Influence of pH and oxygen-inhibited layer on fluoride release properties of fluoride sealant
Abstract Objectives This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant. Methods Forty-eight discs...
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| Published in: | Journal of dentistry Vol. 35; no. 4; pp. 275 - 281 |
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| Main Authors: | , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier Ltd
01-04-2007
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| Abstract | Abstract Objectives This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant. Methods Forty-eight discs (16-mm diameter × 1-mm thick) were made from FluroShield (<5 wt% NaF) and Helioseal F (<30 wt% fluorosilicate glass) sealants. For each sealant, 24 discs were cured through a Mylar® strip that covered the surface and the remaining 24 discs were cured in air allowing formation of the oxygen-inhibited surface. Each specimen in the 24-disc groups was stored individually in 25-mL vials, and divided into four six-vial groups to receive 10 mL of pH4–pH7 (designation of pH 4–7) lactate buffer solutions. The buffer solutions were replaced periodically up to 121 days. The cumulative fluoride release over time was used to determine the coefficients for short-term and long-term release. Results Two-way ANOVA showed that the mean coefficient values for either sealant were significantly influenced by the curing condition ( p < 0.0001) and pH ( p < 0.0001), except for short-term release from NaF sealant. The duration of short-term release was much longer for the fluorosilicate glass sealant. Conclusions Both pH and the source of fluoride source incorporated in the sealant play significant roles in fluoride release. |
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| AbstractList | Abstract Objectives This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant. Methods Forty-eight discs (16-mm diameter × 1-mm thick) were made from FluroShield (<5 wt% NaF) and Helioseal F (<30 wt% fluorosilicate glass) sealants. For each sealant, 24 discs were cured through a Mylar® strip that covered the surface and the remaining 24 discs were cured in air allowing formation of the oxygen-inhibited surface. Each specimen in the 24-disc groups was stored individually in 25-mL vials, and divided into four six-vial groups to receive 10 mL of pH4–pH7 (designation of pH 4–7) lactate buffer solutions. The buffer solutions were replaced periodically up to 121 days. The cumulative fluoride release over time was used to determine the coefficients for short-term and long-term release. Results Two-way ANOVA showed that the mean coefficient values for either sealant were significantly influenced by the curing condition ( p < 0.0001) and pH ( p < 0.0001), except for short-term release from NaF sealant. The duration of short-term release was much longer for the fluorosilicate glass sealant. Conclusions Both pH and the source of fluoride source incorporated in the sealant play significant roles in fluoride release. This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant. Forty-eight discs (16-mm diameter x 1-mm thick) were made from FluroShield (<5 wt% NaF) and Helioseal F (<30 wt% fluorosilicate glass) sealants. For each sealant, 24 discs were cured through a Mylar strip that covered the surface and the remaining 24 discs were cured in air allowing formation of the oxygen-inhibited surface. Each specimen in the 24-disc groups was stored individually in 25-mL vials, and divided into four six-vial groups to receive 10 mL of pH4-pH7 (designation of pH 4-7) lactate buffer solutions. The buffer solutions were replaced periodically up to 121 days. The cumulative fluoride release over time was used to determine the coefficients for short-term and long-term release. Two-way ANOVA showed that the mean coefficient values for either sealant were significantly influenced by the curing condition (p<0.0001) and pH (p<0.0001), except for short-term release from NaF sealant. The duration of short-term release was much longer for the fluorosilicate glass sealant. Both pH and the source of fluoride source incorporated in the sealant play significant roles in fluoride release. OBJECTIVESThis study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant.METHODSForty-eight discs (16-mm diameter x 1-mm thick) were made from FluroShield (<5 wt% NaF) and Helioseal F (<30 wt% fluorosilicate glass) sealants. For each sealant, 24 discs were cured through a Mylar strip that covered the surface and the remaining 24 discs were cured in air allowing formation of the oxygen-inhibited surface. Each specimen in the 24-disc