Preparation of poly(N-vinylpyrrolidone)-stabilized ZnO colloid nanoparticles

We propose a method for the synthesis of a colloidal ZnO solution with poly(N-vinylpyrrolidone) (PVP) as stabilizer. Stable colloidal solutions with good luminescence properties are obtained by using PVP as stabilizer in the synthesis of ZnO nanoparticles by a sol-gel method assisted by ultrasound....

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Published in:	Beilstein journal of nanotechnology Vol. 5; no. 1; pp. 402 - 406
Main Authors:	Gutul, Tatyana, Rusu, Emil, Condur, Nadejda, Ursaki, Veaceslav, Goncearenco, Evgenii, Vlazan, Paulina
Format:	Journal Article
Language:	English
Published:	Germany Beilstein-Institut 03-04-2014
Subjects:	colloidal solutions Full Research Paper nanocomposite Nanoscience Nanotechnology poly(N-vinylpyrrolidone) sol–gel zinc oxide poly(N-vinylpyrrolidone) nanocomposite colloidal solutions sol–gel zinc oxide
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Abstract	We propose a method for the synthesis of a colloidal ZnO solution with poly(N-vinylpyrrolidone) (PVP) as stabilizer. Stable colloidal solutions with good luminescence properties are obtained by using PVP as stabilizer in the synthesis of ZnO nanoparticles by a sol-gel method assisted by ultrasound. Nanoparticles with sizes of 30-40 nm in a PVP matrix are produced as a solid product. The colloidal ZnO/PVP/methanol solution, apart from the most intense PL band at 356 nm coming from the PVP, exhibits a strong PL band at 376 nm (3.30 eV) which corresponds to the emission of the free exciton recombination in ZnO nanoparticles.
AbstractList	We propose a method for the synthesis of a colloidal ZnO solution with poly( N -vinylpyrrolidone) (PVP) as stabilizer. Stable colloidal solutions with good luminescence properties are obtained by using PVP as stabilizer in the synthesis of ZnO nanoparticles by a sol–gel method assisted by ultrasound. Nanoparticles with sizes of 30–40 nm in a PVP matrix are produced as a solid product. The colloidal ZnO/PVP/methanol solution, apart from the most intense PL band at 356 nm coming from the PVP, exhibits a strong PL band at 376 nm (3.30 eV) which corresponds to the emission of the free exciton recombination in ZnO nanoparticles. We propose a method for the synthesis of a colloidal ZnO solution with poly(N-vinylpyrrolidone) (PVP) as stabilizer. Stable colloidal solutions with good luminescence properties are obtained by using PVP as stabilizer in the synthesis of ZnO nanoparticles by a sol-gel method assisted by ultrasound. Nanoparticles with sizes of 30-40 nm in a PVP matrix are produced as a solid product. The colloidal ZnO/PVP/methanol solution, apart from the most intense PL band at 356 nm coming from the PVP, exhibits a strong PL band at 376 nm (3.30 eV) which corresponds to the emission of the free exciton recombination in ZnO nanoparticles.
Author	Condur, Nadejda Rusu, Emil Gutul, Tatyana Vlazan, Paulina Ursaki, Veaceslav Goncearenco, Evgenii
AuthorAffiliation	3 National Institute of Electrochemistry and Condensed Matter, 144 Dr. A. Paunescu Podeanu str., Timisoara 300569, Romania 1 Institute of Electronic Engineering and Nanotechnologies D. Ghitu, Academy of Sciences of Moldova, 3 Academiei str., Chisinau, MD-2028, Moldova 2 State University of Republic of Moldova, 60 Alexe Mateevici str., Chisinau MD-2009, Moldova
AuthorAffiliation_xml	– name: 3 National Institute of Electrochemistry and Condensed Matter, 144 Dr. A. Paunescu Podeanu str., Timisoara 300569, Romania – name: 2 State University of Republic of Moldova, 60 Alexe Mateevici str., Chisinau MD-2009, Moldova – name: 1 Institute of Electronic Engineering and Nanotechnologies D. Ghitu, Academy of Sciences of Moldova, 3 Academiei str., Chisinau, MD-2028, Moldova
Author_xml	– sequence: 1 givenname: Tatyana surname: Gutul fullname: Gutul, Tatyana organization: Institute of Electronic Engineering and Nanotechnologies D. Ghitu, Academy of Sciences of Moldova, 3 Academiei str., Chisinau, MD-2028, Moldova – sequence: 2 givenname: Emil surname: Rusu fullname: Rusu, Emil organization: Institute of Electronic Engineering and Nanotechnologies D. Ghitu, Academy of Sciences of Moldova, 3 Academiei str., Chisinau, MD-2028, Moldova – sequence: 3 givenname: Nadejda surname: Condur fullname: Condur, Nadejda organization: Institute of Electronic Engineering and Nanotechnologies D. Ghitu, Academy of Sciences of Moldova, 3 Academiei str., Chisinau, MD-2028, Moldova – sequence: 4 givenname: Veaceslav surname: Ursaki fullname: Ursaki, Veaceslav organization: Institute of Electronic Engineering and Nanotechnologies D. Ghitu, Academy of Sciences of Moldova, 3 Academiei str., Chisinau, MD-2028, Moldova – sequence: 5 givenname: Evgenii surname: Goncearenco fullname: Goncearenco, Evgenii organization: State University of Republic of Moldova, 60 Alexe Mateevici str., Chisinau MD-2009, Moldova – sequence: 6 givenname: Paulina surname: Vlazan fullname: Vlazan, Paulina organization: National Institute of Electrochemistry and Condensed Matter, 144 Dr. A. Paunescu Podeanu str., Timisoara 300569, Romania
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Keywords	poly(N-vinylpyrrolidone) nanocomposite colloidal solutions sol–gel zinc oxide
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Title	Preparation of poly(N-vinylpyrrolidone)-stabilized ZnO colloid nanoparticles
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