Microwave-assisted synthesis of barium molybdate by a citrate complex method and oriented aggregation

Microwave-assisted synthesis of barium molybdate by a citrate complex method and oriented aggregation

BaMoO 4 powders, which have scheelite type structure, were successfully synthesized at low temperatures by a modified citrate complex method assisted by microwave irradiation. The citrate complex precursors were heat-treated at temperatures from 300 to 500 °C for 3 h. Crystallization of the BaMoO 4...

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Published in:Materials research bulletin Vol. 40; no. 9; pp. 1468 - 1476
Main Authors: Ryu, Jeong Ho, Yoon, Jong-Won, Lim, Chang Sung, Shim, Kwang Bo
Format: Journal Article
Language:English
Published: United States Elsevier Ltd 01-09-2005
Subjects:
A. Ceramics
AGGLOMERATION
ANISOTROPY
B. Chemical synthesis
BARIUM
C. Electron microscopy
CERAMICS
CHEMICAL PREPARATION
CITRATES
COMPLEXES
CRYSTAL GROWTH
CRYSTALLIZATION
D. Luminescence
ELECTRON MICROSCOPY
HEAT TREATMENTS
IRRADIATION
MATERIALS SCIENCE
MICROWAVE RADIATION
MOLYBDATES
MORPHOLOGY
PHOTOLUMINESCENCE
B. Chemical synthesis
A. Ceramics
C. Electron microscopy
D. Luminescence
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Abstract BaMoO 4 powders, which have scheelite type structure, were successfully synthesized at low temperatures by a modified citrate complex method assisted by microwave irradiation. The citrate complex precursors were heat-treated at temperatures from 300 to 500 °C for 3 h. Crystallization of the BaMoO 4 powders were detected at 350 °C, and completed at a temperature of 400 °C. TEM image of the BaMoO 4 product obtained above 400 °C revealed spindle-rods-like or flake-like morphology. The anisotropic growth habit of BaMoO 4 leads to the oriented aggregation, which is attributed to the high chemical potentials of the intrinsic structure of BaMoO 4. The BaMoO 4 powder prepared at 500 °C showed the strongest photoluminescent intensity.
AbstractList BaMoO{sub 4} powders, which have scheelite type structure, were successfully synthesized at low temperatures by a modified citrate complex method assisted by microwave irradiation. The citrate complex precursors were heat-treated at temperatures from 300 to 500 deg. C for 3 h. Crystallization of the BaMoO{sub 4} powders were detected at 350 deg. C, and completed at a temperature of 400 deg. C. TEM image of the BaMoO{sub 4} product obtained above 400 deg. C revealed spindle-rods-like or flake-like morphology. The anisotropic growth habit of BaMoO{sub 4} leads to the oriented aggregation, which is attributed to the high chemical potentials of the intrinsic structure of BaMoO{sub 4}. The BaMoO{sub 4} powder prepared at 500 deg. C showed the strongest photoluminescent intensity.
BaMoO 4 powders, which have scheelite type structure, were successfully synthesized at low temperatures by a modified citrate complex method assisted by microwave irradiation. The citrate complex precursors were heat-treated at temperatures from 300 to 500 °C for 3 h. Crystallization of the BaMoO 4 powders were detected at 350 °C, and completed at a temperature of 400 °C. TEM image of the BaMoO 4 product obtained above 400 °C revealed spindle-rods-like or flake-like morphology. The anisotropic growth habit of BaMoO 4 leads to the oriented aggregation, which is attributed to the high chemical potentials of the intrinsic structure of BaMoO 4. The BaMoO 4 powder prepared at 500 °C showed the strongest photoluminescent intensity.
Author Ryu, Jeong Ho
Shim, Kwang Bo
Yoon, Jong-Won
Lim, Chang Sung
Author_xml – sequence: 1
  givenname: Jeong Ho
  surname: Ryu
  fullname: Ryu, Jeong Ho
  email: jimihen@ihanyang.ac.kr
  organization: Department of Ceramic Engineering, CPRC, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791, Korea
– sequence: 2
  givenname: Jong-Won
  surname: Yoon
  fullname: Yoon, Jong-Won
  organization: Department of Ceramic Engineering, CPRC, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791, Korea
– sequence: 3
  givenname: Chang Sung
  surname: Lim
  fullname: Lim, Chang Sung
  organization: Department of Adv. Mat. Sci. & Eng., CPRC, Hanseo University, Seosan 356-706, Korea
– sequence: 4
  givenname: Kwang Bo
  surname: Shim
  fullname: Shim, Kwang Bo
  organization: Department of Ceramic Engineering, CPRC, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791, Korea
BackLink https://www.osti.gov/biblio/20891584$$D View this record in Osti.gov
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Snippet BaMoO 4 powders, which have scheelite type structure, were successfully synthesized at low temperatures by a modified citrate complex method assisted by...
BaMoO{sub 4} powders, which have scheelite type structure, were successfully synthesized at low temperatures by a modified citrate complex method assisted by...
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SubjectTerms A. Ceramics
AGGLOMERATION
ANISOTROPY
B. Chemical synthesis
BARIUM
C. Electron microscopy
CERAMICS
CHEMICAL PREPARATION
CITRATES
COMPLEXES
CRYSTAL GROWTH
CRYSTALLIZATION
D. Luminescence
ELECTRON MICROSCOPY
HEAT TREATMENTS
IRRADIATION
MATERIALS SCIENCE
MICROWAVE RADIATION
MOLYBDATES
MORPHOLOGY
PHOTOLUMINESCENCE
Title Microwave-assisted synthesis of barium molybdate by a citrate complex method and oriented aggregation
URI https://dx.doi.org/10.1016/j.materresbull.2005.04.032
https://www.osti.gov/biblio/20891584
Volume 40
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