Phonolite Material as Catalyst Support for the Hydrotreatment of Gas Oil and Vegetable Oil Type Feedstocks

Phonolite material has shown to be promising catalyst support for the deoxygenation of triglycerides. In this work, we continue with our previous research by synthesising and testing three acid-treated phonolite-supported Co-Mo, Ni-Mo and Ni-W catalysts for the hydrotreating of atmospheric gas oil a...

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Published in:	Materials Vol. 15; no. 1; p. 386
Main Authors:	de Paz Carmona, Héctor, Frątczak, Jakub, Tišler, Zdeněk, Hidalgo Herrador, José Miguel
Format:	Journal Article
Language:	English
Published:	Switzerland MDPI AG 05-01-2022 MDPI
Subjects:	Alkanes Biodiesel fuels Biofuels Catalysts Consumption Deoxygenation Experiments Gas oil Molybdenum Nickel Oils & fats Rapeseed Rapeseed oil Sulfur Triglycerides Vegetable oils United States > US Germany natural materials co-processing phonolite hydrotreating hydrotreated vegetable oil
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Abstract	Phonolite material has shown to be promising catalyst support for the deoxygenation of triglycerides. In this work, we continue with our previous research by synthesising and testing three acid-treated phonolite-supported Co-Mo, Ni-Mo and Ni-W catalysts for the hydrotreating of atmospheric gas oil and co-processing with rapeseed oil at industrial operating conditions (350-370 °C, WHSV 1-2 h , 5.5 MPa) in the continuous regime for more than 270 h. The phonolite-supported catalysts showed hydrotreating activity comparable with commercial catalysts, together with a complete conversion of triglycerides into n-alkanes. During co-processing, the Ni-promoted catalyst showed strong stability, with similar activity previous to the rapeseed oil addition. Our results enable us to evaluate the suitability of phonolite as catalyst support for the development of plausible alternatives to conventional hydrotreating catalysts for the co-processing of middle distillates with vegetable oils.
AbstractList	Phonolite material has shown to be promising catalyst support for the deoxygenation of triglycerides. In this work, we continue with our previous research by synthesising and testing three acid-treated phonolite-supported Co-Mo, Ni-Mo and Ni-W catalysts for the hydrotreating of atmospheric gas oil and co-processing with rapeseed oil at industrial operating conditions (350–370 °C, WHSV 1–2 h−1, 5.5 MPa) in the continuous regime for more than 270 h. The phonolite-supported catalysts showed hydrotreating activity comparable with commercial catalysts, together with a complete conversion of triglycerides into n-alkanes. During co-processing, the Ni-promoted catalyst showed strong stability, with similar activity previous to the rapeseed oil addition. Our results enable us to evaluate the suitability of phonolite as catalyst support for the development of plausible alternatives to conventional hydrotreating catalysts for the co-processing of middle distillates with vegetable oils. Phonolite material has shown to be promising catalyst support for the deoxygenation of triglycerides. In this work, we continue with our previous research by synthesising and testing three acid-treated phonolite-supported Co-Mo, Ni-Mo and Ni-W catalysts for the hydrotreating of atmospheric gas oil and co-processing with rapeseed oil at industrial operating conditions (350–370 °C, WHSV 1–2 h −1 , 5.5 MPa) in the continuous regime for more than 270 h. The phonolite-supported catalysts showed hydrotreating activity comparable with commercial catalysts, together with a complete conversion of triglycerides into n-alkanes. During co-processing, the Ni-promoted catalyst showed strong stability, with similar activity previous to the rapeseed oil addition. Our results enable us to evaluate the suitability of phonolite as catalyst support for the development of plausible alternatives to conventional hydrotreating catalysts for the co-processing of middle distillates with vegetable oils. Phonolite material has shown to be promising catalyst support for the deoxygenation of triglycerides. In this work, we continue with our previous research by synthesising and testing three acid-treated phonolite-supported Co-Mo, Ni-Mo and Ni-W catalysts for the hydrotreating of atmospheric gas oil and co-processing with rapeseed oil at industrial operating conditions (350-370 °C, WHSV 1-2 h , 5.5 MPa) in the continuous regime for more than 270 h. The phonolite-supported catalysts showed hydrotreating activity comparable with commercial catalysts, together with a complete conversion of triglycerides into n-alkanes. During co-processing, the Ni-promoted catalyst showed strong stability, with similar activity previous to the rapeseed oil addition. Our results enable us to evaluate the suitability of phonolite as catalyst support for the development of plausible alternatives to conventional hydrotreating catalysts for the co-processing of middle distillates with vegetable oils.
Author	Frątczak, Jakub Tišler, Zdeněk Hidalgo Herrador, José Miguel de Paz Carmona, Héctor
AuthorAffiliation	1 ORLEN UniCRE a.s., Revoluční 1521/84, 400 01 Ústí nad Labem, Czech Republic; jakub.fratczak@orlenunicre.cz (J.F.); zdenek.tisler@orlenunicre.cz (Z.T.); jose.hidalgo@orlenunicre.cz (J.M.H.H.) 2 Department of Chemistry, Faculty of Agrobiology, Food and Natural Resources, Czech University of Life Sciences Prague, Kamýcká 129, 165 00 Prague, Czech Republic
AuthorAffiliation_xml	– name: 1 ORLEN UniCRE a.s., Revoluční 1521/84, 400 01 Ústí nad Labem, Czech Republic; jakub.fratczak@orlenunicre.cz (J.F.); zdenek.tisler@orlenunicre.cz (Z.T.); jose.hidalgo@orlenunicre.cz (J.M.H.H.) – name: 2 Department of Chemistry, Faculty of Agrobiology, Food and Natural Resources, Czech University of Life Sciences Prague, Kamýcká 129, 165 00 Prague, Czech Republic
Author_xml	– sequence: 1 givenname: Héctor orcidid: 0000-0002-8849-0977 surname: de Paz Carmona fullname: de Paz Carmona, Héctor organization: ORLEN UniCRE a.s., Revoluční 1521/84, 400 01 Ústí nad Labem, Czech Republic – sequence: 2 givenname: Jakub orcidid: 0000-0001-6188-5728 surname: Frątczak fullname: Frątczak, Jakub organization: Department of Chemistry, Faculty of Agrobiology, Food and Natural Resources, Czech University of Life Sciences Prague, Kamýcká 129, 165 00 Prague, Czech Republic – sequence: 3 givenname: Zdeněk orcidid: 0000-0003-3457-1285 surname: Tišler fullname: Tišler, Zdeněk organization: ORLEN UniCRE a.s., Revoluční 1521/84, 400 01 Ústí nad Labem, Czech Republic – sequence: 4 givenname: José Miguel orcidid: 0000-0002-5397-1578 surname: Hidalgo Herrador fullname: Hidalgo Herrador, José Miguel organization: ORLEN UniCRE a.s., Revoluční 1521/84, 400 01 Ústí nad Labem, Czech Republic
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Keywords	natural materials co-processing phonolite hydrotreating hydrotreated vegetable oil
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Snippet	Phonolite material has shown to be promising catalyst support for the deoxygenation of triglycerides. In this work, we continue with our previous research by...
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SubjectTerms	Alkanes Biodiesel fuels Biofuels Catalysts Consumption Deoxygenation Experiments Gas oil Molybdenum Nickel Oils & fats Rapeseed Rapeseed oil Sulfur Triglycerides Vegetable oils
Title	Phonolite Material as Catalyst Support for the Hydrotreatment of Gas Oil and Vegetable Oil Type Feedstocks
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