Reinforcement of Castor Oil-Based Polyurethane with Surface Modification of Attapulgite
Polyurethane/attapulgite (PU/ATT) nanocomposites derived from castor oil were prepared by incorporation of 8 wt % ATT, acid-treated ATT, and KH560-treated ATT. The effects of three ATTs (ATT, acid-ATT, and KH560-ATT) on the comprehensive properties of PU/ATT nanocomposites were systematically invest...
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| Published in: | Polymers Vol. 10; no. 11; p. 1236 |
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| Main Authors: | , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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| Abstract | Polyurethane/attapulgite (PU/ATT) nanocomposites derived from castor oil were prepared by incorporation of 8 wt % ATT, acid-treated ATT, and KH560-treated ATT. The effects of three ATTs (ATT, acid-ATT, and KH560-ATT) on the comprehensive properties of PU/ATT nanocomposites were systematically investigated. The results showed that the incorporation of 8 wt % of three ATTs could produce an obvious reinforcement on the castor oil-based PU and that the silane modification treatment, rather than the acid treatment, has the more effective reinforcement effect. SEM images revealed the uniform dispersion of ATT in the PU matrix. DMA confirmed that the storage modulus and glass transition temperature (
) of PU/ATT nanocomposites were significantly increased after blending with different ATTs. For PU/KH560-ATT8 nanocomposites, the thermal stability of the PU was obviously enhanced by the addition of KH560-ATT. In particular, 8 wt % KH560-ATT loaded castor oil-based PU nanocomposites exhibit an obvious improvement in tensile strength (255%), Young's modulus (200%),
(5.1 °C), the storage modulus at 25 °C (104%), and the initial decomposition temperature (7.7 °C). The prepared bio-based PU materials could be a potential candidate to replace petroleum-based PU products in practical applications. |
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| AbstractList | Polyurethane/attapulgite (PU/ATT) nanocomposites derived from castor oil were prepared by incorporation of 8 wt % ATT, acid-treated ATT, and KH560-treated ATT. The effects of three ATTs (ATT, acid-ATT, and KH560-ATT) on the comprehensive properties of PU/ATT nanocomposites were systematically investigated. The results showed that the incorporation of 8 wt % of three ATTs could produce an obvious reinforcement on the castor oil-based PU and that the silane modification treatment, rather than the acid treatment, has the more effective reinforcement effect. SEM images revealed the uniform dispersion of ATT in the PU matrix. DMA confirmed that the storage modulus and glass transition temperature (Tg) of PU/ATT nanocomposites were significantly increased after blending with different ATTs. For PU/KH560-ATT8 nanocomposites, the thermal stability of the PU was obviously enhanced by the addition of KH560-ATT. In particular, 8 wt % KH560-ATT loaded castor oil-based PU nanocomposites exhibit an obvious improvement in tensile strength (255%), Young’s modulus (200%), Tg (5.1 °C), the storage modulus at 25 °C (104%), and the initial decomposition temperature (7.7 °C). The prepared bio-based PU materials could be a potential candidate to replace petroleum-based PU products in practical applications. Polyurethane/attapulgite (PU/ATT) nanocomposites derived from castor oil were prepared by incorporation of 8 wt % ATT, acid-treated ATT, and KH560-treated ATT. The effects of three ATTs (ATT, acid-ATT, and KH560-ATT) on the comprehensive properties of PU/ATT nanocomposites were systematically investigated. The results showed that the incorporation of 8 wt % of three ATTs could produce an obvious reinforcement on the castor oil-based PU and that the silane modification treatment, rather than the acid treatment, has the more effective reinforcement effect. SEM images revealed the uniform dispersion of ATT in the PU matrix. DMA confirmed that the storage modulus and glass transition temperature ( ) of PU/ATT nanocomposites were significantly increased after blending with different ATTs. For PU/KH560-ATT8 nanocomposites, the thermal stability of the PU was obviously enhanced by the addition of KH560-ATT. In particular, 8 wt % KH560-ATT loaded castor oil-based PU nanocomposites exhibit an obvious improvement in tensile strength (255%), Young's modulus (200%), (5.1 °C), the storage modulus at 25 °C (104%), and the initial decomposition temperature (7.7 °C). The prepared bio-based PU materials could be a potential candidate to replace petroleum-based PU products in practical applications. Polyurethane/attapulgite (PU/ATT) nanocomposites derived from castor oil were prepared by incorporation of 8 wt % ATT, acid-treated ATT, and KH560-treated ATT. The effects of three ATTs (ATT, acid-ATT, and KH560-ATT) on the comprehensive properties of PU/ATT nanocomposites were systematically investigated. The results showed that the incorporation of 8 wt % of three ATTs could produce an obvious reinforcement on the castor oil-based PU and that the silane modification treatment, rather than the acid treatment, has the more effective reinforcement effect. SEM images revealed the uniform dispersion of ATT in the PU matrix. DMA confirmed that the storage modulus and glass transition temperature ( T g ) of PU/ATT nanocomposites were significantly increased after blending with different ATTs. For PU/KH560-ATT8 nanocomposites, the thermal stability of the PU was obviously enhanced by the addition of KH560-ATT. In particular, 8 wt % KH560-ATT loaded castor oil-based PU nanocomposites exhibit an obvious improvement in tensile strength (255%), Young’s modulus (200%), T g (5.1 °C), the storage modulus at 25 °C (104%), and the initial decomposition temperature (7.7 °C). The prepared bio-based PU materials could be a potential candidate to replace petroleum-based PU products in practical applications. |
