Preparation of multi-functional magnetic–plasmonic nanocomposite for adsorption and detection of thiram using SERS
[Display omitted] •Multifunctional magnetic–plasmonic nanocomposite were fabricated via decorating Ag NPs on surface of porous Fe microsphere.•The porous Fe microspheres with controllable size were prepared through a simple and facile way.•The Fe@Ag were used for adsorption and detection of thiram b...
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| Published in: | Journal of hazardous materials Vol. 392; p. 122356 |
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| Main Authors: | , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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Elsevier B.V
15-06-2020
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| Abstract | [Display omitted]
•Multifunctional magnetic–plasmonic nanocomposite were fabricated via decorating Ag NPs on surface of porous Fe microsphere.•The porous Fe microspheres with controllable size were prepared through a simple and facile way.•The Fe@Ag were used for adsorption and detection of thiram by SERS.
Magnetic materials have been widely used for constructing substrate in surface enhanced Raman scattering (SERS) sensing due to the magnetic responsibility. Here, we reported a facile and effective approach to construct multi-functional SERS substrate based on assembling Ag nanoparticles (NPs) on porous Fe microspheres. The porous Fe microspheres were prepared through hydrogen reduction of Fe2O3 NPs with porous structure, in which the size and morphology of Fe could be well controlled. The surface of Fe was grafted with amino group, and then decorated with Ag NPs. The surface area and pore size of Fe microsphere were characterized by nitrogen adsorption and desorption. The Fe@Ag nanocomposite illustrated a good SERS activity. Furthermore, this substrate could be used for pesticide monitoring by portable Raman spectrometer. Especially, the porous Fe microsphere could adsorb analyte from target sample and the Fe@Ag could be concentrated by magnetic force to amplify the SERS signal for thiram detection. |
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| AbstractList | [Display omitted]
•Multifunctional magnetic–plasmonic nanocomposite were fabricated via decorating Ag NPs on surface of porous Fe microsphere.•The porous Fe microspheres with controllable size were prepared through a simple and facile way.•The Fe@Ag were used for adsorption and detection of thiram by SERS.
Magnetic materials have been widely used for constructing substrate in surface enhanced Raman scattering (SERS) sensing due to the magnetic responsibility. Here, we reported a facile and effective approach to construct multi-functional SERS substrate based on assembling Ag nanoparticles (NPs) on porous Fe microspheres. The porous Fe microspheres were prepared through hydrogen reduction of Fe2O3 NPs with porous structure, in which the size and morphology of Fe could be well controlled. The surface of Fe was grafted with amino group, and then decorated with Ag NPs. The surface area and pore size of Fe microsphere were characterized by nitrogen adsorption and desorption. The Fe@Ag nanocomposite illustrated a good SERS activity. Furthermore, this substrate could be used for pesticide monitoring by portable Raman spectrometer. Especially, the porous Fe microsphere could adsorb analyte from target sample and the Fe@Ag could be concentrated by magnetic force to amplify the SERS signal for thiram detection. Magnetic materials have been widely used for constructing substrate in surface enhanced Raman scattering (SERS) sensing due to the magnetic responsibility. Here, we reported a facile and effective approach to construct multi-functional SERS substrate based on assembling Ag nanoparticles (NPs) on porous Fe microspheres. The porous Fe microspheres were prepared through hydrogen reduction of Fe O NPs with porous structure, in which the size and morphology of Fe could be well controlled. The surface of Fe was grafted with amino group, and then decorated with Ag NPs. The surface area and pore size of Fe microsphere were characterized by nitrogen adsorption and desorption. The Fe@Ag nanocomposite illustrated a good SERS activity. Furthermore, this substrate could be used for pesticide monitoring by portable Raman spectrometer. Especially, the porous Fe microsphere could adsorb analyte from target sample and the Fe@Ag could be concentrated by magnetic force to amplify the SERS signal for thiram detection. |
| ArticleNumber | 122356 |
| Author | Yang, Zhanxu Fan, Qinzhen Wang, Ying Kong, Xianming Liu, Xinquan Tong, Xiaoxue Fu, Ziwei Shen, Zhengdong Hao, Shaoxian |
| Author_xml | – sequence: 1 givenname: Ziwei surname: Fu fullname: Fu, Ziwei organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 2 givenname: Zhengdong surname: Shen fullname: Shen, Zhengdong organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 3 givenname: Qinzhen surname: Fan fullname: Fan, Qinzhen organization: College of Chemical Engineering, Guangdong University of Petrochemical Technology, Maoming 525000, PR China – sequence: 4 givenname: Shaoxian surname: Hao fullname: Hao, Shaoxian organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 5 givenname: Ying surname: Wang fullname: Wang, Ying organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 6 givenname: Xinquan surname: Liu fullname: Liu, Xinquan organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 7 givenname: Xiaoxue surname: Tong fullname: Tong, Xiaoxue organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 8 givenname: Xianming orcidid: 0000-0001-7622-7744 surname: Kong fullname: Kong, Xianming email: xmkong@lnpu.edu organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China – sequence: 9 givenname: Zhanxu surname: Yang fullname: Yang, Zhanxu email: yangzhanxu@lnpu.edu.cn organization: College of Chemistry, Chemical Engineering and Environment Engineering, Liaoning Shihua University, Fushun, Liaoning 113001, PR China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/32109795$$D View this record in MEDLINE/PubMed |
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| Copyright | 2020 Elsevier B.V. Copyright © 2020 Elsevier B.V. All rights reserved. |
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| Keywords | Porous Fe micro-sphere Thiram Multi-Functional SERS |
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•Multifunctional magnetic–plasmonic nanocomposite were fabricated via decorating Ag NPs on surface of porous Fe microsphere.•The porous Fe... Magnetic materials have been widely used for constructing substrate in surface enhanced Raman scattering (SERS) sensing due to the magnetic responsibility.... |
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| Title | Preparation of multi-functional magnetic–plasmonic nanocomposite for adsorption and detection of thiram using SERS |
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