Facile one step-synthesis and characterisation of high aspect ratio core-shell copper-polyaniline nanowires

Metal nanowire/polyaniline core‐shell nanoparticles have significant potential for the development of materials for electrostatical dissipation, electromagnetic interference shields, chemical and biological sensors, charge and hydrogen storage. In this study, the synthesis of novel core‐shell nanost...

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Published in:	Canadian journal of chemical engineering Vol. 92; no. 7; pp. 1207 - 1212
Main Authors:	Sarvi, Ali, Gelves, Genaro A., Sundararaj, Uttandaraman
Format:	Journal Article
Language:	English
Published:	Blackwell Publishing Ltd 01-07-2014
Subjects:	ANILINE ASPECT RATIO conductivity Copper ELECTRICAL CONDUCTIVITY High aspect ratio metal nanowires MICROSTRUCTURES MICROWIRE nano-coating Nanostructure Nanowires PARTICLES polyaniline Polyanilines POLYMERS Surface chemistry Transmission electron microscopy X RAY SPECTROSCOPY X-ray photoelectron spectroscopy
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Abstract	Metal nanowire/polyaniline core‐shell nanoparticles have significant potential for the development of materials for electrostatical dissipation, electromagnetic interference shields, chemical and biological sensors, charge and hydrogen storage. In this study, the synthesis of novel core‐shell nanostructures of polyaniline‐coated copper nanowires (PANI/CuNWs) is presented. CuNWs of 25 nm in diameter and several microns in length were synthesised using hard template method and were subsequently coated with doped or undoped polyanilines to obtain high aspect ratio core‐shell nanoparticles. SEM, TEM, XPS and electrical conductivity measurements were used to characterise these novel nanomaterials. TEM characterisation showed a smooth polyaniline nanocoating of about 6 nm in thickness over the CuNW surface. The thickness of the coating can be controlled by changing PANI concentration in the solution. XPS results indicate that spontaneous adsorption of polyaniline results from the strong surficial interaction between copper atoms at the nanowire surface and imine groups in the polyaniline backbone.
AbstractList	Metal nanowire/polyaniline core-shell nanoparticles have significant potential for the development of materials for electrostatical dissipation, electromagnetic interference shields, chemical and biological sensors, charge and hydrogen storage. In this study, the synthesis of novel core-shell nanostructures of polyaniline-coated copper nanowires (PANI/CuNWs) is presented. CuNWs of 25nm in diameter and several microns in length were synthesised using hard template method and were subsequently coated with doped or undoped polyanilines to obtain high aspect ratio core-shell nanoparticles. SEM, TEM, XPS and electrical conductivity measurements were used to characterise these novel nanomaterials. TEM characterisation showed a smooth polyaniline nanocoating of about 6nm in thickness over the CuNW surface. The thickness of the coating can be controlled by changing PANI concentration in the solution. XPS results indicate that spontaneous adsorption of polyaniline results from the strong surficial interaction between copper atoms at the nanowire surface and imine groups in the polyaniline backbone. Metal nanowire/polyaniline core‐shell nanoparticles have significant potential for the development of materials for electrostatical dissipation, electromagnetic interference shields, chemical and biological sensors, charge and hydrogen storage. In this study, the synthesis of novel core‐shell nanostructures of polyaniline‐coated copper nanowires (PANI/CuNWs) is presented. CuNWs of 25 nm in diameter and several microns in length were synthesised using hard template method and were subsequently coated with doped or undoped polyanilines to obtain high aspect ratio core‐shell nanoparticles. SEM, TEM, XPS and electrical conductivity measurements were used to characterise these novel nanomaterials. TEM characterisation showed a smooth polyaniline nanocoating of about 6 nm in thickness over the CuNW surface. The thickness of the coating can be controlled by changing PANI concentration in the solution. XPS results indicate that spontaneous adsorption of polyaniline results from the strong surficial interaction between copper atoms at the nanowire surface and imine groups in the polyaniline backbone.
Author	Sarvi, Ali Sundararaj, Uttandaraman Gelves, Genaro A.
Author_xml	– sequence: 1 givenname: Ali surname: Sarvi fullname: Sarvi, Ali organization: Department of Chemical and Petroleum Engineering, University of Calgary, 2500 University Dr., T2N 1N4, CalgaryAlberta, Canada – sequence: 2 givenname: Genaro A. surname: Gelves fullname: Gelves, Genaro A. organization: Department of Chemical and Petroleum Engineering, University of Calgary, 2500 University Dr., T2N 1N4, CalgaryAlberta, Canada – sequence: 3 givenname: Uttandaraman surname: Sundararaj fullname: Sundararaj, Uttandaraman email: u.sundararaj@ucalgary.ca organization: Department of Chemical and Petroleum Engineering, University of Calgary, 2500 University Dr., T2N 1N4, CalgaryAlberta, Canada
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Cites_doi	10.1016/S0032-3861(00)00340-2 10.1039/C0JM02546A 10.1080/01932690701688490 10.1002/sia.740201006 10.1002/sia.740190110 10.1016/j.carbon.2011.04.039 10.1039/b603442j 10.1016/j.polymer.2006.03.060 10.1021/jp808582f 10.1016/j.progpolymsci.2003.08.001 10.1016/S0379-6779(98)01095-9 10.1002/marc.200500490 10.1016/j.electacta.2010.02.022 10.1016/0379-6779(93)91097-L 10.1016/j.apsusc.2004.02.022 10.1007/s10800-006-9284-y 10.1021/ma00035a035 10.1016/S0379-6779(98)01093-5 10.1088/0957-4484/19/21/215712 10.1021/ie061285c 10.1021/la980205 10.1016/S0379-6779(00)01393-X 10.1016/0379-6779(94)02418-X 10.1051/jcp:1998315 10.1016/S0032-3861(96)00698-2 10.1039/CT9120101117 10.1002/adfm.200600336
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Snippet	Metal nanowire/polyaniline core‐shell nanoparticles have significant potential for the development of materials for electrostatical dissipation,... Metal nanowire/polyaniline core-shell nanoparticles have significant potential for the development of materials for electrostatical dissipation,...
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SubjectTerms	ANILINE ASPECT RATIO conductivity Copper ELECTRICAL CONDUCTIVITY High aspect ratio metal nanowires MICROSTRUCTURES MICROWIRE nano-coating Nanostructure Nanowires PARTICLES polyaniline Polyanilines POLYMERS Surface chemistry Transmission electron microscopy X RAY SPECTROSCOPY X-ray photoelectron spectroscopy
Title	Facile one step-synthesis and characterisation of high aspect ratio core-shell copper-polyaniline nanowires
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