Custom particle morphology in energetic nanocomposites prepared by arrested reactive milling in immiscible liquids

Custom particle morphology in energetic nanocomposites prepared by arrested reactive milling in immiscible liquids

The effect of polar and nonpolar liquid process control agents (PCA) on properties of metal rich Al/CuO thermites prepared by Arrested Reactive Milling was studied. Acetonitrile and hexane, and their mixtures were used as PCA. Milling in nonpolar hexane results in fully dense, micron-sized composite...

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Published in:Powder technology Vol. 359; pp. 238 - 246
Main Authors: Mursalat, Mehnaz, Schoenitz, Mirko, Dreizin, Edward L.
Format: Journal Article
Language:English
Published: Lausanne Elsevier B.V 01-01-2020
Elsevier BV
Subjects:
Acetonitrile
Aluminum
Arrested reactive milling
Colloidosomes
Emulsions
Immiscible liquids
Inclusions
Liquids
Miscibility
Morphology
Nanocomposites
Oxidation
Particulate composites
Particulates
Process control
Process control agents
Reaction kinetics
Reactive composites
Thermites
Process control agents
Arrested reactive milling
Immiscible liquids
Reactive composites
Emulsions
Colloidosomes
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Abstract The effect of polar and nonpolar liquid process control agents (PCA) on properties of metal rich Al/CuO thermites prepared by Arrested Reactive Milling was studied. Acetonitrile and hexane, and their mixtures were used as PCA. Milling in nonpolar hexane results in fully dense, micron-sized composite particles of 100nm-scale CuO inclusions in an Al matrix. Using polar acetonitrile results in a mixture of nano-sized, largely unagglomerated Al and CuO particles. Porous composites, agglomerated to different degrees, formed in hexane-acetonitrile mixtures. In particular, micron-sized porous spherical composite particles formed in a mixture with 25% acetonitrile. Such spherical composites may result from interaction of suspended powder particles with stressed droplets of a Pickering emulsion forming when immiscible liquids serve as PCA. Despite dramatic changes in the powder morphology, all composites were reactive. Systematic differences, discussed in the text, were observed in their ignition temperatures and oxidation kinetics. [Display omitted] •Energetic composite materials prepared by arrested reactive milling.•Novel use of immiscible solvents as process control agents.•Resulting emulsion determine properties of produced composite particles.
AbstractList The effect of polar and nonpolar liquid process control agents (PCA) on properties of metal rich Al/CuO thermites prepared by Arrested Reactive Milling was studied. Acetonitrile and hexane, and their mixtures were used as PCA. Milling in nonpolar hexane results in fully dense, micron-sized composite particles of 100 nm-scale CuO inclusions in an Al matrix. Using polar acetonitrile results in a mixture of nano-sized, largely unagglomerated Al and CuO particles. Porous composites, agglomerated to different degrees, formed in hexane-acetonitrile mixtures. In particular, micron-sized porous spherical composite particles formed in a mixture with 25% acetonitrile. Such spherical composites may result from interaction of suspended powder particles with stressed droplets of a Pickering emulsion forming when immiscible liquids serve as PCA. Despite dramatic changes in the powder morphology, all composites were reactive. Systematic differences, discussed in the text, were observed in their ignition temperatures and oxidation kinetics.
The effect of polar and nonpolar liquid process control agents (PCA) on properties of metal rich Al/CuO thermites prepared by Arrested Reactive Milling was studied. Acetonitrile and hexane, and their mixtures were used as PCA. Milling in nonpolar hexane results in fully dense, micron-sized composite particles of 100nm-scale CuO inclusions in an Al matrix. Using polar acetonitrile results in a mixture of nano-sized, largely unagglomerated Al and CuO particles. Porous composites, agglomerated to different degrees, formed in hexane-acetonitrile mixtures. In particular, micron-sized porous spherical composite particles formed in a mixture with 25% acetonitrile. Such spherical composites may result from interaction of suspended powder particles with stressed droplets of a Pickering emulsion forming when immiscible liquids serve as PCA. Despite dramatic changes in the powder morphology, all composites were reactive. Systematic differences, discussed in the text, were observed in their ignition temperatures and oxidation kinetics. [Display omitted] •Energetic composite materials prepared by arrested reactive milling.•Novel use of immiscible solvents as process control agents.•Resulting emulsion determine properties of produced composite particles.
Author Schoenitz, Mirko
Mursalat, Mehnaz
Dreizin, Edward L.
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  givenname: Mirko
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  givenname: Edward L.
  surname: Dreizin
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  organization: Tomsk State University, Tomsk 634050, Russia
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Keywords Process control agents
Arrested reactive milling
Immiscible liquids
Reactive composites
Emulsions
Colloidosomes
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Snippet The effect of polar and nonpolar liquid process control agents (PCA) on properties of metal rich Al/CuO thermites prepared by Arrested Reactive Milling was...
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SubjectTerms Acetonitrile
Aluminum
Arrested reactive milling
Colloidosomes
Emulsions
Immiscible liquids
Inclusions
Liquids
Miscibility
Morphology
Nanocomposites
Oxidation
Particulate composites
Particulates
Process control
Process control agents
Reaction kinetics
Reactive composites
Thermites
Title Custom particle morphology in energetic nanocomposites prepared by arrested reactive milling in immiscible liquids
URI https://dx.doi.org/10.1016/j.powtec.2019.10.006
https://www.proquest.com/docview/2361952259
Volume 359
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