Selective adsorption of Ag (Ⅰ) from aqueous solutions using Chitosan/polydopamine@C@magnetic fly ash adsorbent beads
•A novel chitosan/polydopamine@C@magnetic fly ash adsorbent beads was synthesized.•The novel adsorbent was prepared by industrial waste magnetic fly ash beads and biopolymer chitosan.•The prepared adsorbent exhibited good selectivity for Ag (Ⅰ) in aqueous solutions.•The prepared adsorbent have stabl...
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| Published in: | Journal of hazardous materials Vol. 381; p. 120943 |
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| Main Authors: | , , , , |
| Format: | Journal Article |
| Language: | English |
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05-01-2020
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| Abstract | •A novel chitosan/polydopamine@C@magnetic fly ash adsorbent beads was synthesized.•The novel adsorbent was prepared by industrial waste magnetic fly ash beads and biopolymer chitosan.•The prepared adsorbent exhibited good selectivity for Ag (Ⅰ) in aqueous solutions.•The prepared adsorbent have stable magnetism in acidic environment.
[Display omitted]
A Chitosan/polydopamine@C@magnetic fly ash (CPCMFA) adsorbent bead was prepared for adsorption of Ag (Ⅰ) in aqueous solutions and exhibited good selectivity for Ag (Ⅰ) ion. To investigate its adsorption behaviors, equilibrium, kinetic and selective studies were conducted through batch experiments. Additionally, the influence of the pH value was also evaluated. In addition, the nature, composition, morphology, and magnetic property of the prepared adsorbent beads were characterized by Fourier transform-infrared (FT-IR) spectroscopy, X-ray diffraction (XRD) analysis, thermogravimetric-differential scanning calorimetry (TG-DSC) analysis, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and vibrating-sample magnetometry (VSM). The freeze-dry form of CPCMFA also exhibited high adsorption capacity and selectivity for Ag (Ⅰ), with a maximum adsorption capacity of 57.02 mg/g at pH 4 and 30 °C. The experimental data were well described by the Langmuir isotherm and elovich kinetic models. The thermodynamics parameters, ΔH = 10.653 kJ/mol, ΔS = 96.63 J/mol K and ΔG < 0, demonstrate that the adsorption of Ag (Ⅰ) on the freeze-dry form adsorbent is spontaneous and endothermic. Moreover, regeneration studies showed the high recyclability of the adsorbent, which after five cycles of use it was still able to adsorb 95.7% of the amount adsorbed by the fresh adsorbent. |
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| AbstractList | A Chitosan/polydopamine@C@magnetic fly ash (CPCMFA) adsorbent bead was prepared for adsorption of Ag (Ⅰ) in aqueous solutions and exhibited good selectivity for Ag (Ⅰ) ion. To investigate its adsorption behaviors, equilibrium, kinetic and selective studies were conducted through batch experiments. Additionally, the influence of the pH value was also evaluated. In addition, the nature, composition, morphology, and magnetic property of the prepared adsorbent beads were characterized by Fourier transform-infrared (FT-IR) spectroscopy, X-ray diffraction (XRD) analysis, thermogravimetric-differential scanning calorimetry (TG-DSC) analysis, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and vibrating-sample magnetometry (VSM). The freeze-dry form of CPCMFA also exhibited high adsorption capacity and selectivity for Ag (Ⅰ), with a maximum adsorption capacity of 57.02 mg/g at pH 4 and 30 °C. The experimental data were well described by the Langmuir isotherm and elovich kinetic models. The thermodynamics parameters, ΔH = 10.653 kJ/mol, ΔS = 96.63 J/mol K and ΔG < 0, demonstrate that the adsorption of Ag (Ⅰ) on the freeze-dry form adsorbent is spontaneous and endothermic. Moreover, regeneration studies showed the high recyclability of the adsorbent, which after five cycles of use it was still able to adsorb 95.7% of the amount adsorbed by the fresh adsorbent. •A novel chitosan/polydopamine@C@magnetic fly ash adsorbent beads was synthesized.