Polychromatic diffraction contrast tomography
This tutorial review introduces the use of polychromatic radiation for 3D grain mapping using X-ray diffraction contrast tomography. The objective is to produce a 3D map of the grain shapes and orientations within a bulk, millimeter-sized polycrystalline sample. The use of polychromatic radiation en...
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| Published in: | Materials characterization Vol. 97; pp. 1 - 10 |
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01-11-2014
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| Abstract | This tutorial review introduces the use of polychromatic radiation for 3D grain mapping using X-ray diffraction contrast tomography. The objective is to produce a 3D map of the grain shapes and orientations within a bulk, millimeter-sized polycrystalline sample. The use of polychromatic radiation enables the standard synchrotron X-ray technique to be applied in a wider range of contexts: 1) Using laboratory X-ray sources allows a much wider application of the diffraction contrast tomography technique. 2) Neutron sources allow large samples, or samples containing high Z elements to be studied. 3) Applied to synchrotron sources, smaller samples may be treated, or faster measurements may be possible. Challenges and particularities in the data acquisition and processing, and the limitations of the different variants, are discussed.
•We present a tutorial review of polychromatic diffraction contrast tomography techniques.•The use of polychromatic radiation allows the standard synchrotron DCT technique to be extended to a range of other sources.•The characteristics and limitations of all variants of the techniques are derived, discussed and compared.•Examples using laboratory X-ray and cold neutron radiation are presented.•Suggestions for the future development of these techniques are presented. |
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| AbstractList | This tutorial review introduces the use of polychromatic radiation for 3D grain mapping using X-ray diffraction contrast tomography. The objective is to produce a 3D map of the grain shapes and orientations within a bulk, millimeter-sized polycrystalline sample. The use of polychromatic radiation enables the standard synchrotron X-ray technique to be applied in a wider range of contexts: 1) Using laboratory X-ray sources allows a much wider application of the diffraction contrast tomography technique. 2) Neutron sources allow large samples, or samples containing high Z elements to be studied. 3) Applied to synchrotron sources, smaller samples may be treated, or faster measurements may be possible. Challenges and particularities in the data acquisition and processing, and the limitations of the different variants, are discussed. - Highlights: • We present a tutorial review of polychromatic diffraction contrast tomography techniques. • The use of polychromatic radiation allows the standard synchrotron DCT technique to be extended to a range of other sources. • The characteristics and limitations of all variants of the techniques are derived, discussed and compared. • Examples using laboratory X-ray and cold neutron radiation are presented. • Suggestions for the future development of these techniques are presented. This tutorial review introduces the use of polychromatic radiation for 3D grain mapping using X-ray diffraction contrast tomography. The objective is to produce a 3D map of the grain shapes and orientations within a bulk, millimeter-sized polycrystalline sample. The use of polychromatic radiation enables the standard synchrotron X-ray technique to be applied in a wider range of contexts: 1) Using laboratory X-ray sources allows a much wider application of the diffraction contrast tomography technique. 2) Neutron sources allow large samples, or samples containing high Z elements to be studied. 3) Applied to synchrotron sources, smaller samples may be treated, or faster measurements may be possible. Challenges and particularities in the data acquisition and processing, and the limitations of the different variants, are discussed. This tutorial review introduces the use of polychromatic radiation for 3D grain mapping using X-ray diffraction contrast tomography. The objective is to produce a 3D map of the grain shapes and orientations within a bulk, millimeter-sized polycrystalline sample. The use of polychromatic radiation enables the standard synchrotron X-ray technique to be applied in a wider range of contexts: 1) Using laboratory X-ray sources allows a much wider application of the diffraction contrast tomography technique. 2) Neutron sources allow large samples, or samples containing high Z elements to be studied. 3) Applied to synchrotron sources, smaller samples may be treated, or faster measurements may be possible. Challenges and particularities in the data acquisition and processing, and the limitations of the different variants, are discussed. •We present a tutorial review of polychromatic diffraction contrast tomography techniques.•The use of polychromatic radiation allows the standard synchrotron DCT technique to be extended to a range of other sources.•The characteristics and limitations of all variants of the techniques are derived, discussed and compared.•Examples using laboratory X-ray and cold neutron radiation are presented.•Suggestions for the future development of these techniques are presented. |
| Author | Ludwig, W. Adrien, J. King, A. Peetermans, S. Reischig, P. |
| Author_xml | – sequence: 1 givenname: A. surname: King fullname: King, A. email: king@synchrotron-soleil.fr organization: Synchrotron SOLEIL, Gif-sur-Yvette 91192, France – sequence: 2 givenname: P. surname: Reischig fullname: Reischig, P. organization: Xnovo Technology ApS, 4600 Køge, Denmark – sequence: 3 givenname: J. orcidid: 0000-0003-0341-3559 surname: Adrien fullname: Adrien, J. organization: MATEIS, INSA de Lyon, Villeurbanne 69621, France – sequence: 4 givenname: S. orcidid: 0000-0003-4206-4902 surname: Peetermans fullname: Peetermans, S. organization: Paul Scherrer Institut, CH-5232 Villigen, Switzerland – sequence: 5 givenname: W. surname: Ludwig fullname: Ludwig, W. organization: MATEIS, INSA de Lyon, Villeurbanne 69621, France |
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| Keywords | Diffraction contrast tomography Laboratory X-rays Neutron imaging Polychromatic radiation Polycrystalline characterization Imaging |
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| SubjectTerms | COLD NEUTRONS COMPARATIVE EVALUATIONS CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY Cross-disciplinary physics: materials science; rheology DATA ACQUISITION Diffraction Diffraction contrast tomography Exact sciences and technology Grains Laboratory X-rays MAPPING MATERIALS SCIENCE Mechanics Mechanics of materials Neutron imaging NEUTRON SOURCES Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics Polychromatic radiation Polycrystalline characterization POLYCRYSTALS Solidification SYNCHROTRON RADIATION SOURCES Synchrotrons Three dimensional TOMOGRAPHY X RADIATION X-RAY DIFFRACTION X-RAY SOURCES X-rays |
| Title | Polychromatic diffraction contrast tomography |
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