Highly birefringent vaterite microspheres: production, characterization and applications for optical micromanipulation
This paper reports on a simple synthesis and characterization of highly birefringent vaterite microspheres, which are composed of 20-30 nm sized nanocrystalls. Scanning electron microscopy shows a quite disordered assembly of nanocrystals within the microspheres. However, using optical tweezers, the...
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| Published in: | Optics express Vol. 17; no. 24; pp. 21944 - 21955 |
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| Main Authors: | , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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23-11-2009
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| Abstract | This paper reports on a simple synthesis and characterization of highly birefringent vaterite microspheres, which are composed of 20-30 nm sized nanocrystalls. Scanning electron microscopy shows a quite disordered assembly of nanocrystals within the microspheres. However, using optical tweezers, the effective birefringence of the microspheres was measured to be Deltan = 0.06, which compares to Deltan = 0.1 of vaterite single crystals. This suggests a very high orientation of the nanocrystals within the microspheres. A hyperbolic model of the direction of the optical axis throughout the vaterite spherulite best fits the experimental data. Results from polarized light microscopy further confirm the hyperbolic model. |
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| AbstractList | This paper reports on a simple synthesis and characterization of highly birefringent vaterite microspheres, which are composed of 20-30 nm sized nanocrystalls. Scanning electron microscopy shows a quite disordered assembly of nanocrystals within the microspheres. However, using optical tweezers, the effective birefringence of the microspheres was measured to be Deltan = 0.06, which compares to Deltan = 0.1 of vaterite single crystals. This suggests a very high orientation of the nanocrystals within the microspheres. A hyperbolic model of the direction of the optical axis throughout the vaterite spherulite best fits the experimental data. Results from polarized light microscopy further confirm the hyperbolic model. This paper reports on a simple synthesis and characterization of highly birefringent vaterite microspheres, which are composed of 20-30 nm sized nanocrystalls. Scanning electron microscopy shows a quite disordered assembly of nanocrystals within the microspheres. However, using optical tweezers, the effective birefringence of the microspheres was measured to Delta n = 0.06, which compares to Delta n = 0.1 of vaterite single crystals. This suggests a very high orientation of the nanocrystals within the microspheres. A hyperbolic model of the direction of the optical axis throughout the vaterite spherulite best fits the experimental data. Results from polarized light microscopy further confirm the hyperbolic model. (C) 2009 Optical Society of America |
| Author | Funk, Maren Vogel, Robert Parkin, Simon J Heckenberg, Norman R Nieminen, Timo A Rubinsztein-Dunlop, Halina Persson, Martin Loke, Vincent L Y |
| Author_xml | – sequence: 1 givenname: Simon J surname: Parkin fullname: Parkin, Simon J organization: University of Queensland, School of Mathematics and Physics, Queensland, Australia – sequence: 2 givenname: Robert surname: Vogel fullname: Vogel, Robert – sequence: 3 givenname: Martin surname: Persson fullname: Persson, Martin – sequence: 4 givenname: Maren surname: Funk fullname: Funk, Maren – sequence: 5 givenname: Vincent L Y surname: Loke fullname: Loke, Vincent L Y – sequence: 6 givenname: Timo A surname: Nieminen fullname: Nieminen, Timo A – sequence: 7 givenname: Norman R surname: Heckenberg fullname: Heckenberg, Norman R – sequence: 8 givenname: Halina surname: Rubinsztein-Dunlop fullname: Rubinsztein-Dunlop, Halina |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/19997439$$D View this record in MEDLINE/PubMed https://gup.ub.gu.se/publication/113933$$DView record from Swedish Publication Index |
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| SubjectTerms | Anisotropy AQUEOUS-SOLUTION Atom and Molecular Physics and Optics Atom- och molekylfysik och optik Birefringence CACO3 CALCIUM-CARBONATE CRYSTAL-GROWTH Equipment Design FORCE HYDROPHILIC BLOCK-COPOLYMERS KINETICS Lasers MICROPARTICLES Microscopy, Electron, Scanning - methods Microscopy, Electron, Transmission - methods Microspheres Nanoparticles Nanotechnology - methods Optics and Photonics Particle Size PRECIPITATION TWEEZERS X-Ray Diffraction |
| Title | Highly birefringent vaterite microspheres: production, characterization and applications for optical micromanipulation |
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