Microstructural characterization of autogenous laser welds on 316L stainless steel using EBSD and EDS

• Published in: Journal of microscopy (Oxford) Vol. 217; no. 2; pp. 167 - 173
• Main Authors: KELL, J., TYRER, J. R., HIGGINSON, R. L., THOMSON, R. C.
• Format: Journal Article
• Language: English
• Published: Oxford, UK Blackwell Science Ltd 01-02-2005
• Subjects: 316L stainless steel; Crystallography; electron backscatter diffraction; energy dispersive spectroscopy; laser welding; Lasers; Metallurgy; Microscopy, Electron, Scanning; microstructure; Stainless Steel - chemistry; Welding
• ISSN: 0022-2720; 1365-2818
• DOI: 10.1111/j.1365-2818.2005.01447.x

Summary
This research is concerned with autogenous welding of 316L stainless steel and the microstructure generated by such a process. Autogenous welding does not require a filler material and in this case relies on an initial shallow melt phase to maintain a conduction limited weld. Essentially, a high power laser beam traverses the substrate, with the beam shaped by conventional optics, which produces a Gaussian irradiance distribution; or with a diffractive optical element, used to produce a uniform irradiance distribution.
Initial results have shown that due to the nature of the heating cycle, complex microstructures are developed. These fine, complicated microstructures cannot be satisfactorily resolved and quantified using standard optical microscopy techniques. Electron backscatter diffraction (EBSD) and energy dispersive spectroscopy (EDS) have been carried out on a number of different microstructures prepared using a range of welding parameters. It is demonstrated that the simultaneous determination of the chemistry and crystallography is a very useful tool for rapid identification of the different phases formed on solidification as a consequence of varying welding procedures.