Characterization, sintering and dielectric properties of nanocrystalline barium titanate synthesized through a modified combustion process
Nanocrystalline barium titanate has been synthesized through a modified combustion process in a single step for the first time. The as-prepared barium titanate powder is cubic perovskite with lattice constant a = 4.018 Å. The phase purity of the nanopowder was examined using thermo gravimetric analy...
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| Published in: | Materials characterization Vol. 60; no. 4; pp. 322 - 326 |
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| Main Authors: | , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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01-04-2009
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| Abstract | Nanocrystalline barium titanate has been synthesized through a modified combustion process in a single step for the first time. The as-prepared barium titanate powder is cubic perovskite with lattice constant
a
=
4.018 Å. The phase purity of the nanopowder was examined using thermo gravimetric analysis, differential thermal analysis and Fourier transform infrared spectroscopy. Transmission electron microscopic investigations have shown that the particle size of the as-prepared powder is in the range 20–40 nm. The agglomerate size distribution of the as-prepared powder was studied using atomic force microscopy. The nanoparticles of barium titanate were sintered to 97% of the theoretical density at a temperature of 1350 °C for 3 h. The microstructure of the sintered surface was examined using scanning electron microscopy. The dielectric constant and loss factor of the sintered pellets at 1 MHz measured at room temperature were 1223 and 3.5
×
10
−
3
respectively. |
|---|---|
| AbstractList | Nanocrystalline barium titanate was synthesised through a modified combustion process in a single step for the first time. The as-prepared barium titanate powder was cubic perovskite with lattice constant a = 4.018 Angstrom. The phase purity of the nanopowder was examined using TGA, DTA and FTIR. TEM showed that the particle size of the as-prepared powder was in the range 20-40 nm. The agglomerate size distribution of the as-prepared powder was studied using AFM. The barium titanate nanoparticles were sintered to 97% of theoretical density at 1350 C for 3 h. The microstructure of the sintered surface was examined by SEM. The dielectric constant and loss factor of the sintered pellets at 1 MHz measured at room temperature were 1223 and 3.5 x 10 exp(-3) respectively. Nanocrystalline barium titanate has been synthesized through a modified combustion process in a single step for the first time. The as-prepared barium titanate powder is cubic perovskite with lattice constant a = 4.018 A. The phase purity of the nanopowder was examined using thermo gravimetric analysis, differential thermal analysis and Fourier transform infrared spectroscopy. Transmission electron microscopic investigations have shown that the particle size of the as-prepared powder is in the range 20-40 nm. The agglomerate size distribution of the as-prepared powder was studied using atomic force microscopy. The nanoparticles of barium titanate were sintered to 97% of the theoretical density at a temperature of 1350 deg. C for 3 h. The microstructure of the sintered surface was examined using scanning electron microscopy. The dielectric constant and loss factor of the sintered pellets at 1 MHz measured at room temperature were 1223 and 3.5 x 10{sup -3} respectively. Nanocrystalline barium titanate has been synthesized through a modified combustion process in a single step for the first time. The as-prepared barium titanate powder is cubic perovskite with lattice constant a = 4.018 Å. The phase purity of the nanopowder was examined using thermo gravimetric analysis, differential thermal analysis and Fourier transform infrared spectroscopy. Transmission electron microscopic investigations have shown that the particle size of the as-prepared powder is in the range 20–40 nm. The agglomerate size distribution of the as-prepared powder was studied using atomic force microscopy. The nanoparticles of barium titanate were sintered to 97% of the theoretical density at a temperature of 1350 °C for 3 h. The microstructure of the sintered surface was examined using scanning electron microscopy. The dielectric constant and loss factor of the sintered pellets at 1 MHz measured at room temperature were 1223 and 3.5 × 10 − 3 respectively. |
| Author | Kumar, V.R. Wariar, P.R.S. George, C.N. Thomas, J.K. Koshy, J. Kumar, H.P. Jose, R. Suresh, M.K. |
| Author_xml | – sequence: 1 givenname: C.N. surname: George fullname: George, C.N. organization: Department of Physics, Bishop Moore College, Mavelikara, Kerala, India – sequence: 2 givenname: J.K. surname: Thomas fullname: Thomas, J.K. email: jkthomasemrl@gmail.com organization: Department of Physics, Mar Ivanios College, Thiruvananthapuram, Kerala, India – sequence: 3 givenname: H.P. surname: Kumar fullname: Kumar, H.P. organization: Department of Physics, Mar Ivanios College, Thiruvananthapuram, Kerala, India – sequence: 4 givenname: M.K. surname: Suresh fullname: Suresh, M.K. organization: Department of Physics, Mar Ivanios College, Thiruvananthapuram, Kerala, India – sequence: 5 givenname: V.R. surname: Kumar fullname: Kumar, V.R. organization: Department of Physics, University College, Thiruvananthapuram, Kerala, India – sequence: 6 givenname: P.R.S. surname: Wariar fullname: Wariar, P.R.S. organization: Department of Physics, University College, Thiruvananthapuram, Kerala, India – sequence: 7 givenname: R. surname: Jose fullname: Jose, R. organization: Nanoscience and Nanotechnology Initiative, National University of Singapore, Singapore – sequence: 8 givenname: J. surname: Koshy fullname: Koshy, J. organization: Department of Physics, Bishop Moore College, Mavelikara, Kerala, India |
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| Keywords | Nanoparticles Characterization Combustion synthesis Barium titanate Dielectric properties Synthesis Dielectric materials Sintering Combustion Powder metallurgy Ultrafine powder Nanocrystal |
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| Snippet | Nanocrystalline barium titanate has been synthesized through a modified combustion process in a single step for the first time. The as-prepared barium titanate... Nanocrystalline barium titanate was synthesised through a modified combustion process in a single step for the first time. The as-prepared barium titanate... |
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| SubjectTerms | Agglomeration Applied sciences ATOMIC FORCE MICROSCOPY BARIUM COMPOUNDS Barium titanate Barium titanates Characterization Combustion Combustion synthesis Cross-disciplinary physics: materials science; rheology CRYSTALS Dielectric properties DIFFERENTIAL THERMAL ANALYSIS Exact sciences and technology FOURIER TRANSFORM SPECTROMETERS GRAVIMETRIC ANALYSIS LATTICE PARAMETERS MATERIALS SCIENCE Metals. Metallurgy MHZ RANGE 01-100 MICROSTRUCTURE Nanocrystals Nanomaterials Nanoparticles Nanostructure NANOSTRUCTURES PELLETS PERMITTIVITY PEROVSKITE Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics Powder metallurgy. Composite materials Production techniques SCANNING ELECTRON MICROSCOPY Sintered metals and alloys. Pseudo alloys. Cermets SINTERING Solidification SURFACES SYNTHESIS TEMPERATURE RANGE 0273-0400 K TEMPERATURE RANGE 1000-4000 K TITANATES |
| Title | Characterization, sintering and dielectric properties of nanocrystalline barium titanate synthesized through a modified combustion process |
| URI | https://dx.doi.org/10.1016/j.matchar.2008.09.012 https://search.proquest.com/docview/1671373981 https://www.osti.gov/biblio/21192613 |
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