Doping nanoparticles using pulsed laser ablation in a liquid containing the doping agent
While doping of semiconductors or oxides is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. In this paper, we show that pulsed laser ablation of an undoped solid target in an aqueous solution contain...
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| Published in: | Nanoscale advances Vol. 1; no. 1; pp. 3963 - 3972 |
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| Main Authors: | , , , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
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08-10-2019
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| Abstract | While doping of semiconductors or oxides is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. In this paper, we show that pulsed laser ablation of an undoped solid target in an aqueous solution containing activator ions offers a new way to synthesise doped-nanoparticles. The doping efficiency is evaluated for laser ablation of an undoped Gd
2
O
3
target in aqueous solutions of EuCl
3
with molar concentration from 10
−5
mol L
−1
to 10
−3
mol L
−1
. Thanks to luminescence experiments, we show that the europium ions penetrate the core of the synthesised monoclinic Gd
2
O
3
nanoparticles. We also show that the concentration of the activators in the nanoparticles is proportional to the initial concentration in europium ions in the aqueous solution, and a doping of about 1% ([Eu]/[Gd] atomic ratio) is reached. On the one hand, this work could open new ways for the synthesis of doped nanomaterials. On the other hand, it also raises the question of undesired penetration of impurities in laser-generated nanoparticles in liquids.
While doping is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. We suggest a new way to dope nanoparticles using laser ablation in liquids. |
|---|---|
| AbstractList | While doping of semiconductors or oxides is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. In this paper, we show that pulsed laser ablation of an undoped solid target in an aqueous solution containing activator ions offers a new way to synthesise doped-nanoparticles. The doping efficiency is evaluated for laser ablation of an undoped Gd
2
O
3
target in aqueous solutions of EuCl
3
with molar concentration from 10
−5
mol L
−1
to 10
−3
mol L
−1
. Thanks to luminescence experiments, we show that the europium ions penetrate the core of the synthesised monoclinic Gd
2
O
3
nanoparticles. We also show that the concentration of the activators in the nanoparticles is proportional to the initial concentration in europium ions in the aqueous solution, and a doping of about 1% ([Eu]/[Gd] atomic ratio) is reached. On the one hand, this work could open new ways for the synthesis of doped nanomaterials. On the other hand, it also raises the question of undesired penetration of impurities in laser-generated nanoparticles in liquids.
While doping is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. We suggest a new way to dope nanoparticles using laser ablation in liquids. While doping of semiconductors or oxides is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. In this paper, we show that pulsed laser ablation of an undoped solid target in an aqueous solution containing activator ions offers a new way to synthesise doped-nanoparticles. The doping efficiency is evaluated for laser ablation of an undoped Gd$_2$O$_3$ target in aqueous solutions of EuCl$_3$ with molar concentration from 10$^{−5}$ mol L$^{−1}$ to 10$^{−3}$ mol L$^{−1}$. Thanks to luminescence experiments, we show that the europium ions penetrate the core of the synthesised monoclinic Gd$_2$O$_3$ nanoparticles. We also show that the concentration of the activators in the nanoparticles is proportional to the initial concentration in europium ions in the aqueous solution, and a doping of about 1% ([Eu]/[Gd] atomic ratio) is reached. On the one hand, this work could open new ways for the synthesis of doped nanomaterials. On the other hand, it also raises the question of undesired penetration of impurities in laser-generated nanoparticles in liquids. While doping of semiconductors or oxides is crucial for numerous technological applications, its control remains difficult especially when the material is reduced down to the nanometric scale. In this paper, we show that pulsed laser ablation of an undoped solid target in an aqueous solution containing activator ions offers a new way to synthesise doped-nanoparticles. The doping efficiency is evaluated for laser ablation of an undoped Gd 2 O 3 target in aqueous solutions of EuCl 3 with molar concentration from 10 −5 mol L −1 to 10 −3 mol L −1 . Thanks to luminescence experiments, we show that the europium ions penetrate the core of the synthesised monoclinic Gd 2 O 3 nanoparticles. We also show that the concentration of the activators in the nanoparticles is proportional to the initial concentration in europium ions in the aqueous solution, and a doping of about 1% ([Eu]/[Gd] atomic ratio) is reached. On the one hand, this work could open new ways for the synthesis of doped nanomaterials. On the other hand, it also raises the question of undesired penetration of impurities in laser-generated nanoparticles in liquids. |
| Author | Laguta, Valentyn Nikl, Martin Amans, David Ledoux, Gilles Dujardin, Christophe Jarý, Vít zslav Trichard, Florian Laurens, Gaétan Chemin, Arsène Lam, Julien Motto-Ros, Vincent |
| AuthorAffiliation | Institut Lumière Matière CNRS Université Libre de Bruxelles Univ Claude Bernard Lyon 1 Inst Phys AS CR Center for Nonlinear Phenomena and Complex Systems Univ Lyon |
| AuthorAffiliation_xml | – name: Inst Phys AS CR – name: Université Libre de Bruxelles – name: Institut Lumière Matière – name: CNRS – name: Univ Lyon – name: Univ Claude Bernard Lyon 1 – name: Center for Nonlinear Phenomena and Complex Systems |
| Author_xml | – sequence: 1 givenname: Arsène surname: Chemin fullname: Chemin, Arsène – sequence: 2 givenname: Julien surname: Lam fullname: Lam, Julien – sequence: 3 givenname: Gaétan surname: Laurens fullname: Laurens, Gaétan – sequence: 4 givenname: Florian surname: Trichard fullname: Trichard, Florian – sequence: 5 givenname: Vincent surname: Motto-Ros fullname: Motto-Ros, Vincent – sequence: 6 givenname: Gilles surname: Ledoux fullname: Ledoux, Gilles – sequence: 7 givenname: Vít zslav surname: Jarý fullname: Jarý, Vít zslav – sequence: 8 givenname: Valentyn surname: Laguta fullname: Laguta, Valentyn – sequence: 9 givenname: Martin surname: Nikl fullname: Nikl, Martin – sequence: 10 givenname: Christophe surname: Dujardin fullname: Dujardin, Christophe – sequence: 11 givenname: David surname: Amans fullname: Amans, David |
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| Title | Doping nanoparticles using pulsed laser ablation in a liquid containing the doping agent |
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