Hollow fiber liquid-phase microextraction combined with supercritical fluid chromatography coupled to mass spectrometry for multiclass emerging contaminant quantification in water samples

The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those analytes through the supercritical fluid chromatography usage is associated with many analytical benefits, which are significantly increased w...

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Published in:	Analytical and bioanalytical chemistry Vol. 413; no. 9; pp. 2467 - 2479
Main Authors:	Salvatierra-Stamp, Vilma del Carmen, Ceballos-Magaña, Silvia G., Pano-Farias, Norma Susana, Leyva-Morales, José Belisario, Pineda-Urbina, Kayim, Muñiz-Valencia, Roberto
Format:	Journal Article
Language:	English
Published:	Berlin/Heidelberg Springer Berlin Heidelberg 01-04-2021 Springer Springer Nature B.V
Subjects:	1-Octanol Analytical Chemistry Biochemistry Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Chromatography Contaminants Food Science Ions Laboratory Medicine Liquid chromatography Liquid phases Mass spectrometry Mass spectroscopy Mathematical analysis Methods Monitoring/Environmental Analysis Octanol Organic compounds Organic solvents Polypropylene Research Paper Scientific imaging Spectroscopy Supercritical fluids Trace levels Wastewater Water analysis Water pollution Water sampling Israel Multiclass emerging contaminants Hollow fiber liquid-phase microextraction Water samples Supercritical fluid chromatography
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Abstract	The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those analytes through the supercritical fluid chromatography usage is associated with many analytical benefits, which are significantly increased when it is coupled to a mass spectrometry detector, thus providing an extremely sensitive analytical technique with minimal consumption of organic solvents. On account of this, a hollow fiber liquid-phase microextraction technique in two-phase mode combined with supercritical fluid chromatography coupled to mass spectrometry was developed for quantifying 19 multiclass emerging contaminants in water samples in a total chromatographic time of 5.5 min. The analytical method used 40 μL of 1-octanol placed in the porous-walled polypropylene fiber as the acceptor phase, and 1 L of water sample was the donor phase. After extraction and quantification techniques were optimized in detail, a good determination coefficient ( r 2 > 0.9905) in the range of 0.1 to 100 μg L −1 , for most of the analytes, and an enrichment factor in the range of 7 to 28,985 were obtained. The recovery percentage (%R) and intraday precision (%RSD) were in the range of 80.80–123.40%, and from 0.48 to 16.89%, respectively. Limit of detection and quantification ranged from 1.90 to 35.66 ng L −1 , and from 3.41 to 62.11 ng L −1 , respectively. Finally, the developed method was successfully used for the determination of the 19 multiclass emerging contaminants in superficial and wastewater samples.
AbstractList	The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those analytes through the supercritical fluid chromatography usage is associated with many analytical benefits, which are significantly increased when it is coupled to a mass spectrometry detector, thus providing an extremely sensitive analytical technique with minimal consumption of organic solvents. On account of this, a hollow fiber liquid-phase microextraction technique in two-phase mode combined with supercritical fluid chromatography coupled to mass spectrometry was developed for quantifying 19 multiclass emerging contaminants in water samples in a total chromatographic time of 5.5 min. The analytical method used 40 μL of 1-octanol placed in the porous-walled polypropylene fiber as the acceptor phase, and 1 L of water sample was the donor phase. After extraction and quantification techniques were optimized in detail, a good determination coefficient (r > 0.9905) in the range of 0.1 to 100 μg L , for most of the analytes, and an enrichment factor in the range of 7 to 28,985 were obtained. The recovery percentage (%R) and intraday precision (%RSD) were in the range of 80.80-123.40%, and from 0.48 to 16.89%, respectively. Limit of detection and quantification ranged from 1.90 to 35.66 ng L , and from 3.41 to 62.11 ng L , respectively. Finally, the developed method was successfully used for the determination of the 19 multiclass emerging contaminants in superficial and wastewater samples. The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those analytes through the supercritical fluid chromatography usage is associated with many analytical benefits, which are significantly increased when it is coupled to a mass spectrometry detector, thus providing an extremely sensitive analytical technique with minimal consumption of organic solvents. On account of this, a hollow fiber liquid-phase microextraction technique in two-phase mode combined with supercritical fluid chromatography coupled to mass spectrometry was developed for quantifying 19 multiclass emerging contaminants in water samples in a total chromatographic time of 5.5 min. The analytical method used 40 μL of 1-octanol placed in the porous-walled polypropylene fiber as the acceptor phase, and 1 L of water sample was the donor phase. After extraction and quantification techniques were optimized in detail, a good determination coefficient ( r 2 > 0.9905) in the range of 0.1 to 100 μg L −1 , for most of the analytes, and an enrichment factor in the range of 7 to 28,985 were obtained. The recovery percentage (%R) and intraday precision (%RSD) were in the range of 80.80–123.40%, and from 0.48 to 16.89%, respectively. Limit of detection and quantification ranged from 1.90 to 35.66 ng L −1 , and from 3.41 to 62.11 ng L −1 , respectively. Finally, the developed method was successfully used for the determination of the 19 multiclass emerging contaminants in superficial and wastewater samples. The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those analytes through the supercritical fluid chromatography usage is associated with many analytical benefits, which are significantly increased when it is coupled to a mass spectrometry detector, thus providing an extremely sensitive analytical technique with minimal consumption of organic solvents. On account of this, a hollow fiber liquid-phase microextraction technique in two-phase mode combined with supercritical fluid chromatography coupled to mass spectrometry was developed for quantifying 19 multiclass emerging contaminants in water samples in a total chromatographic time of 5.5 min. The analytical method used 40 μL of 1-octanol placed in the porous-walled polypropylene fiber as the acceptor phase, and 1 L of water sample was the donor phase. After extraction and quantification techniques were optimized in detail, a good determination coefficient (r2 > 0.9905) in the range of 0.1 to 100 μg L−1, for most of the analytes, and an enrichment factor in the range of 7 to 28,985 were obtained. The recovery percentage (%R) and intraday precision (%RSD) were in the range of 80.80–123.40%, and from 0.48 to 16.89%, respectively. Limit of detection and quantification ranged from 1.90 to 35.66 ng L−1, and from 3.41 to 62.11 ng L−1, respectively. Finally, the developed method was successfully used for the determination of the 19 multiclass emerging contaminants in superficial and wastewater samples. The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those analytes through the supercritical fluid chromatography usage is associated with many analytical benefits, which are significantly increased when it is coupled to a mass spectrometry detector, thus providing an extremely sensitive analytical technique with minimal consumption of organic solvents. On account of this, a hollow fiber liquid-phase microextraction technique in two-phase mode combined with supercritical fluid chromatography coupled to mass spectrometry was developed for quantifying 19 multiclass emerging contaminants in water samples in a total chromatographic time of 5.5 min. The analytical method used 40 [mu]L of 1-octanol placed in the porous-walled polypropylene fiber as the acceptor phase, and 1 L of water sample was the donor phase. After extraction and quantification techniques were optimized in detail, a good determination coefficient (r.sup.2 > 0.9905) in the range of 0.1 to 100 [mu]g L.sup.-1, for most of the analytes, and an enrichment factor in the range of 7 to 28,985 were obtained. The recovery percentage (%R) and intraday precision (%RSD) were in the range of 80.80-123.40%, and from 0.48 to 16.89%, respectively. Limit of detection and quantification ranged from 1.90 to 35.66 ng L.sup.-1, and from 3.41 to 62.11 ng L.sup.-1, respectively. Finally, the developed method was successfully used for the determination of the 19 multiclass emerging contaminants in superficial and wastewater samples.
Audience	Academic
Author	Pano-Farias, Norma Susana Ceballos-Magaña, Silvia G. Salvatierra-Stamp, Vilma del Carmen Muñiz-Valencia, Roberto Pineda-Urbina, Kayim Leyva-Morales, José Belisario
Author_xml	– sequence: 1 givenname: Vilma del Carmen surname: Salvatierra-Stamp fullname: Salvatierra-Stamp, Vilma del Carmen organization: Facultad de Ciencias Químicas, Universidad de Colima – sequence: 2 givenname: Silvia G. surname: Ceballos-Magaña fullname: Ceballos-Magaña, Silvia G. organization: Facultad de Ciencias, Universidad de Colima – sequence: 3 givenname: Norma Susana surname: Pano-Farias fullname: Pano-Farias, Norma Susana organization: Centro de Innovación y Desarrollo Agroalimentario de Michoacán, CIDAM A.C – sequence: 4 givenname: José Belisario surname: Leyva-Morales fullname: Leyva-Morales, José Belisario organization: Departamento de Salud, Universidad Autónoma de Occidente – sequence: 5 givenname: Kayim surname: Pineda-Urbina fullname: Pineda-Urbina, Kayim organization: Facultad de Ciencias Químicas, Universidad de Colima – sequence: 6 givenname: Roberto surname: Muñiz-Valencia fullname: Muñiz-Valencia, Roberto email: robemuva@yahoo.com organization: Facultad de Ciencias Químicas, Universidad de Colima
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CitedBy_id	crossref_primary_10_1016_j_greeac_2022_100023 crossref_primary_10_1016_j_microc_2024_110445 crossref_primary_10_1021_acs_est_3c00120 crossref_primary_10_1016_j_trac_2022_116550
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Keywords	Multiclass emerging contaminants Hollow fiber liquid-phase microextraction Water samples Supercritical fluid chromatography
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Snippet	The hollow fiber liquid-phase microextraction allows highly selective concentration of organic compounds that are at trace levels. The determination of those...
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SubjectTerms	1-Octanol Analytical Chemistry Biochemistry Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Chromatography Contaminants Food Science Ions Laboratory Medicine Liquid chromatography Liquid phases Mass spectrometry Mass spectroscopy Mathematical analysis Methods Monitoring/Environmental Analysis Octanol Organic compounds Organic solvents Polypropylene Research Paper Scientific imaging Spectroscopy Supercritical fluids Trace levels Wastewater Water analysis Water pollution Water sampling
Title	Hollow fiber liquid-phase microextraction combined with supercritical fluid chromatography coupled to mass spectrometry for multiclass emerging contaminant quantification in water samples
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