Electrodeposition of platinum on polytyramine-modified electrodes for electrocatalytic applications

Cyclic voltammetry was used in order to deposit conducting polytyramine (PTy) on graphite substrates. In acidic media, ca. 40 deposition cycles resulted in the formation of stable polymer films with reasonably good resistivity. Electrochemical deposition of platinum on the PTy-covered graphite subst...

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Published in:	Electrochimica acta Vol. 54; no. 12; pp. 3316 - 3319
Main Authors:	Spătaru, Tanţa, Marcu, Maria, Banu, Alexandra, Roman, Eugen, Spătaru, Nicolae
Format:	Journal Article
Language:	English
Published:	Kidlington Elsevier Ltd 30-04-2009 Elsevier
Subjects:	Chemistry Composite material Electrochemistry Electrodeposition Exact sciences and technology General and physical chemistry Phenol oxidation Platinum deposition Polytyramine Study of interfaces Phenol oxidation Polytyramine Composite material Platinum deposition Aromatic polymer Transition metal Ether polymer Functional polymer Sulfuric acid Electrodes Electrocatalysis Phenylene derivative polymer Amine polymer Platinum Graphite Phenols Electrodeposition Oxidation Electrochemical reaction Application Modified material
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Abstract	Cyclic voltammetry was used in order to deposit conducting polytyramine (PTy) on graphite substrates. In acidic media, ca. 40 deposition cycles resulted in the formation of stable polymer films with reasonably good resistivity. Electrochemical deposition of platinum on the PTy-covered graphite substrate allowed us to obtain a composite material that exhibits, for a platinum loading of 0.34 mg cm −2, a specific electrochemically active surface area of the Pt particles of ca. 57 m 2 g −1. Good electrocatalytic activity of this electrode material for phenol oxidation in acidic media was found, and the results suggested that, when deposited as small particles in a PTy matrix, platinum is less sensitive to deactivation by phenol oxidation polymeric products.
AbstractList	Cyclic voltammetry was used in order to deposit conducting polytyramine (PTy) on graphite substrates. In acidic media, ca. 40 deposition cycles resulted in the formation of stable polymer films with reasonably good resistivity. Electrochemical deposition of platinum on the PTy-covered graphite substrate allowed us to obtain a composite material that exhibits, for a platinum loading of 0.34 mg cm-2, a specific electrochemically active surface area of the Pt particles of ca. 57 m2 g-1. Good electrocatalytic activity of this electrode material for phenol oxidation in acidic media was found, and the results suggested that, when deposited as small particles in a PTy matrix, platinum is less sensitive to deactivation by phenol oxidation polymeric products. Cyclic voltammetry was used in order to deposit conducting polytyramine (PTy) on graphite substrates. In acidic media, ca. 40 deposition cycles resulted in the formation of stable polymer films with reasonably good resistivity. Electrochemical deposition of platinum on the PTy-covered graphite substrate allowed us to obtain a composite material that exhibits, for a platinum loading of 0.34 mg cm −2, a specific electrochemically active surface area of the Pt particles of ca. 57 m 2 g −1. Good electrocatalytic activity of this electrode material for phenol oxidation in acidic media was found, and the results suggested that, when deposited as small particles in a PTy matrix, platinum is less sensitive to deactivation by phenol oxidation polymeric products.
Author	Marcu, Maria Spătaru, Nicolae Roman, Eugen Spătaru, Tanţa Banu, Alexandra
Author_xml	– sequence: 1 givenname: Tanţa surname: Spătaru fullname: Spătaru, Tanţa organization: Institute of Physical Chemistry “Ilie Murgulescu”, 202 Spl. Independenţei, 060021, Bucharest, Romania – sequence: 2 givenname: Maria surname: Marcu fullname: Marcu, Maria organization: Institute of Physical Chemistry “Ilie Murgulescu”, 202 Spl. Independenţei, 060021, Bucharest, Romania – sequence: 3 givenname: Alexandra surname: Banu fullname: Banu, Alexandra organization: University POLITEHNICA Bucharest, Faculty of Engineering and Management of Technological Systems, 313 Spl. Independenţei, 060042, Bucharest, Romania – sequence: 4 givenname: Eugen surname: Roman fullname: Roman, Eugen organization: Institute of Physical Chemistry “Ilie Murgulescu”, 202 Spl. Independenţei, 060021, Bucharest, Romania – sequence: 5 givenname: Nicolae surname: Spătaru fullname: Spătaru, Nicolae email: nspataru@chimfiz.icf.ro organization: Institute of Physical Chemistry “Ilie Murgulescu”, 202 Spl. Independenţei, 060021, Bucharest, Romania
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Keywords	Phenol oxidation Polytyramine Composite material Platinum deposition Aromatic polymer Transition metal Ether polymer Functional polymer Sulfuric acid Electrodes Electrocatalysis Phenylene derivative polymer Amine polymer Platinum Graphite Phenols Electrodeposition Oxidation Electrochemical reaction Application Modified material
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Title	Electrodeposition of platinum on polytyramine-modified electrodes for electrocatalytic applications
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