A waste valorization strategy for the synthesis of phenols from (hetero)arylboronic acids using pomegranate peel ash extract

Phenols are prominent in organic reactions and highly significant biologically active substances. We report a versatile and sustainable CuI-catalyzed protocol for their synthesis through an oxidative ipso-functionalization (hydroxy deborylation) strategy of (hetero)arylboronic acids [(H)ABAs] using...

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Published in:	Green chemistry letters and reviews Vol. 15; no. 2; pp. 427 - 436
Main Authors:	Lakshmidevi, Jangam, Ramesh Naidu, Bandameeda, Avula, Satya Kumar, Majhi, Anjoy, Chia, Poh Wai, Al-Harrasi, Ahmed, Venkateswarlu, Katta
Format:	Journal Article
Language:	English
Published:	Abingdon Taylor & Francis 03-04-2022 Taylor & Francis Ltd Taylor & Francis Group
Subjects:	Acids Air temperature Aqueous solutions Ashes Biological activity Catalysts Chemical synthesis CuI Flavonoids Functional groups Green chemistry Hydroxylation ipso-hydroxylation Laboratories Natural products Organic solvents Oxidants Oxidizing agents phenol synthesis Phenols Pomegranate peel ash Protocol Raw materials Reagents Room temperature Substrates Sustainability Sustainable development waste valorization technique
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Abstract	Phenols are prominent in organic reactions and highly significant biologically active substances. We report a versatile and sustainable CuI-catalyzed protocol for their synthesis through an oxidative ipso-functionalization (hydroxy deborylation) strategy of (hetero)arylboronic acids [(H)ABAs] using the water extract of pomegranate peel ash (WEPA) in open-air. They are formed at room temperature (RT). This process shows high significance toward the environmental sustainability over the reported procedures of ipso-hydroxylation of (H)ABAs. The application of a waste-derived biorenewable basic reaction medium, air as an oxidant, wide substrate scope, high functional group tolerance, reusability of the catalyst, ambient conditions, less expensive and safer catalyst with low loading, aqueous medium, avoidance of volatile organic solvents, and external oxidant, and tremendous further scope are the noteworthy features of this protocol.
AbstractList	Phenols are prominent in organic reactions and highly significant biologically active substances. We report a versatile and sustainable CuI-catalyzed protocol for their synthesis through an oxidative ipso-functionalization (hydroxy deborylation) strategy of (hetero)arylboronic acids [(H)ABAs] using the water extract of pomegranate peel ash (WEPA) in open-air. They are formed at room temperature (RT). This process shows high significance toward the environmental sustainability over the reported procedures of ipso-hydroxylation of (H)ABAs. The application of a waste-derived biorenewable basic reaction medium, air as an oxidant, wide substrate scope, high functional group tolerance, reusability of the catalyst, ambient conditions, less expensive and safer catalyst with low loading, aqueous medium, avoidance of volatile organic solvents, and external oxidant, and tremendous further scope are the noteworthy features of this protocol.
Author	Majhi, Anjoy Al-Harrasi, Ahmed Ramesh Naidu, Bandameeda Chia, Poh Wai Lakshmidevi, Jangam Venkateswarlu, Katta Avula, Satya Kumar
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SubjectTerms	Acids Air temperature Aqueous solutions Ashes Biological activity Catalysts Chemical synthesis CuI Flavonoids Functional groups Green chemistry Hydroxylation ipso-hydroxylation Laboratories Natural products Organic solvents Oxidants Oxidizing agents phenol synthesis Phenols Pomegranate peel ash Protocol Raw materials Reagents Room temperature Substrates Sustainability Sustainable development waste valorization technique
Title	A waste valorization strategy for the synthesis of phenols from (hetero)arylboronic acids using pomegranate peel ash extract
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