•The novel adsorbent was prepared by industrial waste magnetic fly ash beads and biopolymer chitosan.•The prepared adsorbent exhibited good selectivity for Ag (Ⅰ) in aqueous solutions.•The prepared adsorbent have stable magnetism in acidic environment. [Display omitted] A Chitosan/polydopamine@C@magnetic fly ash (CPCMFA) adsorbent bead was prepared for adsorption of Ag (Ⅰ) in aqueous solutions and exhibited good selectivity for Ag (Ⅰ) ion. To investigate its adsorption behaviors, equilibrium, kinetic and selective studies were conducted through batch experiments. Additionally, the influence of the pH value was also evaluated. In addition, the nature, composition, morphology, and magnetic property of the prepared adsorbent beads were characterized by Fourier transform-infrared (FT-IR) spectroscopy, X-ray diffraction (XRD) analysis, thermogravimetric-differential scanning calorimetry (TG-DSC) analysis, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and vibrating-sample magnetometry (VSM). The freeze-dry form of CPCMFA also exhibited high adsorption capacity and selectivity for Ag (Ⅰ), with a maximum adsorption capacity of 57.02 mg/g at pH 4 and 30 °C. The experimental data were well described by the Langmuir isotherm and elovich kinetic models. The thermodynamics parameters, ΔH = 10.653 kJ/mol, ΔS = 96.63 J/mol K and ΔG < 0, demonstrate that the adsorption of Ag (Ⅰ) on the freeze-dry form adsorbent is spontaneous and endothermic. Moreover, regeneration studies showed the high recyclability of the adsorbent, which after five cycles of use it was still able to adsorb 95.7% of the amount adsorbed by the fresh adsorbent. |
| ArticleNumber | 120943 |
| Author | Zhang, Xiaomin Li, Yue Zhang, Liang Mu, Chaoqun Zhong, Lvling |
| Author_xml | – sequence: 1 givenname: Chaoqun surname: Mu fullname: Mu, Chaoqun organization: School of Chemistry and Chemical Engineering, Xi’an University of Architecture and Technology, Xi’an, Shaanxi, 710055, China – sequence: 2 givenname: Liang orcidid: 0000-0002-4056-9803 surname: Zhang fullname: Zhang, Liang email: zl98zl@hotmail.com organization: School of Chemistry and Chemical Engineering, Xi’an University of Architecture and Technology, Xi’an, Shaanxi, 710055, China – sequence: 3 givenname: Xiaomin surname: Zhang fullname: Zhang, Xiaomin email: xmzhangxauat@vip.163.com organization: College of Materials and Mineral Resources, Xi’an University of Architecture and Technology, Xi’an, Shaanxi, 710055, China – sequence: 4 givenname: Lvling surname: Zhong fullname: Zhong, Lvling organization: School of Chemistry and Chemical Engineering, Xi’an University of Architecture and Technology, Xi’an, Shaanxi, 710055, China – sequence: 5 givenname: Yue orcidid: 0000-0002-1202-4224 surname: Li fullname: Li, Yue organization: College of Materials and Mineral Resources, Xi’an University of Architecture and Technology, Xi’an, Shaanxi, 710055, China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31400716$$D View this record in MEDLINE/PubMed |
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| Keywords | Magnetic fly ash Adsorbent beads Chitosan Ag (Ⅰ) Selective adsorption |
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| Snippet | •A novel chitosan/polydopamine@C@magnetic fly ash adsorbent beads was synthesized.•The novel adsorbent was prepared by industrial waste magnetic fly ash beads... A Chitosan/polydopamine@C@magnetic fly ash (CPCMFA) adsorbent bead was prepared for adsorption of Ag (Ⅰ) in aqueous solutions and exhibited good selectivity... |
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| SubjectTerms | Adsorbent beads Ag (Ⅰ) Chitosan Magnetic fly ash Selective adsorption |
| Title | Selective adsorption of Ag (Ⅰ) from aqueous solutions using Chitosan/polydopamine@C@magnetic fly ash adsorbent beads |
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