| Author | Dai, Lili Wang, Chengshuang He, Meng Ge, Chengcheng Ding, Liang Xie, Hongfeng Li, Shuiping Yang, Zhengrui |
| AuthorAffiliation | 2 You Pei College, Yancheng Institute of Technology, Yancheng 224051, China 4 Key Laboratory of High Performance Polymer Materials and Technology (Nanjing University), Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China 3 Department of Chemical and Environmental Engineering, University of California-Riverside, Riverside, CA 92521, USA 1 School of Materials Science and Engineering, Yancheng 224051, China; dll081218@163.com (L.D.); 15190638055@163.com (Z.Y.); gcc13626213109@163.com (C.G.); lishuiping2002@126.com (S.L.); hemeng315@163.com (M.H.); dl1984911@ycit.edu.cn (L.D.) |
| AuthorAffiliation_xml | – name: 4 Key Laboratory of High Performance Polymer Materials and Technology (Nanjing University), Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China – name: 2 You Pei College, Yancheng Institute of Technology, Yancheng 224051, China – name: 1 School of Materials Science and Engineering, Yancheng 224051, China; dll081218@163.com (L.D.); 15190638055@163.com (Z.Y.); gcc13626213109@163.com (C.G.); lishuiping2002@126.com (S.L.); hemeng315@163.com (M.H.); dl1984911@ycit.edu.cn (L.D.) – name: 3 Department of Chemical and Environmental Engineering, University of California-Riverside, Riverside, CA 92521, USA |
| Author_xml | – sequence: 1 givenname: Chengshuang surname: Wang fullname: Wang, Chengshuang email: wangcs@ycit.cn, wangcs@ycit.cn, wangcs@ycit.cn organization: Department of Chemical and Environmental Engineering, University of California-Riverside, Riverside, CA 92521, USA. wangcs@ycit.cn – sequence: 2 givenname: Lili surname: Dai fullname: Dai, Lili email: dll081218@163.com, dll081218@163.com organization: You Pei College, Yancheng Institute of Technology, Yancheng 224051, China. dll081218@163.com – sequence: 3 givenname: Zhengrui surname: Yang fullname: Yang, Zhengrui email: 15190638055@163.com, 15190638055@163.com organization: You Pei College, Yancheng Institute of Technology, Yancheng 224051, China. 15190638055@163.com – sequence: 4 givenname: Chengcheng surname: Ge fullname: Ge, Chengcheng email: gcc13626213109@163.com, gcc13626213109@163.com organization: You Pei College, Yancheng Institute of Technology, Yancheng 224051, China. gcc13626213109@163.com – sequence: 5 givenname: Shuiping surname: Li fullname: Li, Shuiping email: lishuiping2002@126.com organization: School of Materials Science and Engineering, Yancheng 224051, China. lishuiping2002@126.com – sequence: 6 givenname: Meng orcidid: 0000-0001-6209-563X surname: He fullname: He, Meng email: hemeng315@163.com organization: School of Materials Science and Engineering, Yancheng 224051, China. hemeng315@163.com – sequence: 7 givenname: Liang surname: Ding fullname: Ding, Liang email: dl1984911@ycit.edu.cn organization: School of Materials Science and Engineering, Yancheng 224051, China. dl1984911@ycit.edu.cn – sequence: 8 givenname: Hongfeng orcidid: 0000-0002-3612-0464 surname: Xie fullname: Xie, Hongfeng email: cwang@ucr.edu organization: Key Laboratory of High Performance Polymer Materials and Technology (Nanjing University), Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China. cwang@ucr.edu |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30961161$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1016_j_porgcoat_2024_108576 crossref_primary_10_1016_j_porgcoat_2022_107120 crossref_primary_10_1016_j_porgcoat_2022_107377 crossref_primary_10_1021_acs_biomac_0c01291 crossref_primary_10_1007_s10973_019_08033_x crossref_primary_10_3390_molecules27207061 crossref_primary_10_1016_j_conbuildmat_2023_133670 crossref_primary_10_1080_15583724_2023_2286706 crossref_primary_10_3390_nano12040609 crossref_primary_10_1007_s10924_023_02786_1 crossref_primary_10_1007_s10965_022_03393_9 crossref_primary_10_1002_vnl_22046 crossref_primary_10_1016_j_cej_2024_151509 |
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| Copyright | 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. 2018 by the authors. 2018 |
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| SubjectTerms | attapulgite Castor oil Cellulose Clay Glass transition temperature Hydrochloric acid Modulus of elasticity Nanocomposites Nanoparticles polyurethane Polyurethane resins Reinforcement Storage modulus Tensile strength Thermal stability Vegetable oils |
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| Title | Reinforcement of Castor Oil-Based Polyurethane with Surface Modification of Attapulgite |
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