Disorder in H + -irradiated HOPG: effect of impinging energy and dose on Raman D-band splitting and surface topography
Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H ions with energies of 0.4 MeV and 1 MeV, and doses of 10 ions/cm and 10 ions/cm . Raman spectroscopy was used as the main technique to characterize different samples and gain new insights on the splittin...
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| Published in: | Beilstein journal of nanotechnology Vol. 9; no. 1; pp. 2708 - 2717 |
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| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
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Beilstein-Institut zur Föerderung der Chemischen Wissenschaften
2018
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| Abstract | Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H
ions with energies of 0.4 MeV and 1 MeV, and doses of 10
ions/cm
and 10
ions/cm
. Raman spectroscopy was used as the main technique to characterize different samples and gain new insights on the splitting of the D band into two components (D
and D
), trying to correlate this feature of the vibrational spectrum with the impinging energy and dose. An increased
/
ratio in comparison with
/
was observed in the irradiated samples. This behavior indicates that the impinging energy mainly affects the D
component, while the D
component is strongly dominated by the dose. We expect a larger contribution of defects (originating from the rupture of C-C sp
symmetry through the formation of C-H sp
bonds) to the D
component than to the D
component. SQUID measurements of the irradiated samples showed an enhancement in the normalized remanence, as well as an increment in coercivity compared to pristine HOPG, consistent with H
-induced point-like defects as well as C-H bonds. AFM scanning after Raman and SQUID characterization showed a distribution of surface defects, which were ascribed to the burst of hydrogen blisters formed as a consequence of the irradiation process. The results presented in this work contribute to the current trend in nanotechnology in areas devoted to the control of properties by defect engineering in carbon-based materials. |
|---|---|
| AbstractList | Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H
ions with energies of 0.4 MeV and 1 MeV, and doses of 10
ions/cm
and 10
ions/cm
. Raman spectroscopy was used as the main technique to characterize different samples and gain new insights on the splitting of the D band into two components (D
and D
), trying to correlate this feature of the vibrational spectrum with the impinging energy and dose. An increased
/
ratio in comparison with
/
was observed in the irradiated samples. This behavior indicates that the impinging energy mainly affects the D
component, while the D
component is strongly dominated by the dose. We expect a larger contribution of defects (originating from the rupture of C-C sp
symmetry through the formation of C-H sp
bonds) to the D
component than to the D
component. SQUID measurements of the irradiated samples showed an enhancement in the normalized remanence, as well as an increment in coercivity compared to pristine HOPG, consistent with H
-induced point-like defects as well as C-H bonds. AFM scanning after Raman and SQUID characterization showed a distribution of surface defects, which were ascribed to the burst of hydrogen blisters formed as a consequence of the irradiation process. The results presented in this work contribute to the current trend in nanotechnology in areas devoted to the control of properties by defect engineering in carbon-based materials. Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H + ions with energies of 0.4 MeV and 1 MeV, and doses of 10 14 ions/cm 2 and 10 16 ions/cm 2 . Raman spectroscopy was used as the main technique to characterize different samples and gain new insights on the splitting of the D band into two components (D 1 and D 2 ), trying to correlate this feature of the vibrational spectrum with the impinging energy and dose. An increased I D2 / I G ratio in comparison with I D1 / I G was observed in the irradiated samples. This behavior indicates that the impinging energy mainly affects the D 1 component, while the D 2 component is strongly dominated by the dose. We expect a larger contribution of defects (originating from the rupture of C–C sp 2 symmetry through the formation of C–H sp 3 bonds) to the D 2 component than to the D 1 component. SQUID measurements of the irradiated samples showed an enhancement in the normalized remanence, as well as an increment in coercivity compared to pristine HOPG, consistent with H + -induced point-like defects as well as C–H bonds. AFM scanning after Raman and SQUID characterization showed a distribution of surface defects, which were ascribed to the burst of hydrogen blisters formed as a consequence of the irradiation process. The results presented in this work contribute to the current trend in nanotechnology in areas devoted to the control of properties by defect engineering in carbon-based materials. Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H+ ions with energies of 0.4 MeV and 1 MeV, and doses of 1014 ions/cm2 and 1016 ions/cm2. Raman spectroscopy was used as the main technique to characterize different samples and gain new insights on the splitting of the D band into two components (D1 and D2), trying to correlate this feature of the vibrational spectrum with the impinging energy and dose. An increased ID2/IG ratio in comparison with ID1/IG was observed in the irradiated samples. This behavior indicates that the impinging energy mainly affects the D1 component, while the D2 component is strongly dominated by the dose. We expect a larger contribution of defects (originating from the rupture of C–C sp2 symmetry through the formation of C–H sp3 bonds) to the D2 component than to the D1 component. SQUID measurements of the irradiated samples showed an enhancement in the normalized remanence, as well as an increment in coercivity compared to pristine HOPG, consistent with H+-induced point-like defects as well as C–H bonds. AFM scanning after Raman and SQUID characterization showed a distribution of surface defects, which were ascribed to the burst of hydrogen blisters formed as a consequence of the irradiation process. The results presented in this work contribute to the current trend in nanotechnology in areas devoted to the control of properties by defect engineering in carbon-based materials. Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H+ ions with energies of 0.4 MeV and 1 MeV, and doses of 1014 ions/cm2 and 1016 ions/cm2. Raman spectroscopy was used as the main technique to characterize different samples and gain new insights on the splitting of the D band into two components (D1 and D2), trying to correlate this feature of the vibrational spectrum with the impinging energy and dose. An increased I D2/I G ratio in comparison with I D1/I G was observed in the irradiated samples. This behavior indicates that the impinging energy mainly affects the D1 component, while the D2 component is strongly dominated by the dose. We expect a larger contribution of defects (originating from the rupture of C–C sp2 symmetry through the formation of C–H sp3 bonds) to the D2 component than to the D1 component. SQUID measurements of the irradiated samples showed an enhancement in the normalized remanence, as well as an increment in coercivity compared to pristine HOPG, consistent with H+-induced point-like defects as well as C–H bonds. AFM scanning after Raman and SQUID characterization showed a distribution of surface defects, which were ascribed to the burst of hydrogen blisters formed as a consequence of the irradiation process. The results presented in this work contribute to the current trend in nanotechnology in areas devoted to the control of properties by defect engineering in carbon-based materials. |
| Author | Bercoff, Paula G Venosta, Lisandro Suárez, Sergio Bajales, Noelia |
| AuthorAffiliation | 1 Universidad Nacional de Córdoba, FAMAF, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina 2 CONICET, IFEG, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina 3 Centro Atómico Bariloche. Av. Bustillo 9500. 8400 San Carlos de Bariloche, Argentina |
| AuthorAffiliation_xml | – name: 1 Universidad Nacional de Córdoba, FAMAF, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina – name: 3 Centro Atómico Bariloche. Av. Bustillo 9500. 8400 San Carlos de Bariloche, Argentina – name: 2 CONICET, IFEG, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina |
| Author_xml | – sequence: 1 givenname: Lisandro orcidid: 0000-0001-7073-8519 surname: Venosta fullname: Venosta, Lisandro organization: CONICET, IFEG, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina – sequence: 2 givenname: Noelia orcidid: 0000-0002-2507-9224 surname: Bajales fullname: Bajales, Noelia organization: CONICET, IFEG, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina – sequence: 3 givenname: Sergio surname: Suárez fullname: Suárez, Sergio organization: Centro Atómico Bariloche. Av. Bustillo 9500. 8400 San Carlos de Bariloche, Argentina – sequence: 4 givenname: Paula G orcidid: 0000-0002-0606-8407 surname: Bercoff fullname: Bercoff, Paula G organization: CONICET, IFEG, Medina Allende s/n, Ciudad Universitaria. 5000 Córdoba, Argentina |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30416922$$D View this record in MEDLINE/PubMed |
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| Cites_doi | 10.3390/c1010077 10.1021/nl300901a 10.1016/j.carbon.2015.12.101 10.1002/pssb.200982314 10.1063/1.4900613 10.1063/1.1674108 10.1002/pssb.201100295 10.1126/science.1167130 10.1103/physrevb.75.153401 10.3762/bjnano.3.96 10.1103/physrevb.80.245422 10.1103/physrevb.81.214404 10.1016/j.carbon.2009.07.033 10.1016/j.nimb.2010.02.091 10.1021/nl802940s 10.1016/j.cap.2015.12.021 10.1103/physrevb.24.1027 10.1103/physrevlett.88.027401 10.1016/j.mspro.2015.04.008 10.3762/bjnano.9.186 10.1007/s10853-006-1453-1 10.1038/nphys1399 10.1016/j.carbon.2012.05.008 10.1103/physrevb.72.085401 10.1002/9783527632695 10.1016/j.carbon.2009.01.032 10.1103/physrevlett.98.187204 10.1116/1.5034433 10.1016/j.carbon.2011.11.040 10.1016/j.carbon.2009.12.057 10.1038/nmat1996 10.1103/physrevlett.97.187401 10.1103/physrevb.61.14095 10.1021/nn201601m 10.1016/j.jnucmat.2010.06.007 10.1103/physrevb.85.144406 10.1016/j.surfcoat.2016.05.064 10.1103/physrevlett.91.227201 10.1039/b613962k 10.1016/j.jmmm.2009.06.038 10.1002/adma.200801205 10.1021/ja00015a012 10.3762/bjnano.9.52 10.1038/nature05545 |
| ContentType | Journal Article |
| Copyright | Copyright © 2018, Venosta et al.; licensee Beilstein-Institut. This work is published under http://creativecommons.org/licenses/by/4.0 (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. Copyright © 2018, Venosta et al. 2018 Venosta et al. |
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| Keywords | disorder Raman spectroscopy highly oriented pyrolytic graphite (HOPG) topography ion–solid interactions |
| Language | English |
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| Snippet | Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H
ions with energies of 0.4 MeV and 1 MeV, and doses of 10... Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H + ions with energies of 0.4 MeV and 1 MeV, and doses of 10 14... Disorder was induced in pristine highly oriented pyrolytic graphite (HOPG) by irradiation with H+ ions with energies of 0.4 MeV and 1 MeV, and doses of 1014... |
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| SubjectTerms | Blistering Blisters Carbon Coercivity Defects disorder Full Research Paper G ratio Graphite highly oriented pyrolytic graphite (HOPG) Hydrogen Hydrogenation ion–solid interactions Irradiation Nanoscience Nanotechnology Pyrolytic graphite Raman spectroscopy Remanence Spectrum analysis Splitting Squid Surface defects Topography |
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| Title | Disorder in H + -irradiated HOPG: effect of impinging energy and dose on Raman D-band splitting and surface topography |
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