Wettability and Adhesion of Polyethylene Powder Treated with Non-Equilibrium Various Gaseous Plasma in Semi-Industrial Equipment

Plasma treatment of polyethylene powder was carried out in low-pressure gaseous plasma sustained in a semi-industrial reactor powered with a microwave source, in which it was specifically worked with the residual atmosphere. Timed applications of plasma-treated powder in air atmosphere were carried...

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Published in:	Materials Vol. 15; no. 2; p. 686
Main Authors:	Jelínek Šourková, Hana, Weberová, Zuzana, Antoň, Jakub, Špatenka, Petr
Format:	Journal Article
Language:	English
Published:	Switzerland MDPI AG 17-01-2022 MDPI
Subjects:	Adhesion Argon Atoms & subatomic particles Composite materials Contact angle Equilibrium Fluidized bed reactors Hydrogen Low pressure Microscopy Nitrogen Oxygen Plasma Polyethylene Polyethylenes Polymers Radiation Sintering (powder metallurgy) Wettability uniformity wettability plasma treatment adhesion polyethylene (LLDPE) powder
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Abstract	Plasma treatment of polyethylene powder was carried out in low-pressure gaseous plasma sustained in a semi-industrial reactor powered with a microwave source, in which it was specifically worked with the residual atmosphere. Timed applications of plasma-treated powder in air atmosphere were carried out to study their influence on the adhesion. Based on wettability and adhesion, a treatment time of 5 min was selected for the study of other working gases (nitrogen, oxygen, hydrogen, argon and a mixture of nitrogen and hydrogen). The measurements of wettability showed the highest adhesion increase for nitrogen. The highest increase of adhesion and of surface oxygen contain shown by oxygen treatment. By contrast, treatment with hydrogen resulted in increased roughness of the sintered surface of the powder. The selection of appropriate working gases which are not standard in industrial processes enables one to atypically regulate the adhesion or wettability.
AbstractList	Plasma treatment of polyethylene powder was carried out in low-pressure gaseous plasma sustained in a semi-industrial reactor powered with a microwave source, in which it was specifically worked with the residual atmosphere. Timed applications of plasma-treated powder in air atmosphere were carried out to study their influence on the adhesion. Based on wettability and adhesion, a treatment time of 5 min was selected for the study of other working gases (nitrogen, oxygen, hydrogen, argon and a mixture of nitrogen and hydrogen). The measurements of wettability showed the highest adhesion increase for nitrogen. The highest increase of adhesion and of surface oxygen contain shown by oxygen treatment. By contrast, treatment with hydrogen resulted in increased roughness of the sintered surface of the powder. The selection of appropriate working gases which are not standard in industrial processes enables one to atypically regulate the adhesion or wettability.
Author	Weberová, Zuzana Špatenka, Petr Jelínek Šourková, Hana Antoň, Jakub
AuthorAffiliation	Department of Materials Engineering, Faculty of Mechanical Engineering, Czech Technical University in Prague, Karlovo Náměstí 13, 121 35 Prague, Czech Republic; hana.sourkova@fs.cvut.cz (H.J.Š.); zuzana.weberova@fs.cvut.cz (Z.W.); jakub.anton@fs.cvut.cz (J.A.)
AuthorAffiliation_xml	– name: Department of Materials Engineering, Faculty of Mechanical Engineering, Czech Technical University in Prague, Karlovo Náměstí 13, 121 35 Prague, Czech Republic; hana.sourkova@fs.cvut.cz (H.J.Š.); zuzana.weberova@fs.cvut.cz (Z.W.); jakub.anton@fs.cvut.cz (J.A.)
Author_xml	– sequence: 1 givenname: Hana orcidid: 0000-0002-9644-468X surname: Jelínek Šourková fullname: Jelínek Šourková, Hana organization: Department of Materials Engineering, Faculty of Mechanical Engineering, Czech Technical University in Prague, Karlovo Náměstí 13, 121 35 Prague, Czech Republic – sequence: 2 givenname: Zuzana orcidid: 0000-0002-9684-6654 surname: Weberová fullname: Weberová, Zuzana organization: Department of Materials Engineering, Faculty of Mechanical Engineering, Czech Technical University in Prague, Karlovo Náměstí 13, 121 35 Prague, Czech Republic – sequence: 3 givenname: Jakub orcidid: 0000-0002-7754-8379 surname: Antoň fullname: Antoň, Jakub organization: Department of Materials Engineering, Faculty of Mechanical Engineering, Czech Technical University in Prague, Karlovo Náměstí 13, 121 35 Prague, Czech Republic – sequence: 4 givenname: Petr surname: Špatenka fullname: Špatenka, Petr organization: Department of Materials Engineering, Faculty of Mechanical Engineering, Czech Technical University in Prague, Karlovo Náměstí 13, 121 35 Prague, Czech Republic
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/35057406$$D View this record in MEDLINE/PubMed
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Cites_doi	10.1016/S0927-7757(03)00242-5 10.3390/polym13060965 10.1016/j.apsusc.2005.02.099 10.1002/ppap.200800115 10.1007/s00396-003-0871-8 10.1016/j.polymdegradstab.2013.04.014 10.1002/ppap.201200062 10.1016/j.apsusc.2014.03.177 10.1002/ppap.201400097 10.1002/app.1991.070420228 10.1103/PhysRev.17.273 10.1016/S0169-4332(03)00879-1 10.1016/S0927-7757(97)00109-X 10.1002/sia.2923 10.3390/ma12030441 10.1088/1361-6463/aa748a 10.3390/ma11060885 10.1002/sia.5403 10.1016/S0032-3861(02)00847-9 10.1088/0963-0252/25/4/045006 10.1007/s11090-008-9126-2 10.1016/S0168-583X(03)00644-X 10.1016/j.reactfunctpolym.2004.06.003 10.1088/0022-3727/41/22/225209 10.1088/1361-6595/aad486 10.1002/ppap.201800175 10.1002/ppap.201800133 10.1016/j.vacuum.2013.02.008 10.1016/j.jiec.2016.08.021 10.1163/156856194X00267 10.3390/coatings9020145 10.1016/j.eurpolymj.2006.02.001
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Keywords	uniformity wettability plasma treatment adhesion polyethylene (LLDPE) powder
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SubjectTerms	Adhesion Argon Atoms & subatomic particles Composite materials Contact angle Equilibrium Fluidized bed reactors Hydrogen Low pressure Microscopy Nitrogen Oxygen Plasma Polyethylene Polyethylenes Polymers Radiation Sintering (powder metallurgy) Wettability
Title	Wettability and Adhesion of Polyethylene Powder Treated with Non-Equilibrium Various Gaseous Plasma in Semi-Industrial Equipment
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