Processing and characterization of amorphous magnesium based alloy for application in biomedical implants

Magnesium-based bulk metallic glasses are attractive due to their single-phase, chemically homogeneous alloy system and the absence of second-phase, which could impair the mechanical properties and corrosion resistance. However, one of the unsolved problems for the manufacturability and the applicat...

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Published in:	Journal of materials research and technology Vol. 3; no. 3; pp. 203 - 209
Main Authors:	Matias, Telma Blanco, Asato, Gabriel Hitoshi, Ramasco, Bruno Torquato, Botta, Walter José, Kiminami, Claudio Shyinti, Bolfarini, Claudemiro
Format:	Journal Article
Language:	English
Published:	Elsevier Editora Ltda 01-07-2014 Elsevier
Subjects:	Amorphous Bioabsorbable implants Biomaterials Magnesium-based alloys Amorphous Bioabsorbable implants Magnesium-based alloys Biomaterials
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Abstract	Magnesium-based bulk metallic glasses are attractive due to their single-phase, chemically homogeneous alloy system and the absence of second-phase, which could impair the mechanical properties and corrosion resistance. However, one of the unsolved problems for the manufacturability and the applications of bulk metallic glasses is that their glass-forming ability is very sensitive to the preparation techniques and impurity of components since oxygen in the environment would markedly deteriorate the glass-forming ability. Therefore, the aim of this study was to establish proper processing conditions to obtain a magnesium-based amorphous ternary alloy and its characterization. The final composition was prepared using two binary master alloys by melting in an induction furnace. Carbon steel crucible was used in argon atmosphere with and without addition of SF6 gas in order to minimize the oxygen contamination. The microstructure, amorphous nature, thermal properties and chemical analysis of samples were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and inductively coupled plasma emission spectrometry, respectively. The oxygen content of the as-cast samples was chemically analyzed by using carrier gas hot extraction (O/N Analyzer TC-436/LECO) and was kept bellow 25ppm (without SF6) and 10ppm (with SF6). Bulk samples were produced by rapid cooling in a cooper mold until 1.5mm thickness, with amorphous structures being observed up to 2.5mm.
AbstractList	Magnesium-based bulk metallic glasses are attractive due to their single-phase, chemically homogeneous alloy system and the absence of second-phase, which could impair the mechanical properties and corrosion resistance. However, one of the unsolved problems for the manufacturability and the applications of bulk metallic glasses is that their glass-forming ability is very sensitive to the preparation techniques and impurity of components since oxygen in the environment would markedly deteriorate the glass-forming ability. Therefore, the aim of this study was to establish proper processing conditions to obtain a magnesium-based amorphous ternary alloy and its characterization. The final composition was prepared using two binary master alloys by melting in an induction furnace. Carbon steel crucible was used in argon atmosphere with and without addition of SF6 gas in order to minimize the oxygen contamination. The microstructure, amorphous nature, thermal properties and chemical analysis of samples were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and inductively coupled plasma emission spectrometry, respectively. The oxygen content of the as-cast samples was chemically analyzed by using carrier gas hot extraction (O/N Analyzer TC-436/LECO) and was kept bellow 25 ppm (without SF6) and 10 ppm (with SF6). Bulk samples were produced by rapid cooling in a cooper mold until 1.5 mm thickness, with amorphous structures being observed up to 2.5 mm. Magnesium-based bulk metallic glasses are attractive due to their single-phase, chemically homogeneous alloy system and the absence of second-phase, which could impair the mechanical properties and corrosion resistance. However, one of the unsolved problems for the manufacturability and the applications of bulk metallic glasses is that their glass-forming ability is very sensitive to the preparation techniques and impurity of components since oxygen in the environment would markedly deteriorate the glass-forming ability. Therefore, the aim of this study was to establish proper processing conditions to obtain a magnesium-based amorphous ternary alloy and its characterization. The final composition was prepared using two binary master alloys by melting in an induction furnace. Carbon steel crucible was used in argon atmosphere with and without addition of SF6 gas in order to minimize the oxygen contamination. The microstructure, amorphous nature, thermal properties and chemical analysis of samples were investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and inductively coupled plasma emission spectrometry, respectively. The oxygen content of the as-cast samples was chemically analyzed by using carrier gas hot extraction (O/N Analyzer TC-436/LECO) and was kept bellow 25ppm (without SF6) and 10ppm (with SF6). Bulk samples were produced by rapid cooling in a cooper mold until 1.5mm thickness, with amorphous structures being observed up to 2.5mm.
Author	Bolfarini, Claudemiro Kiminami, Claudio Shyinti Matias, Telma Blanco Asato, Gabriel Hitoshi Ramasco, Bruno Torquato Botta, Walter José
Author_xml	– sequence: 1 givenname: Telma Blanco surname: Matias fullname: Matias, Telma Blanco email: telmabmatias@gmail.com, telma_blanco@hotmail.com – sequence: 2 givenname: Gabriel Hitoshi surname: Asato fullname: Asato, Gabriel Hitoshi – sequence: 3 givenname: Bruno Torquato surname: Ramasco fullname: Ramasco, Bruno Torquato – sequence: 4 givenname: Walter José surname: Botta fullname: Botta, Walter José – sequence: 5 givenname: Claudio Shyinti surname: Kiminami fullname: Kiminami, Claudio Shyinti – sequence: 6 givenname: Claudemiro surname: Bolfarini fullname: Bolfarini, Claudemiro
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Title	Processing and characterization of amorphous magnesium based alloy for application in biomedical implants
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