Fused Nickel(II) Porphyrins—Sensing of Toxic Anions and Selected Metal Ions Through Supramolecular Interactions
Ni(II) porphyrins having fused –NH group were synthesized and characterized by various spectroscopic techniques. The fused porphyrins 1 and 2 were used to detect species of opposite polarity. 1 was used to sense toxic anions viz . cyanide and fluoride ions whereas 2 was used for detecting some selec...
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| Published in: | Frontiers in chemistry Vol. 8 |
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| Abstract | Ni(II) porphyrins having fused –NH group were synthesized and characterized by various spectroscopic techniques. The fused porphyrins
1
and
2
were used to detect species of opposite polarity.
1
was used to sense toxic anions
viz
. cyanide and fluoride ions whereas
2
was used for detecting some selective metal ions including toxic mercury(II) ions.
1
is having acidic –NH proton, which detects anions
via
hydrogen bonding interactions followed by anion-induced deprotonation. On the other hand,
2
senses the metal species
via
weak charge transfer interactions from oxygen atom of the formyl group to the added metal ions. The limit of detection was calculated in case of
1
as 2.13 and 3.15 ppm for cyanide and fluoride ions, respectively. Similarly, the detection limit was found to be 0.930, 2.231, and 0.718 ppm for Cu(II), Fe(III), and Hg(II) ions, respectively, for probe
2
. The probes were recovered and reused for several cycles. |
|---|---|
| AbstractList | Ni(II) porphyrins having fused –NH group were synthesized and characterized by various spectroscopic techniques. The fused porphyrins 1 and 2 were used to detect species of opposite polarity. 1 was used to sense toxic anions viz. cyanide and fluoride ions whereas 2 was used for detecting some selective metal ions including toxic mercury(II) ions. 1 is having acidic –NH proton, which detects anions via hydrogen bonding interactions followed by anion-induced deprotonation. On the other hand, 2 senses the metal species via weak charge transfer interactions from oxygen atom of the formyl group to the added metal ions. The limit of detection was calculated in case of 1 as 2.13 and 3.15 ppm for cyanide and fluoride ions, respectively. Similarly, the detection limit was found to be 0.930, 2.231, and 0.718 ppm for Cu(II), Fe(III), and Hg(II) ions, respectively, for probe 2. The probes were recovered and reused for several cycles. Ni(II) porphyrins having fused –NH group were synthesized and characterized by various spectroscopic techniques. The fused porphyrins 1 and 2 were used to detect species of opposite polarity. 1 was used to sense toxic anions viz . cyanide and fluoride ions whereas 2 was used for detecting some selective metal ions including toxic mercury(II) ions. 1 is having acidic –NH proton, which detects anions via hydrogen bonding interactions followed by anion-induced deprotonation. On the other hand, 2 senses the metal species via weak charge transfer interactions from oxygen atom of the formyl group to the added metal ions. The limit of detection was calculated in case of 1 as 2.13 and 3.15 ppm for cyanide and fluoride ions, respectively. Similarly, the detection limit was found to be 0.930, 2.231, and 0.718 ppm for Cu(II), Fe(III), and Hg(II) ions, respectively, for probe 2 . The probes were recovered and reused for several cycles. |
| Author | Sankar, Muniappan Dar, Tawseef Ahmad |
| AuthorAffiliation | Department of Chemistry, Indian Institute of Technology , Roorkee , India |
| AuthorAffiliation_xml | – name: Department of Chemistry, Indian Institute of Technology , Roorkee , India |
| Author_xml | – sequence: 1 givenname: Tawseef Ahmad surname: Dar fullname: Dar, Tawseef Ahmad – sequence: 2 givenname: Muniappan surname: Sankar fullname: Sankar, Muniappan |
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| CitedBy_id | crossref_primary_10_1007_s00604_022_05430_2 crossref_primary_10_1016_j_addr_2022_114134 crossref_primary_10_3390_nano12111930 crossref_primary_10_1016_j_diamond_2024_111265 crossref_primary_10_1016_j_dyepig_2022_110573 crossref_primary_10_1039_D2CP00408A crossref_primary_10_1039_D2CP01553F crossref_primary_10_1039_D1RA06567J |
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| Notes | Edited by: Mosae Selvakumar Paulraj, Asian University for Women, Bangladesh Reviewed by: Paramasivan Rajasingh, Chikkanna Government Arts College, India; Lokesh K. Kumawat, Maynooth University, Ireland This article was submitted to Supramolecular Chemistry, a section of the journal Frontiers in Chemistry |
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| Snippet | Ni(II) porphyrins having fused –NH group were synthesized and characterized by various spectroscopic techniques. The fused porphyrins
1
and
2
were used to... Ni(II) porphyrins having fused –NH group were synthesized and characterized by various spectroscopic techniques. The fused porphyrins 1 and 2 were used to... |
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| SubjectTerms | Chemistry colorimetric fused porphyrin reusability sensor toxic ions |
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| Title | Fused Nickel(II) Porphyrins—Sensing of Toxic Anions and Selected Metal Ions Through Supramolecular Interactions |
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