Effect of specimen gripping device, geometry and fixation method on microtensile bond strength, failure mode and stress distribution: Laboratory and finite element analyses

• Published in: Dental materials Vol. 28; no. 5; pp. e50 - e62
• Main Authors: Raposo, Luís H.A, Armstrong, Steven R, Maia, Rodrigo R, Qian, Fang, Geraldeli, Saulo, Soares, Carlos J
• Format: Journal Article
• Language: English
• Published: England Elsevier Ltd 01-05-2012
• Subjects: Acid Etching, Dental - methods; Adhesives - chemistry; Advanced Basic Science; Bond strength; Composite Resins - chemistry; Cyanoacrylates - chemistry; Dental Bonding; Dental Cements - chemistry; Dental Materials - chemistry; Dental Stress Analysis - instrumentation; Dentin - ultrastructure; Dentistry; Energy dispersive X-ray spectroscopy; Equipment Design; Failure mode; Finite Element Analysis; Finite elements; Humans; Hydrogen-Ion Concentration; Imaging, Three-Dimensional - methods; Materials Testing - instrumentation; Methacrylates - chemistry; Microscopy, Electron, Scanning; Microtensile; Polymethyl Methacrylate - chemistry; Saliva, Artificial - chemistry; Scanning electron microscopy; Spectrometry, X-Ray Emission; Stress, Mechanical; Surface Properties; Temperature; Tensile Strength; Testing parameters; Time Factors; Failure mode; Finite elements; Scanning electron microscopy; Microtensile; Bond strength; Energy dispersive X-ray spectroscopy; Testing parameters
• ISSN: 0109-5641; 1879-0097
• DOI: 10.1016/j.dental.2012.02.010

Abstract Objectives Innumerous modifications have been proposed for the microtensile test since its introduction; however, testing parameters are not often well described and wide variations in bond strength are commonly reported. The aim of this study was to evaluate the effect of the test specimen's gripping device, specimen geometry and fixation method on microtensile bond strength, failure mode, and stress distribution when using an etch-and-rinse 2-step adhesive system bonded to human dentin. Methods Resin-based composite bonded to occlusal dentin from 21 human molars was used to fabricate dumbbell- and stick-shaped test specimens which were divided into three groups: Di – dumbbell-specimens placed in a Dircks device; GeS – stick-specimens gripped in a Geraldeli's device with Superglue; GeZ – stick-specimens gripped in a Geraldeli's device with Zapit. Specimens were tested to failure in tensile mode and the failure mode was examined under stereomicroscopy and fracture initiation sites were verified by scanning electron microscopy and energy dispersive X-ray spectroscopy. Three-dimensional models of each device/specimen were created and finite element calculations were performed. Results The effect of the gripping devices on the bond strength was not significant, unless the bond test areas were normalized. The failure mode was influenced by the type of device. Dircks device was less sensitive to human error than Geraldeli's, and produced a more uniform stress distribution at the dumbbell specimen adhesive layer than did the Geraldeli's device at the stick layer. Significance Microtensile testing parameters can directly influence the results and consequently inter-study comparisons.