Chlorination of Calix[4]arene Derivatives

New convenient method for synthesis of p-chlorinated calix[4]arenes is reported. The sulfuryl chloride was used for chlorination of unsubstituted at the lower rim calix[4]arenes. The products of this reaction were very suitable for further O-alkylation.

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Bibliographic Details
Published in:Synthetic communications Vol. 45; no. 13; pp. 1592 - 1597
Main Authors: Ivanova, E. A., Prokhorova, P. E., Mitin, V. V., Glukhareva, T. V., Morzherin, Yu. Yu
Format: Journal Article
Language:English
Published: Philadelphia Taylor & Francis 03-07-2015
Taylor & Francis Ltd
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Description
Summary:New convenient method for synthesis of p-chlorinated calix[4]arenes is reported. The sulfuryl chloride was used for chlorination of unsubstituted at the lower rim calix[4]arenes. The products of this reaction were very suitable for further O-alkylation.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397911.2015.1036452