Synthesis of Platinum Catalysts over Thick Slurries of Oxide Supports by Strong Electrostatic Adsorption

Synthesis of Platinum Catalysts over Thick Slurries of Oxide Supports by Strong Electrostatic Adsorption

Platinum uptake by strong electrostatic adsorption on alumina, silica, and titania supports was studied at different slurry thicknesses (or surface loadings). For the anionic platinum chloride precursor, a high counterion concentration at high surface loadings hindered adsorption on the high point o...

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Published in:ChemCatChem Vol. 7; no. 21; pp. 3460 - 3463
Main Authors: Samad, Jadid E., Hoenig, Sean, Regalbuto, John R.
Format: Journal Article
Language:English
Published: Weinheim Blackwell Publishing Ltd 01-11-2015
Wiley Subscription Services, Inc
Subjects:
Adsorption
electrostatic adsorption
ionic strength
Platinum
slurries
supported catalysts
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Abstract Platinum uptake by strong electrostatic adsorption on alumina, silica, and titania supports was studied at different slurry thicknesses (or surface loadings). For the anionic platinum chloride precursor, a high counterion concentration at high surface loadings hindered adsorption on the high point of zero charge alumina support, as predicted by the revised physical adsorption model. Owing to this adsorption retardation in thicker slurries, a highly dispersed Pt/Al2O3 catalyst could only be prepared with a lower weight fraction of Pt than that in thin slurries. However, for cationic platinum tetraamine complexes, the effect of counterions in retarding the adsorption at high surface loadings was unexpectedly diminished. As a result, it was possible to synthesize highly dispersed Pt/SiO2 even at a maximum slurry thickness (incipient wetness) without having to sacrifice the Pt loading. Conveniently Lost at SEA: Platinum uptake by strong electrostatic adsorption (SEA) on alumina, silica, and titania supports is studied at different slurry thicknesses. For cationic platinum tetraamine complexes, the effect of counterions in retarding adsorption at high surface loadings is diminished, and as such, highly dispersed Pt/SiO2 at a maximum slurry thickness (incipient wetness) without sacrifice to the Pt loading is possible.
AbstractList Platinum uptake by strong electrostatic adsorption on alumina, silica, and titania supports was studied at different slurry thicknesses (or surface loadings). For the anionic platinum chloride precursor, a high counterion concentration at high surface loadings hindered adsorption on the high point of zero charge alumina support, as predicted by the revised physical adsorption model. Owing to this adsorption retardation in thicker slurries, a highly dispersed Pt/Al2O3 catalyst could only be prepared with a lower weight fraction of Pt than that in thin slurries. However, for cationic platinum tetraamine complexes, the effect of counterions in retarding the adsorption at high surface loadings was unexpectedly diminished. As a result, it was possible to synthesize highly dispersed Pt/SiO2 even at a maximum slurry thickness (incipient wetness) without having to sacrifice the Pt loading.
Platinum uptake by strong electrostatic adsorption on alumina, silica, and titania supports was studied at different slurry thicknesses (or surface loadings). For the anionic platinum chloride precursor, a high counterion concentration at high surface loadings hindered adsorption on the high point of zero charge alumina support, as predicted by the revised physical adsorption model. Owing to this adsorption retardation in thicker slurries, a highly dispersed Pt/Al2O3 catalyst could only be prepared with a lower weight fraction of Pt than that in thin slurries. However, for cationic platinum tetraamine complexes, the effect of counterions in retarding the adsorption at high surface loadings was unexpectedly diminished. As a result, it was possible to synthesize highly dispersed Pt/SiO2 even at a maximum slurry thickness (incipient wetness) without having to sacrifice the Pt loading. Conveniently Lost at SEA: Platinum uptake by strong electrostatic adsorption (SEA) on alumina, silica, and titania supports is studied at different slurry thicknesses. For cationic platinum tetraamine complexes, the effect of counterions in retarding adsorption at high surface loadings is diminished, and as such, highly dispersed Pt/SiO2 at a maximum slurry thickness (incipient wetness) without sacrifice to the Pt loading is possible.
Platinum uptake by strong electrostatic adsorption on alumina, silica, and titania supports was studied at different slurry thicknesses (or surface loadings). For the anionic platinum chloride precursor, a high counterion concentration at high surface loadings hindered adsorption on the high point of zero charge alumina support, as predicted by the revised physical adsorption model. Owing to this adsorption retardation in thicker slurries, a highly dispersed Pt/Al 2 O 3 catalyst could only be prepared with a lower weight fraction of Pt than that in thin slurries. However, for cationic platinum tetraamine complexes, the effect of counterions in retarding the adsorption at high surface loadings was unexpectedly diminished. As a result, it was possible to synthesize highly dispersed Pt/SiO 2 even at a maximum slurry thickness (incipient wetness) without having to sacrifice the Pt loading.
Author Samad, Jadid E.
Regalbuto, John R.
Hoenig, Sean
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  givenname: Sean
  surname: Hoenig
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  surname: Regalbuto
  fullname: Regalbuto, John R.
  email: regalbuj@cec.sc.edu
  organization: Department of Chemical Engineering, University of South Carolina, 301 Main Street, SC, 29208, Columbia, USA
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Snippet Platinum uptake by strong electrostatic adsorption on alumina, silica, and titania supports was studied at different slurry thicknesses (or surface loadings)....
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SubjectTerms Adsorption
electrostatic adsorption
ionic strength
Platinum
slurries
supported catalysts
Title Synthesis of Platinum Catalysts over Thick Slurries of Oxide Supports by Strong Electrostatic Adsorption
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