Rational design of Mg–Al mixed oxide-supported bimetallic catalysts for dry reforming of methane
A novel synthetic strategy for preparing bimetallic Ru–M (M = Cr, Fe, Co, Ni and Cu) catalysts, supported on Mg–Al mixed oxide, has been introduced. It was based on a “memory effect”, i.e. on the ability of Mg–Al mixed oxide to reconstruct a layered structure upon rehydration with an aqueous solutio...
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| Published in: | Applied catalysis. A, General Vol. 292; pp. 328 - 343 |
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| Main Authors: | , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
18-09-2005
Elsevier |
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| Abstract | A novel synthetic strategy for preparing bimetallic Ru–M (M
=
Cr, Fe, Co, Ni and Cu) catalysts, supported on Mg–Al mixed oxide, has been introduced. It was based on a “memory effect”, i.e. on the ability of Mg–Al mixed oxide to reconstruct a layered structure upon rehydration with an aqueous solution. By repeated calcinations–rehydration cycles, layered double hydroxide (LDH) precursors of catalysts containing two different metals were synthesized. Bimetallic catalysts were then generated (i) in situ from LDH under methane reforming reaction conditions and (ii) from mixed metal oxides obtained by preliminary LDH calcination. Among all the LDH-derived catalysts, a Ru
0.1%–Ni
5.0%/MgAlO
x
sample revealed the highest activity and selectivity to syngas, a suitable durability and a low coking capacity. A promoting effect of ruthenium on catalytic function of supported nickel was demonstrated. Preliminary LDH calcination was shown to markedly affect the catalytic activity of the derived catalysts and especially their coking properties. |
|---|---|
| AbstractList | A novel synthetic strategy for preparing bimetallic Ru-M (M=Cr, Fe, Co, Ni and Cu) catalysts, supported on Mg-Al mixed oxide, has been introduced. It was based on a 'memory effect', i.e. on the ability of Mg-Al mixed oxide to reconstruct a layered structure upon rehydration with an aqueous solution. By repeated calcinations-rehydration cycles, layered double hydroxide (LDH) precursors of catalysts containing two different metals were synthesized. Bimetallic catalysts were then generated (i) in situ from LDH under methane reforming reaction conditions and (ii) from mixed metal oxides obtained by preliminary LDH calcination. Among all the LDH-derived catalysts, a Ru0.1%-Ni5.0%/MgAlOx sample revealed the highest activity and selectivity to syngas, a suitable durability and a low coking capacity. A promoting effect of ruthenium on catalytic function of supported nickel was demonstrated. Preliminary LDH calcination was shown to markedly affect the catalytic activity of the derived catalysts and especially their coking properties. A novel synthetic strategy for preparing bimetallic Ru–M (M = Cr, Fe, Co, Ni and Cu) catalysts, supported on Mg–Al mixed oxide, has been introduced. It was based on a “memory effect”, i.e. on the ability of Mg–Al mixed oxide to reconstruct a layered structure upon rehydration with an aqueous solution. By repeated calcinations–rehydration cycles, layered double hydroxide (LDH) precursors of catalysts containing two different metals were synthesized. Bimetallic catalysts were then generated (i) in situ from LDH under methane reforming reaction conditions and (ii) from mixed metal oxides obtained by preliminary LDH calcination. Among all the LDH-derived catalysts, a Ru 0.1%–Ni 5.0%/MgAlO x sample revealed the highest activity and selectivity to syngas, a suitable durability and a low coking capacity. A promoting effect of ruthenium on catalytic function of supported nickel was demonstrated. Preliminary LDH calcination was shown to markedly affect the catalytic activity of the derived catalysts and especially their coking properties. |
| Author | Tsunoda, Tatsuo Hayakawa, Takashi Uchida, Kunio Takehira, Katsuomi Tsyganok, Andrey I. Inaba, Mieko Suzuki, Kunio |
| Author_xml | – sequence: 1 givenname: Andrey I. surname: Tsyganok fullname: Tsyganok, Andrey I. email: Andrey.Tsyganok@science.uottawa.ca organization: Centre for Catalysis Research and Innovation, Department of Chemistry, University of Ottawa, D’Iorio Hall, 10 Marie Curie Street, Ottawa, Ont., Canada K1N 6N5 – sequence: 2 givenname: Mieko surname: Inaba fullname: Inaba, Mieko organization: Natural Gas Technology Development Team, Teikoku Oil Co., 9-23-30 Kitakarasuyama, Setagaya-ku, Tokyo 157-0061, Japan – sequence: 3 givenname: Tatsuo surname: Tsunoda fullname: Tsunoda, Tatsuo organization: Institute for Materials and Chemical Process, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba Central 5, 1-1-1 Higashi, Tsukuba 305-8565, Japan – sequence: 4 givenname: Kunio surname: Uchida fullname: Uchida, Kunio organization: Institute for Materials and Chemical Process, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba Central 5, 1-1-1 Higashi, Tsukuba 305-8565, Japan – sequence: 5 givenname: Kunio surname: Suzuki fullname: Suzuki, Kunio organization: Institute for Materials and Chemical Process, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba Central 5, 1-1-1 Higashi, Tsukuba 305-8565, Japan – sequence: 6 givenname: Katsuomi surname: Takehira fullname: Takehira, Katsuomi organization: Department of Applied Chemistry, Faculty of Engineering, Hiroshima University, 1-4-1 Kagamiyama, Higashi-Hiroshima 739-8527, Japan – sequence: 7 givenname: Takashi surname: Hayakawa fullname: Hayakawa, Takashi email: T.Hayakawa@aist.go.jp organization: Institute for Materials and Chemical Process, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba Central 5, 1-1-1 Higashi, Tsukuba 305-8565, Japan |
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| Keywords | Methane Bimetallic catalysts Dry reforming Memory effect Synthesis gas Layered double hydroxides Hydroxides Oxides Iron Reforming Cobalt Supported catalyst Design Aluminium Oxides Alkane Copper Magnesium Oxides Platinoid Catalyst support Mixed catalyst Ruthenium Hydrocarbon Transition metal Heterogeneous catalysis Chromium Nickel |
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| Snippet | A novel synthetic strategy for preparing bimetallic Ru–M (M
=
Cr, Fe, Co, Ni and Cu) catalysts, supported on Mg–Al mixed oxide, has been introduced. It was... A novel synthetic strategy for preparing bimetallic Ru-M (M=Cr, Fe, Co, Ni and Cu) catalysts, supported on Mg-Al mixed oxide, has been introduced. It was based... |
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| SubjectTerms | Bimetallic catalysts Catalysis Chemistry Dry reforming Exact sciences and technology General and physical chemistry Layered double hydroxides Memory effect Methane Synthesis gas Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry |
| Title | Rational design of Mg–Al mixed oxide-supported bimetallic catalysts for dry reforming of methane |
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