quickly monitor the catalytic reaction. A multifunctional catalyst electrode mimicking external stimuli-responsive property has been prepared by the in situ growth of nitrogen (N)-doped NiFe double layered hydroxide (N-NiFe LDH) nanolayers on a 3D nickel foam substrate framework. The electrode demonstrates superior performance toward catalyzing oxygen evolution reaction (OER), affording a low overpotential of 0.23 V at the current density of 10 mA cm super(-2), high Faradaic efficiency of approximately 98%, and stable operation for >60 h. Meanwhile, the electrode can dynamically change its color from gray silver to dark black with the OER happening, and the coloration/bleaching processes persist for at least 5000 cycles, rendering it a useful tool to monitor the catalytic process. Mechanism study reveals that the excellent structural properties of electrode such as 3D conductive framework, ultra thickness of N-NiFe LDH nanolayer ( approximately 0.8 nm), and high N-doping content ( approximately 17.8%) make significant contribution to achieving enhanced catalytic performance, while N-NiFe LDH nanolayer on electrode is the main contributor to the stimuli-responsive property with the reversible extraction/insertion of electrons from/into N-NiFe LDH leading to the coloration/bleaching processes. Potential application of this electrode has been further demonstrated by integrating it into a Zn-air battery device to identify the charging process during electrochemical cycling. A 3D catalyst electrode mimicking external stimuli-responsive functionality is fabricated. It exhibits superior performance toward catalyzing oxygen evolution reaction (OER) and dynamically changes its color with the OER, providing an opportunity to quickly monitor the catalytic reaction. A multifunctional catalyst electrode mimicking external stimuli-responsive property has been prepared by the in situ growth of nitrogen (N)-doped NiFe double layered hydroxide (N-NiFe LDH) nanolayers on a 3D nickel foam substrate framework. The electrode demonstrates superior performance toward catalyzing oxygen evolution reaction (OER), affording a low overpotential of 0.23 V at the current density of 10 mA cm-2, high Faradaic efficiency of [asymptotically =]98%, and stable operation for >60 h. Meanwhile, the electrode can dynamically change its color from gray silver to dark black with the OER happening, and the coloration/bleaching processes persist for at least 5000 cycles, rendering it a useful tool to monitor the catalytic process. Mechanism study reveals that the excellent structural properties of electrode such as 3D conductive framework, ultra thickness of N-NiFe LDH nanolayer ([asymptotically =]0.8 nm), and high N-doping content ([asymptotically =]17.8%) make significant contribution to achieving enhanced catalytic performance, while N-NiFe LDH nanolayer on electrode is the main contributor to the stimuli-responsive property with the reversible extraction/insertion of electrons from/into N-NiFe LDH leading to the coloration/bleaching processes. Potential application of this electrode has been further demonstrated by integrating it into a Zn-air battery device to identify the charging process during electrochemical cycling. A multifunctional catalyst electrode mimicking external stimuli–responsive property has been prepared by the in situ growth of nitrogen (N)‐doped NiFe double layered hydroxide (N–NiFe LDH) nanolayers on a 3D nickel foam substrate framework. The electrode demonstrates superior performance toward catalyzing oxygen evolution reaction (OER), affording a low overpotential of 0.23 V at the current density of 10 mA cm −2 , high Faradaic efficiency of ≈98%, and stable operation for >60 h. Meanwhile, the electrode can dynamically change its color from gray silver to dark black with the OER happening, and the coloration/bleaching processes persist for at least 5000 cycles, rendering it a useful tool to monitor the catalytic process. Mechanism study reveals that the excellent structural properties of electrode such as 3D conductive framework, ultra thickness of N–NiFe LDH nanolayer (≈0.8 nm), and high N‐doping content (≈17.8%) make significant contribution to achieving enhanced catalytic performance, while N–NiFe LDH nanolayer on electrode is the main contributor to the stimuli‐responsive property with the reversible extraction/insertion of electrons from/into N–NiFe LDH leading to the coloration/bleaching processes. Potential application of this electrode has been further demonstrated by integrating it into a Zn–air battery device to identify the charging process during electrochemical cycling. |
| Author | Zheng, Rongkun Tang, Youhong Qiao, Shi-Zhang Chen, Sheng Duan, Jingjing Bian, Pengju |
| Author_xml | – sequence: 1 givenname: Sheng surname: Chen fullname: Chen, Sheng organization: School of Chemical Engineering, The University of Adelaide, SA, 5005, Adelaide, Australia – sequence: 2 givenname: Jingjing surname: Duan fullname: Duan, Jingjing organization: School of Chemical Engineering, The University of Adelaide, SA, 5005, Adelaide, Australia – sequence: 3 givenname: Pengju surname: Bian fullname: Bian, Pengju organization: School of Physics, The University of Sydney, 2006, New South Wales, Australia – sequence: 4 givenname: Youhong surname: Tang fullname: Tang, Youhong organization: Centre for Nanoscale Science and Technology and Centre for Maritime Engineering, Control and Imaging, Flinders University, 5042, Adelaide, Australia – sequence: 5 givenname: Rongkun surname: Zheng fullname: Zheng, Rongkun organization: School of Physics, The University of Sydney, 2006, New South Wales, Australia – sequence: 6 givenname: Shi-Zhang surname: Qiao fullname: Qiao, Shi-Zhang email: s.qiao@adelaide.edu.au organization: School of Chemical Engineering, The University of Adelaide, SA, 5005, Adelaide, Australia |
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| Copyright | 2015 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim |
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| Snippet | A multifunctional catalyst electrode mimicking external stimuli–responsive property has been prepared by the in situ growth of nitrogen (N)‐doped NiFe double... A multifunctional catalyst electrode mimicking external stimuli-responsive property has been prepared by the in situ growth of nitrogen (N)-doped NiFe double... |
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| SubjectTerms | Bleaching Catalysis catalyst electrodes Catalysts Electrodes Evolution heteroatom doping Monitors Nanostructure Oxygen oxygen evolution reaction smart material Three dimensional Two-dimensional nanolayers |
| Title | Three-Dimensional Smart Catalyst Electrode for Oxygen Evolution Reaction |
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