Structural development of poly(ethylene terephthalate) during uniaxial stretching above the glass-transition temperature: Study of the statistical influence of the stretching variables
In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass-transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the...
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| Published in: | Journal of applied polymer science Vol. 120; no. 3; pp. 1253 - 1265 |
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| Format: | Journal Article |
| Language: | English |
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| Abstract | In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass-transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the structural development. Amorphous PET was submitted to a stretching program with variations in the stretching temperature (Tst), stretching rate ( $\dot {\varepsilon}_{st}$), and stretching ratio (λst). Stretched samples were rapidly quenched and characterized by wide-angle X-ray scattering, optical birefringence, and differential scanning calorimetry. The relevance and influence of the stretching variables on the obtained parameters (phase fraction, phase orientation, and thermal parameters) were analyzed. The strain-induced crystallinity was controlled by Tst, λst, and the interactions between them. Mesophase development was not dependant on Tst but on the interactions between $\dot {\varepsilon}_{st}$ and λst. The molecular orientation was proportionally dependent on Tst, λst, and their interactions. |
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| AbstractList | In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass-transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the structural development. Amorphous PET was submitted to a stretching program with variations in the stretching temperature (Tst), stretching rate ( $\dot {\varepsilon}_{st}$), and stretching ratio (λst). Stretched samples were rapidly quenched and characterized by wide-angle X-ray scattering, optical birefringence, and differential scanning calorimetry. The relevance and influence of the stretching variables on the obtained parameters (phase fraction, phase orientation, and thermal parameters) were analyzed. The strain-induced crystallinity was controlled by Tst, λst, and the interactions between them. Mesophase development was not dependant on Tst but on the interactions between $\dot {\varepsilon}_{st}$ and λst. The molecular orientation was proportionally dependent on Tst, λst, and their interactions. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2011 [PUBLICATION ABSTRACT] In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass‐transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the structural development. Amorphous PET was submitted to a stretching program with variations in the stretching temperature ( T st ), stretching rate ( $\dot {\varepsilon}_{st}$ ), and stretching ratio (λ st ). Stretched samples were rapidly quenched and characterized by wide‐angle X‐ray scattering, optical birefringence, and differential scanning calorimetry. The relevance and influence of the stretching variables on the obtained parameters (phase fraction, phase orientation, and thermal parameters) were analyzed. The strain‐induced crystallinity was controlled by T st , λ st , and the interactions between them. Mesophase development was not dependant on T st but on the interactions between $\dot {\varepsilon}_{st}$ and λ st . The molecular orientation was proportionally dependent on T st , λ st , and their interactions. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2011 In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass-transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the structural development. Amorphous PET was submitted to a stretching program with variations in the stretching temperature (Tst), stretching rate ( ), and stretching ratio ( lambda st). Stretched samples were rapidly quenched and characterized by wide-angle X-ray scattering, optical birefringence, and differential scanning calorimetry. The relevance and influence of the stretching variables on the obtained parameters (phase fraction, phase orientation, and thermal parameters) were analyzed. The strain-induced crystallinity was controlled by Tst, lambda st, and the interactions between them. Mesophase development was not dependant on Tst but on the interactions between and lambda st. The molecular orientation was proportionally dependent on Tst, lambda st, and their interactions. [copy 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2011 In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass‐transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the structural development. Amorphous PET was submitted to a stretching program with variations in the stretching temperature (Tst), stretching rate ( $\dot {\varepsilon}_{st}$), and stretching ratio (λst). Stretched samples were rapidly quenched and characterized by wide‐angle X‐ray scattering, optical birefringence, and differential scanning calorimetry. The relevance and influence of the stretching variables on the obtained parameters (phase fraction, phase orientation, and thermal parameters) were analyzed. The strain‐induced crystallinity was controlled by Tst, λst, and the interactions between them. Mesophase development was not dependant on Tst but on the interactions between $\dot {\varepsilon}_{st}$ and λst. The molecular orientation was proportionally dependent on Tst, λst, and their interactions. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2011 In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the glass-transition temperature; this followed a statistical design of experiment approach to determine the influence of the stretching variables on the structural development. Amorphous PET was submitted to a stretching program with variations in the stretching temperature (Tst), stretching rate ( $\dot {\varepsilon}_{st}$), and stretching ratio (λst). Stretched samples were rapidly quenched and characterized by wide-angle X-ray scattering, optical birefringence, and differential scanning calorimetry. The relevance and influence of the stretching variables on the obtained parameters (phase fraction, phase orientation, and thermal parameters) were analyzed. The strain-induced crystallinity was controlled by Tst, λst, and the interactions between them. Mesophase development was not dependant on Tst but on the interactions between $\dot {\varepsilon}_{st}$ and λst. The molecular orientation was proportionally dependent on Tst, λst, and their interactions. |
| Author | Martins, Carla I. Viana, Júlio C. Todorov, Lyudmil V. |
| Author_xml | – sequence: 1 fullname: Todorov, Lyudmil V – sequence: 2 fullname: Martins, Carla I – sequence: 3 fullname: Viana, Júlio C |
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| Keywords | Ethylene terephthalate polymer differential scanning calorimetry (DSC) Ester polymer Temperature effect Crystallinity Experimental study Glass transition temperature WAXS Uniaxial drawing Thermal properties Structure processing relationship Hot drawing Molecular orientation Experimental design drawing X ray scattering orientation polyesters |
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| Snippet | In this article, we present an investigation of the structural development of poly(ethylene terephthalate) (PET) during uniaxial stretching above the... |
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| SubjectTerms | Applied sciences Birefringence Crystallinity Design of experiments Differential scanning calorimetry differential scanning calorimetry (DSC) Exact sciences and technology Glass transition temperature Materials science Organic polymers Orientation orientation polyesters Physicochemistry of polymers Polyethylene terephthalates Polymers Properties and characterization Stretching Structure, morphology and analysis Terephthalate WAXS |
| Title | Structural development of poly(ethylene terephthalate) during uniaxial stretching above the glass-transition temperature: Study of the statistical influence of the stretching variables |
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