Shrinking of Rapidly Evaporating Water Microdroplets Reveals their Extreme Supercooling

The fast evaporative cooling of micrometer-sized water droplets in a vacuum offers the appealing possibility to investigate supercooled water-below the melting point but still a liquid-at temperatures far beyond the state of the art. However, it is challenging to obtain a reliable value of the dropl...

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Published in:	Physical review letters Vol. 120; no. 1; p. 015501
Main Authors:	Goy, Claudia, Potenza, Marco A C, Dedera, Sebastian, Tomut, Marilena, Guillerm, Emmanuel, Kalinin, Anton, Voss, Kay-Obbe, Schottelius, Alexander, Petridis, Nikolaos, Prosvetov, Alexey, Tejeda, Guzmán, Fernández, José M, Trautmann, Christina, Caupin, Frédéric, Glasmacher, Ulrich, Grisenti, Robert E
Format:	Journal Article
Language:	English
Published:	United States American Physical Society 05-01-2018
Subjects:	Chemical Sciences Engineering Sciences Physics Temperature Liquids Sample preparation Raman spectroscopy Light scattering Structural properties
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Abstract	The fast evaporative cooling of micrometer-sized water droplets in a vacuum offers the appealing possibility to investigate supercooled water-below the melting point but still a liquid-at temperatures far beyond the state of the art. However, it is challenging to obtain a reliable value of the droplet temperature under such extreme experimental conditions. Here, the observation of morphology-dependent resonances in the Raman scattering from a train of perfectly uniform water droplets allows us to measure the variation in droplet size resulting from evaporative mass losses with an absolute precision of better than 0.2%. This finding proves crucial to an unambiguous determination of the droplet temperature. In particular, we find that a fraction of water droplets with an initial diameter of 6379±12 nm remain liquid down to 230.6±0.6 K. Our results question temperature estimates reported recently for larger supercooled water droplets and provide valuable information on the hydrogen-bond network in liquid water in the hard-to-access deeply supercooled regime.
AbstractList	The fast evaporative cooling of micrometer-sized water droplets in a vacuum offers the appealing possibility to investigate supercooled water-below the melting point but still a liquid-at temperatures far beyond the state of the art. However, it is challenging to obtain a reliable value of the droplet temperature under such extreme experimental conditions. Here, the observation of morphology-dependent resonances in the Raman scattering from a train of perfectly uniform water droplets allows us to measure the variation in droplet size resulting from evaporative mass losses with an absolute precision of better than 0.2%. This finding proves crucial to an unambiguous determination of the droplet temperature. In particular, we find that a fraction of water droplets with an initial diameter of 6379±12 nm remain liquid down to 230.6±0.6 K. Our results question temperature estimates reported recently for larger supercooled water droplets and provide valuable information on the hydrogen-bond network in liquid water in the hard-to-access deeply supercooled regime.
ArticleNumber	015501
Author	Petridis, Nikolaos Glasmacher, Ulrich Trautmann, Christina Kalinin, Anton Tejeda, Guzmán Guillerm, Emmanuel Fernández, José M Potenza, Marco A C Caupin, Frédéric Goy, Claudia Schottelius, Alexander Grisenti, Robert E Tomut, Marilena Prosvetov, Alexey Voss, Kay-Obbe Dedera, Sebastian
Author_xml	– sequence: 1 givenname: Claudia surname: Goy fullname: Goy, Claudia organization: Institut für Kernphysik, J. W. Goethe-Universität Frankfurt(M), 60438 Frankfurt(M), Germany – sequence: 2 givenname: Marco A C surname: Potenza fullname: Potenza, Marco A C organization: Dipartimento di Fisica, Università degli Studi di Milano, 20133 Milano, Italy – sequence: 3 givenname: Sebastian surname: Dedera fullname: Dedera, Sebastian organization: Institute of Earth Sciences, 69120 Heidelberg, Germany – sequence: 4 givenname: Marilena surname: Tomut fullname: Tomut, Marilena organization: GSI-Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt, Germany – sequence: 5 givenname: Emmanuel surname: Guillerm fullname: Guillerm, Emmanuel organization: Université Lyon, Université Claude Bernard Lyon 1, CNRS, Institut Lumière Matière, 69622 Lyon, France – sequence: 6 givenname: Anton surname: Kalinin fullname: Kalinin, Anton organization: GSI-Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt, Germany – sequence: 7 givenname: Kay-Obbe surname: Voss fullname: Voss, Kay-Obbe organization: GSI-Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt, Germany – sequence: 8 givenname: Alexander surname: Schottelius fullname: Schottelius, Alexander organization: Institut für Kernphysik, J. W. Goethe-Universität Frankfurt(M), 60438 Frankfurt(M), Germany – sequence: 9 givenname: Nikolaos surname: Petridis fullname: Petridis, Nikolaos organization: GSI-Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt, Germany – sequence: 10 givenname: Alexey surname: Prosvetov fullname: Prosvetov, Alexey organization: GSI-Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt, Germany – sequence: 11 givenname: Guzmán surname: Tejeda fullname: Tejeda, Guzmán organization: Laboratory of Molecular Fluid Dynamics, Instituto de Estructura de la Materia, CSIC, 28006 Madrid, Spain – sequence: 12 givenname: José M surname: Fernández fullname: Fernández, José M organization: Laboratory of Molecular Fluid Dynamics, Instituto de Estructura de la Materia, CSIC, 28006 Madrid, Spain – sequence: 13 givenname: Christina surname: Trautmann fullname: Trautmann, Christina organization: Material- und Geowissenschaften, Technische Universität Darmstadt, 64287 Darmstadt, Germany – sequence: 14 givenname: Frédéric surname: Caupin fullname: Caupin, Frédéric organization: Université Lyon, Université Claude Bernard Lyon 1, CNRS, Institut Lumière Matière, 69622 Lyon, France – sequence: 15 givenname: Ulrich surname: Glasmacher fullname: Glasmacher, Ulrich organization: Institute of Earth Sciences, 69120 Heidelberg, Germany – sequence: 16 givenname: Robert E surname: Grisenti fullname: Grisenti, Robert E organization: GSI-Helmholtzzentrum für Schwerionenforschung, 64291 Darmstadt, Germany
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Snippet	The fast evaporative cooling of micrometer-sized water droplets in a vacuum offers the appealing possibility to investigate supercooled water-below the melting... The fast evaporative cooling of micrometer-sized water droplets in a vacuum offers the appealing possibility to investigate supercooled water—below the melting...
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Title	Shrinking of Rapidly Evaporating Water Microdroplets Reveals their Extreme Supercooling
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