Controlling particle size in the Stöber process and incorporation of calcium
[Display omitted] The Stӧber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process variables can be used to obtain monodispersed particles of specific size. The modal particle size could be selected within in the r...
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| Published in: | Journal of colloid and interface science Vol. 469; pp. 213 - 223 |
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| Main Authors: | , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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01-05-2016
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| Abstract | [Display omitted]
The Stӧber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process variables can be used to obtain monodispersed particles of specific size. The modal particle size could be selected within in the range 20–500nm. There is great therapeutic potential for bioactive glass nanoparticles, as they can be internalised within cells and perform sustained delivery of active ions. Biodegradable bioactive glass nanoparticles are also used in nanocomposites. Modification of the Stӧber process so that the particles can contain cations such as calcium, whilst maintaining monodispersity, is desirable. Here, whilst calcium incorporation is achieved, with a homogenous distribution, careful characterisation shows that much of the calcium is not incorporated. A maximum of 10mol% CaO can be achieved and previous reports are likely to have overestimated the amount of calcium incorporated. |
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| AbstractList | [Display omitted]
The Stӧber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process variables can be used to obtain monodispersed particles of specific size. The modal particle size could be selected within in the range 20–500nm. There is great therapeutic potential for bioactive glass nanoparticles, as they can be internalised within cells and perform sustained delivery of active ions. Biodegradable bioactive glass nanoparticles are also used in nanocomposites. Modification of the Stӧber process so that the particles can contain cations such as calcium, whilst maintaining monodispersity, is desirable. Here, whilst calcium incorporation is achieved, with a homogenous distribution, careful characterisation shows that much of the calcium is not incorporated. A maximum of 10mol% CaO can be achieved and previous reports are likely to have overestimated the amount of calcium incorporated. The Stӧber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process variables can be used to obtain monodispersed particles of specific size. The modal particle size could be selected within in the range 20-500 nm. There is great therapeutic potential for bioactive glass nanoparticles, as they can be internalised within cells and perform sustained delivery of active ions. Biodegradable bioactive glass nanoparticles are also used in nanocomposites. Modification of the Stӧber process so that the particles can contain cations such as calcium, whilst maintaining monodispersity, is desirable. Here, whilst calcium incorporation is achieved, with a homogenous distribution, careful characterisation shows that much of the calcium is not incorporated. A maximum of 10 mol% CaO can be achieved and previous reports are likely to have overestimated the amount of calcium incorporated. The Stoeber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process variables can be used to obtain monodispersed particles of specific size. The modal particle size could be selected within in the range 20-500 nm. There is great therapeutic potential for bioactive glass nanoparticles, as they can be internalised within cells and perform sustained delivery of active ions. Biodegradable bioactive glass nanoparticles are also used in nanocomposites. Modification of the Stoeber process so that the particles can contain cations such as calcium, whilst maintaining monodispersity, is desirable. Here, whilst calcium incorporation is achieved, with a homogenous distribution, careful characterisation shows that much of the calcium is not incorporated. A maximum of 10 mol% CaO can be achieved and previous reports are likely to have overestimated the amount of calcium incorporated. |
| Author | Sirovica, Slobodan Page, Samuel J. Riveiro, Antonio Jones, Julian R. Greasley, Sarah L. Martin, Richard A. Chen, Shu Porter, Alexandra E. Hanna, John V. |
| Author_xml | – sequence: 1 givenname: Sarah L. surname: Greasley fullname: Greasley, Sarah L. organization: Department of Materials, Imperial College London, UK – sequence: 2 givenname: Samuel J. surname: Page fullname: Page, Samuel J. organization: Department of Physics, University of Warwick, UK – sequence: 3 givenname: Slobodan surname: Sirovica fullname: Sirovica, Slobodan organization: School of Engineering & Applied Science and Aston Research Centre for Healthy Ageing, University of Aston, UK – sequence: 4 givenname: Shu surname: Chen fullname: Chen, Shu organization: Department of Materials, Imperial College London, UK – sequence: 5 givenname: Richard A. surname: Martin fullname: Martin, Richard A. organization: School of Engineering & Applied Science and Aston Research Centre for Healthy Ageing, University of Aston, UK – sequence: 6 givenname: Antonio surname: Riveiro fullname: Riveiro, Antonio organization: Department of Materials, Imperial College London, UK – sequence: 7 givenname: John V. surname: Hanna fullname: Hanna, John V. organization: Department of Physics, University of Warwick, UK – sequence: 8 givenname: Alexandra E. surname: Porter fullname: Porter, Alexandra E. organization: Department of Materials, Imperial College London, UK – sequence: 9 givenname: Julian R. orcidid: 0000-0002-2647-8024 surname: Jones fullname: Jones, Julian R. email: julian.r.jones@imperial.ac.uk organization: Department of Materials, Imperial College London, UK |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/26890387$$D View this record in MEDLINE/PubMed |
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| Copyright | 2016 Elsevier Inc. Copyright © 2016 Elsevier Inc. All rights reserved. |
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| Keywords | Nanoparticles Bioactive glass Stӧber process Biodegradable Sol–gel |
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The Stӧber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how... The Stӧber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process... The Stoeber process is commonly used for synthesising spherical silica particles. This article reports the first comprehensive study of how the process... |
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| SubjectTerms | Bioactive glass Biocompatibility Biodegradability Biodegradable Calcium Cations Glass Nanocomposites Nanoparticles Particle size Sol–gel Stӧber process |
| Title | Controlling particle size in the Stöber process and incorporation of calcium |
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