groups was stored individually in 25-mL vials, and divided into four six-vial groups to receive 10 mL of pH4-pH7 (designation of pH 4-7) lactate buffer solutions. The buffer solutions were replaced periodically up to 121 days. The cumulative fluoride release over time was used to determine the coefficients for short-term and long-term release.RESULTSTwo-way ANOVA showed that the mean coefficient values for either sealant were significantly influenced by the curing condition (p<0.0001) and pH (p<0.0001), except for short-term release from NaF sealant. The duration of short-term release was much longer for the fluorosilicate glass sealant.CONCLUSIONSBoth pH and the source of fluoride source incorporated in the sealant play significant roles in fluoride release. This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant. Forty-eight discs (16-mm diameter×1-mm thick) were made from FluroShield (<5wt% NaF) and Helioseal F (<30wt% fluorosilicate glass) sealants. For each sealant, 24 discs were cured through a Mylar® strip that covered the surface and the remaining 24 discs were cured in air allowing formation of the oxygen-inhibited surface. Each specimen in the 24-disc groups was stored individually in 25-mL vials, and divided into four six-vial groups to receive 10mL of pH4-pH7 (designation of pH 4-7) lactate buffer solutions. The buffer solutions were replaced periodically up to 121 days. The cumulative fluoride release over time was used to determine the coefficients for short-term and long-term release. Two-way ANOVA showed that the mean coefficient values for either sealant were significantly influenced by the curing condition (p <0.0001) and pH (p <0.0001), except for short-term release from NaF sealant. The duration of short-term release was much longer for the fluorosilicate glass sealant. Both pH and the source of fluoride source incorporated in the sealant play significant roles in fluoride release. This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase significantly the initial fluoride release and long-term release rate from fluoride dental sealant. Forty-eight discs (16-mm diameter × 1-mm thick) were made from FluroShield (<5 wt% NaF) and Helioseal F (<30 wt% fluorosilicate glass) sealants. For each sealant, 24 discs were cured through a Mylar ® strip that covered the surface and the remaining 24 discs were cured in air allowing formation of the oxygen-inhibited surface. Each specimen in the 24-disc groups was stored individually in 25-mL vials, and divided into four six-vial groups to receive 10 mL of pH4–pH7 (designation of pH 4–7) lactate buffer solutions. The buffer solutions were replaced periodically up to 121 days. The cumulative fluoride release over time was used to determine the coefficients for short-term and long-term release. Two-way ANOVA showed that the mean coefficient values for either sealant were significantly influenced by the curing condition ( p < 0.0001) and pH ( p < 0.0001), except for short-term release from NaF sealant. The duration of short-term release was much longer for the fluorosilicate glass sealant. Both pH and the source of fluoride source incorporated in the sealant play significant roles in fluoride release. |
| Author | Shokry, T.E Anusavice, K.J Shen, C |
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| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/17118506$$D View this record in MEDLINE/PubMed |
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| Keywords | pH Oxygen-inhibition Sealant NaF Fluorosilicate glass Fluoride release |
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| Snippet | Abstract Objectives This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium... This study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would increase... OBJECTIVESThis study tested the hypothesis that the oxygen-inhibited layer on a light-cured methacrylate based resin and the pH of the storage medium would... |
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| SubjectTerms | Bisphenol A-Glycidyl Methacrylate - chemistry Cariostatic Agents - analysis Composite Resins - chemistry Curing Dental caries Dentistry Fluoride release Fluorides Fluorides - analysis Fluorides - chemistry Fluorosilicate glass Hydrogen-Ion Concentration NaF Oxygen Oxygen - chemistry Oxygen-inhibition Phase Transition Pit and Fissure Sealants - chemistry Polyurethanes - chemistry Sealant Sealing compounds Silicic Acid - chemistry Sodium Fluoride - chemistry Studies Surface Properties |
| Title | Influence of pH and oxygen-inhibited layer on fluoride release properties of fluoride sealant |
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